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51. 发明专利

JPS6348328A PRODUCTION OF THERMOSETTING HYDROCARBON RESIN 失效
公开(公告)号：JPS6348328A
公开(公告)日：1988-03-01
申请号：JP19111086
申请日：1986-08-14
申请人： OTANI SUGIRO , FUJI SEKYU KK , FUJI STANDARD RES INC
发明人： OTANI SUGIRO , OKADA SHINICHI , SASAKI TAKUMI , ARAI TOMIO
IPC分类号： C08J3/24 , C08G61/00 , C08G61/02 , C10C3/02 , C10C3/10
摘要： PURPOSE:To obtain the title resin of a high softening point, by reacting a starting material based on a benzene ring-bearing condensed polycyclic aromatic compound with a specified crosslinking agent in the presence of an acid catalyst in a water solvent. CONSTITUTION:A starting material (A) (e.g., coal tar) obtained from petroleum or coal and based on a condensed polycyclic aromatic compound having 2-5 benzene nuclei, having an aromatic carbon fraction >=0.6, an aromatic ring hydrogen content >=30% and an MW >=200, is reacted with a crosslinking agent (B) [e.g., di(hydroxymethyl)benzene] based on an aromatic compound having at least two hydroxymethyl or halomethyl group in a molar ratio of 0.2-10 at 70-300 deg.C and an autogenous pressure in the presence of 1-50wt%, based on components A and B, acid catalyst (C) (e.g., sulfuric acid) in 0.5-10pts.wt., per pt.wt. components A and B, water solvent (D) until the yield reaches 60% of the theoretical value, and the reaction is stopped by cooling the reaction mixture to 70 deg.C or below.

52. 发明专利

JPS6348326A PRODUCTION OF THERMOSETTING HYDROCARBON RESIN 失效
公开(公告)号：JPS6348326A
公开(公告)日：1988-03-01
申请号：JP19110886
申请日：1986-08-14
申请人： OTANI SUGIRO , FUJI SEKYU KK , FUJI STANDARD RES INC
发明人： OTANI SUGIRO , OKADA SHINICHI , HASEBE YOSHIAKI , ARAI TOMIO
IPC分类号： C10C3/02 , C08G61/00 , C08G61/02
摘要： PURPOSE:To produce the title resin of a highsoftening point and a high yield of carbonization, by reacting a starting material based on a benzene ring-bearing condensed polycyclic aromatic compound with a specified crosslinking agent in the presence of an acid catalyst in a hydrocarbon solvent. CONSTITUTION:A starting material (A) (e.g., coal tar) obtained from petroleum or coal and based on a condensed polycyclic aromatic compound having an aromatic carbon fraction >=0.6, an aromatic ring hydrogen content >=30% and an MW >=200, is reacted with a crosslinking agent (B) [e.g., di (hydroxymethyl) benzene] based on an aromatic compound having at least two hydroxymethyl or halomethyl groups in a molar ratio of 0.2-10 at 70-300 deg.C and a pressure of normal pressure to 20kg/cm G in the presence of 0.2-20wt%, based on (A+B), acid catalyst (C) (e.g., sulfuric acid) in 0.5-10pts.wt., per pt.wt. components A and B, hydrocarbon solvent (D) (e.g., n-heptane). The reaction is stopped by cooling the reaction mixture to 70 deg.C or below when the yield reaches at least 60% of the theoretical value.

53. 发明专利

JPS62283856A IMPERMEABLE CARBON MATERIAL AND MANUFACTURE 失效
公开(公告)号：JPS62283856A
公开(公告)日：1987-12-09
申请号：JP12450286
申请日：1986-05-29
申请人： OTANI SUGIRO , IBIDEN CO LTD
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C04B14/36 , C04B26/04 , C08K3/04 , C08L65/00 , C09K3/10

54. 发明专利

JPS62283807A IMPERMEABLE CARBON MATERIAL AND ITS PRODUCTION 失效
公开(公告)号：JPS62283807A
公开(公告)日：1987-12-09
申请号：JP12450186
申请日：1986-05-29
申请人： OTANI SUGIRO , IBIDEN CO LTD
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C04B35/52 , C01B31/02 , C01B31/04 , C08K3/00 , C08L65/00 , C09K3/10
摘要： PURPOSE:To develop an impermeable carbon material which has a high carbonization rate and is small in shrinkage at the time of carbonization by subjecting a thermally cured molding consisting of a thermosetting intermediate product which is obtd. by a reaction of a mixture composed of a condensed polycyclic arom. compd., arom. crosslinking agent and acid catalyst and a specific aggregate to thermal curing and molding, then carbonizing the molding. CONSTITUTION:The mixture composed of the condensed polycyclic arom. compd. which is a deriv. consisting of naphthalene, etc., as main skeleton, heavy gravity oils of coal and petroleum, tar, etc., and the oxide, sulfide, halide, etc. of said materials, the arom. crosslinking agent consisting of 1 or >=2 arom. rings contg. a hydroxyl methyl group, etc., and the acid catalyst such as aluminum chloride or phosphoric acid or the thermosetting intermediate product obtd. by the thermal reaction of such mixture is compounded with the aggregate such as fibers and granular particles of carbon or graphite. Such mixture is heated to 100-400 deg.C in an oxidative or nonoxidative atmosphere and is plasticized. The mixture is thereafter thermally cured and molded to the prescribed shape and is heated in succession to carbonize and further to graphitize the same. The impermeable carbon material which has high carbonization rate, is small in shrinkage at the time of carbonization and has intricate shape is thus produced.

55. 发明专利

JPS62275011A IMPERMEABLE CARBON MATERIAL AND ITS PRODUCTION 失效
公开(公告)号：JPS62275011A
公开(公告)日：1987-11-30
申请号：JP12450386
申请日：1986-05-29
申请人： OTANI SUGIRO , IBIDEN CO LTD
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C01B31/02 , C01B31/04 , C04B14/36 , C04B26/04 , C04B35/52 , C08K3/04 , C08L65/00 , C09K3/10
摘要： PURPOSE:To produce an impermeable carbon material having superior heat and chemical resistances, dimensional stability and strength by combining a specified thermosetting composition with a carbonaceous or graphitic skeleton material treated with an aromatic cross-linking agent and by molding the resulting composite body by heat curing. CONSTITUTION:The surface of a carbonaceous or graphitic skeleton material having hydrogen, halogen, hydroxyl or other functional groups on the surface is treated with an aromatic cross-linking agent having one or more aromatic rings each having two or more hydroxymethyl or halomethyl groups. A mixture of a condensed polycyclic aromatic compound having oxygen, sulfur, halogen or the like in the molecule having two or more rings with said aromatic cross-linking agent and an acid catalyst is prepd. or the mixture is brought into a reaction by heating to prepare a thermosetting intermediate reaction product. The treated skeleton material is combined with the thermosetting composition and the resulting composite body is plasticized at 100-400 deg.C in an oxidizing or nonoxidizing atmosphere and molded by heat curing. Thus, the skeleton materials and the thermosetting composition are bonded to each other with the aromatic cross-linking agent in-between and an impermeable carbon material suitable for various machine parts is obtd.

56. 发明专利

JPS62156124A CARBON OR GRAPHITE PRECURSOR WITH THERMOSETTING RESIN AS BINDER 失效
公开(公告)号：JPS62156124A
公开(公告)日：1987-07-11
申请号：JP29741485
申请日：1985-12-28
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： OTANI SUGIRO , MAEDA YOSHIHIRO
IPC分类号： C08L65/00 , C01B31/02 , C08G61/00 , C08G61/02
摘要： PURPOSE:To provide the titled precursor outstanding in dimensional stability and carbonization yield, capable of control of its physical properties, consisting of aggregates having surface functional group and specific thermosetting resin as binder both of which are mutually bonding through the surface-treating agent. etc. consisting mainly of the crosslinking component in said binder. CONSTITUTION:First, a thermosetting composition (generally, a B-stage resin) as the binder is prepared by reaction between (A) condensed polycyclic aromatic compound (e.g. heavy oil, tar, pitch, naphthalene), (B) aromatic crosslinking agent having at least two hydroxy-methyl and/or halomethyl groups (e.g. p- xylylene dichloride) and (C) acid catalyst (e.g p-toluenesulfonic acid) subsequently, aggregates having surface functional group, treated with surface-treating agent consisting mainly of the component B in said binder (or incorporated with the component B as an additive) and the binder mentioned above are blended to obtain the objective precursor.

57. 发明专利

JPS62138569A ELECTRICALLY CONDUCTIVE ADHESIVE 失效
公开(公告)号：JPS62138569A
公开(公告)日：1987-06-22
申请号：JP27977785
申请日：1985-12-12
申请人： IBIDEN CO LTD , OTANI SUGIRO
发明人： OTANI SUGIRO , KAKEGAWA HIROYA
IPC分类号： C09J9/02 , C09J11/04 , C09J11/06 , C09J145/00 , C09J159/00 , C09J165/00 , C09J201/00 , H01B1/12
摘要： PURPOSE:An electrically conductive adhesive, obtained by reacting a condensed polycyclic aromatic compound with an aromatic crosslinking agent and acid catalyst and further reacting the resultant thermosetting composition with an electrically conducting promotion catalyst, capable of exhibiting electric conductivity without containing an electrically conductive aggregate and having improved heat resistance, thermal conductivity, etc. CONSTITUTION:An electrically conductive adhesive obtained by reacting a condensed polycyclic aromatic compound, preferably naphthalene, etc., with an aromatic crosslinking agent, preferably p-xylylene dichloride, etc., and an acid catalyst, preferably aluminum chloride, etc., preferably at 0.5-4.0molar ratio of the aromatic crosslinking agent to the condensed polycyclic aromatic compound using the acid catalyst in an amount of 0.5-10wt% based on the mixture of the condensed polycyclic aromatic compound with the aromatic crosslinking agent while heating and further reacting the resultant thermosetting composition with an electrically conducting promotion catalyst, preferably an oxidixing agent, e.g. air, or a mixture thereof with aluminum chloride. USE:A heat-resistant material, electromagnetic wave shielding material, etc.

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