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41. 发明授权

US5462923A 1-oxo-substituted and unsubstituted isobutyl-4-ethoxy-benzenes and mixtures thereof with bicyclopentadiene derivatives, uses of same in perfumery and methods for preparing same 失效
标题翻译： 1-氧代取代和未取代的异丁基-4-乙氧基苯及其与双环戊二烯衍生物的混合物，在香料中的用途及其制备方法
公开(公告)号：US5462923A
公开(公告)日：1995-10-31
申请号：US299966
申请日：1994-09-02
申请人： Michael G. Monteleone , Richard A. Weiss , Mark D. Evans , Marie R. Hanna
发明人： Michael G. Monteleone , Richard A. Weiss , Mark D. Evans , Marie R. Hanna
IPC分类号： C07C45/46 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0061 , C07C45/46
摘要： Described are 1-oxo-substituted and unsubstituted isobutyl-4-ethoxy-benzenes and mixtures thereof with bicyclopentadiene derivatives, wherein the 1-oxo-substituted and unsubstituted isobutyl-4-ethoxy-benzenes are defined according to the structure: ##STR1## wherein Y.sub.1 represents one of the moieties: ##STR2## and wherein the bicyclopentadiene derivatives are defined according to the structure: ##STR3## wherein Z.sub.1 and Z.sub.2 represent hydrogen, C.sub.1 -C.sub.3 lower alkyl or C.sub.2 -C.sub.3 acyl and Z.sub.3 represents methyl or hydrogen with the proviso that Z.sub.1 and Z.sub.2 are not both hydrogen, and uses thereof in augmenting, enhancing or imparting aromas in and to perfume compositions, colognes, perfumed polymers and perfumed articles.
摘要翻译：描述的是1-氧代取代的和未取代的异丁基-4-乙氧基苯及其与双环戊二烯衍生物的混合物，其中1-氧代取代和未取代的异丁基-4-乙氧基 - 苯根据以下结构定义：es：[CH2 ]，或，其中双环戊二烯衍生物根据以下结构定义：其中Z1和Z2表示氢，C1-C3低级烷基或C2-C3酰基，Z3表示甲基或氢，条件是 Z1和Z2不同时为氢，也可用于增加，增强或赋予香料组合物，古龙水，加香聚合物和香料制品中的香气。

42. 发明授权

US5274133A p-Methylenedioxyphenyl propionitrile derivatives, process for producing same, intermediates used in said process and organoleptic uses of said derivatives and intermediates 失效
标题翻译：对亚甲二氧基苯基丙腈衍生物，其制备方法，所述方法中使用的中间体和所述衍生物和中间体的感官用途
公开(公告)号：US5274133A
公开(公告)日：1993-12-28
申请号：US6605
申请日：1993-01-21
申请人： Anubhav P. S. Narula , John J. De Virgilio , Charles E. J. Beck , Marie R. Hanna , Jan T. Van Elst
发明人： Anubhav P. S. Narula , John J. De Virgilio , Charles E. J. Beck , Marie R. Hanna , Jan T. Van Elst
IPC分类号： C07D317/58 , C07D317/60 , C11B9/00
CPC分类号： C07D317/60 , C07D317/58 , C11B9/0076
摘要： Described are p-methylenedioxyphenyl propionitrile and prophiohydroxylamine derivatives defined according to the generic structure: ##STR1## wherein Z.sub.1 represents the moiety: ##STR2## and the moiety: ##STR3## and R.sub.1 is hydrogen or methyl and also having the generic structure; ##STR4## wherein X is HSO.sub.4.sup.- ; SO.sub.4 ; .sup.= Cl.sup.- ; BR.sup.- ; PO.sub.4 ; H.sub.2 PO.sub.4.sup.- ; and HPO.sub.4.
摘要翻译：描述了根据通用结构定义的对亚甲二氧基苯基丙腈和起始羟基胺衍生物：其中Z1表示部分：其中R1是氢或甲基，并且还具有通用结构; 其中X是HSO4-; SO4; = Cl-; BR-; PO4; H2PO4-; 和HPO4。

43. 发明授权

US4822515A Ethyl norbornyl alkyl ethers, organoleptic uses thereof and process for preparing same 失效
标题翻译：乙基降冰片基烷基醚，其感官用途及其制备方法
公开(公告)号：US4822515A
公开(公告)日：1989-04-18
申请号：US213318
申请日：1988-06-30
申请人： Mark A. Sprecker , Margo Androulakis , Marie R. Hanna
发明人： Mark A. Sprecker , Margo Androulakis , Marie R. Hanna
IPC分类号： C07C43/18 , C11B9/00 , C11D3/50 , C11D7/18
CPC分类号： C11D3/3956 , C07C43/18 , C11B9/0042 , C11B9/0046 , C11D3/50
摘要： Described are ethyl norbornyl alkyl ethers of our invention defined according to the generic structure: ##STR1## wherein R represents 1-C.sub.2, 1-C.sub.4 or 1-C.sub.6 straight chain lower alkyl and organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to bleach compositions, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations. Also described is a process for preparing such ethyl norbornyl alkyl ethers of our invention by means of reaction of compounds defined according to the structure: ##STR2## and/or compounds defined according to the structure: ##STR3## in admixture with compounds having the structure: ##STR4## with hydrogen in the presence of a hydrogenation catalyst.
摘要翻译：描述了根据以下通用结构定义的本发明的乙基降冰片烷基烷基醚：其中R代表1-C2，1-C4或1-C6直链低级烷基和感官用途，用于增强或增强香料组合物的香气包括但不限于漂白组合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，加香聚合物，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。还描述了通过根据以下结构定义的化合物的反应来制备本发明的这种乙基降冰片基烷基醚的方法：＆lt; IMAGE＆gt;和/或根据以下结构定义的化合物：＆lt; IMAGE＆gt;与具有结构的化合物：在氢化催化剂存在下用氢气。

44. 发明授权

US4622172A Alkyl-substituted spiroundecenone derivatives, organoleptic utility thereof and processes for preparing same 失效
标题翻译：烷基取代的十六烯酮衍生物，其感官效用及其制备方法
公开(公告)号：US4622172A
公开(公告)日：1986-11-11
申请号：US805739
申请日：1985-12-06
申请人： William L. Schreiber , William D. Gillaspey , Futoshi Fujioka , Marie R. Hanna
发明人： William L. Schreiber , William D. Gillaspey , Futoshi Fujioka , Marie R. Hanna
IPC分类号： C07C45/66 , C07C45/69 , C07C45/72 , C07C45/74 , C07C45/75 , C07C49/497 , C07C49/623 , C07C49/647 , C11B9/00 , C07C49/603
CPC分类号： C11B9/0057 , C07C45/66 , C07C45/69 , C07C45/72 , C07C45/74 , C07C45/75 , C07C49/497 , C07C49/623 , C07C49/647
摘要： Described are alkyl-substituted spiroundecenone derivatives defined according to the structure: ##STR1## wherein R.sub.1 represents isopropyl or hydrogen; R.sub.2, R.sub.3 and R.sub.4 are the same and each represents methyl or hydrogen; with the provisos that:(i) when R.sub.1 is isopropyl, R.sub.2, R.sub.3 and R.sub.4 are hydrogen; and(ii) when R.sub.2, R.sub.3 and R.sub.4 are each methyl, R.sub.1 is hydrogen,and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles and hair preparations; as well as processes for preparing said alkyl-substituted spiroundecenone derivatives.
摘要翻译：描述了根据以下结构定义的烷基取代的十六烯酮衍生物：其中R 1表示异丙基或氢; R2，R3和R4相同，各自表示甲基或氢; 条件是：（i）当R 1是异丙基时，R 2，R 3和R 4是氢; 和（ii）当R 2，R 3和R 4各自为甲基时，R 1为氢，并且其用于增强或增强香料组合物，古龙水和香料制品的香气，包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品和头发制剂; 以及制备所述烷基取代的十六烯酮衍生物的方法。

45. 发明授权

US4549982A 1-Oxoalkyl-2-isopropylnorbornane derivatives, uses thereof in augmenting or enhancing the aroma of consumable materials and processes for preparing same 失效
标题翻译： 1-氧代烷基-2-异丙基降冰片烷衍生物，其用于增强或增强消耗材料的香气及其制备方法
公开(公告)号：US4549982A
公开(公告)日：1985-10-29
申请号：US644058
申请日：1984-08-24
申请人： John B. Hall , Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
发明人： John B. Hall , Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
IPC分类号： C07C31/137 , C07C33/12 , C07C45/62 , C07C45/69 , C07C49/323 , C07C49/553 , C11B9/00 , C07C49/115 , A61K7/46
CPC分类号： C11B9/0046 , C07C31/137 , C07C33/12 , C07C45/62 , C07C45/69 , C07C49/323 , C07C49/553
摘要： Described are 1-oxoalkyl-2-isopropylnorbornane derivatives defined according to the generic structure: ##STR1## wherein X represents a moiety selected from the group consisting of: ##STR2## wherein the dashed line represents a carbon-carbon double bond or a carbon-carbon single bond and wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that R.sub.1 and R.sub.2 are not both methyl, and uses thereof in augmenting or enhancing the aroma of consumable materials selected from the group consisting of perfume compositions, colognes and perfumed articles. Also described are processes for preparing said 1-oxoalkyl-2-isopropylnorbornane derivatives by means of a low temperature catalytic Diels Alder reaction or high temperature thermal Diels Alder reaction between a bicyclopentadiene derivative and 2-methyl-3- buten-5-one according to the reaction: ##STR3## wherein R represents methyl or hydrogen.
摘要翻译：描述根据以下通用结构定义的1-氧代烷基-2-异丙基降冰片烷衍生物：其中X表示选自以下的部分：其中虚线表示碳 - 碳双键或碳 - 碳单键，其中R 1和R 2表示氢或甲基，条件是R 1和R 2不是甲基，以及其用于增强或增强从由香料组合物，古龙水和香料制品组成的组中选择的可消耗材料的香气的用途。还描述了通过低温催化Diels Alder反应或双环戊二烯衍生物与2-甲基-3-丁烯-5-酮之间的高温热狄尔斯阿尔德反应制备所述1-氧代烷基-2-异丙基降冰片烷衍生物的方法，根据反应：其中R表示甲基或氢。

46. 发明授权

US4525364A Flavoring with a macrocyclic carbonate 失效
标题翻译：用大环碳酸酯调味
公开(公告)号：US4525364A
公开(公告)日：1985-06-25
申请号：US623446
申请日：1984-06-22
申请人： Wilhelmus J. Wiegers , Augustinus G. Van Loveren , Marie R. Hanna , Domenick Luccarelli, Jr. , David R. Bowen , Manfred H. Vock
发明人： Wilhelmus J. Wiegers , Augustinus G. Van Loveren , Marie R. Hanna , Domenick Luccarelli, Jr. , David R. Bowen , Manfred H. Vock
IPC分类号： C07D321/00 , C11B9/00 , A23L1/226 , A23L1/235
CPC分类号： C07D321/00 , C11B9/0084
摘要： Described is a class of macrocyclic carbonates defined according to the structure: ##STR1## wherein n is an integer of from 1 up to 8 and m is an integer of from 1 up to 8 and where n and m may be the same or different and organoleptic uses thereof in augmenting or enhancing the aroma or taste of foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, perfume compositions, colognes and perfumed articles (i.e. solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders and perfumed polymers).
摘要翻译：描述了根据以下结构定义的一类大环碳酸酯：其中n是1至8的整数，m是1至8的整数，并且其中n和m可以相同或不同，用于增强或增强食品，口香糖，牙膏，药用产品，咀嚼烟草，香水组合物，古龙水和香料制品（即固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物）的芳香或味道的感官用途，织物柔软剂制品，化妆粉和加香聚合物）。

47. 发明授权

US4524020A Isopropyl substituted cyclohexenyl methyl ketones and perfumery uses thereof 失效
标题翻译：异丙基取代的环己烯基甲基酮及其香料用途
公开(公告)号：US4524020A
公开(公告)日：1985-06-18
申请号：US643827
申请日：1984-08-24
申请人： Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
IPC分类号： C07C45/69 , C07C49/543 , C11B9/00 , A61K7/46 , C07C49/21
CPC分类号： C11B9/0034 , C07C45/69 , C07C49/543
摘要： Described are isopropyl substituted cyclohexenyl methyl ketones defined according to the structure: ##STR1## wherein R.sub.1, R.sub.2, R.sub.11 and R.sub.21 each represents hydrogen or methyl with the provisos that:(a) at least two of R.sub.1, R.sub.21, R.sub.2 and R.sub.11 represent hydrogen;(b) either R.sub.2 is methyl and R.sub.21 is hydrogen or R.sub.21 is methyl and R.sub.2 is hydrogen; and(c) R.sub.1 is methyl only when R.sub.2 is methyl and R.sub.11 is methyl only when R.sub.21 is methyl,as well as uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers.
摘要翻译：描述了根据以下结构定义的异丙基取代的环己烯基甲基酮：其中R 1，R 2，R 11和R 21各自表示氢或甲基，条件是：（a）R 1，R 21，R 2和R 11中的至少两个表示氢 ; （b）R2是甲基，R21是氢或R21是甲基，R2是氢; 和（c）仅当R 2为甲基时，R 1为甲基，R 21为甲基时，R 21为甲基时，R 11为甲基，以及其用于增强或增强香料组合物，古龙水和香料的芳香物质的用途，包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂和加香聚合物。

48. 发明授权

US4476042A Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, organoleptic uses thereof and processes for preparing same 失效
公开(公告)号：US4476042A
公开(公告)日：1984-10-09
申请号：US546384
申请日：1983-10-28
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , A61K7/46 , C11B9/00
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represents hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

49. 发明授权

US4446060A Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, organoleptic uses thereof and processes for preparing same 失效
公开(公告)号：US4446060A
公开(公告)日：1984-05-01
申请号：US478353
申请日：1983-03-24
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , A61K7/46 , C11B9/00
CPC分类号： C07C47/445 , A24B15/345 , C07C47/347
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 take separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

50. 发明授权

US5767305A Cyclopropyl carboxylic acid esters and uses thereof in imparting, augmenting and enhancing aromas 失效
标题翻译：环丙基羧酸酯及其在赋予，增强和增强香味中的用途
公开(公告)号：US5767305A
公开(公告)日：1998-06-16
申请号：US832094
申请日：1997-04-03
申请人： Michael G. Monteleone , Gail I. Malcolm , Marie R. Hanna , Marc D. Evans
发明人： Michael G. Monteleone , Gail I. Malcolm , Marie R. Hanna , Marc D. Evans
IPC分类号： C07C69/74 , C11B9/00 , C11D3/50
CPC分类号： C11B9/003 , C07C69/74 , C11D3/50
摘要： Described are cyclopropyl carboxylic acid esters defined according to the structure: ##STR1## or the structure: ##STR2## wherein R.sub.1 is cis-3-hexenyl or cyclohexyl methyl and R.sub.2 is one of n-hexyl, cis-3-hexenyl, cyclohexyl methyl or n-heptyl and uses thereof in augmenting, enhancing or imparting aromas in or to perfume compositions, colognes and perfumed articles. The compounds having the structure: ##STR3## are novel compounds.
摘要翻译：根据以下结构定义的环丙基羧酸酯：其中R 1是顺式-3-己烯基或环己基甲基，R 2是正己基，顺式-3-己烯基，环己基甲基或正庚基及其用途来增强，增强或赋予香料或香水组合物，古龙水和香料制品中的香味。具有以下结构的化合物：是新化合物。

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