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31. 发明授权

US07780927B2 Spinning tube in tube reactors and their methods of operation 有权
标题翻译：管式反应器中的旋转管及其操作方法
公开(公告)号：US07780927B2
公开(公告)日：2010-08-24
申请号：US12034533
申请日：2008-02-20
申请人： Richard A Holl
发明人： Richard A Holl
IPC分类号： B01J8/08
CPC分类号： B01J19/1843 , B01F7/008 , B01J2219/00189
摘要： A spinning tube in tube reactor has the usual elongated transverse annular cross section reaction passage through which reactants pass to force reaction between them; the passage being between the rotor tube exterior surface and the stator tube interior surface. The radial dimension of the annual passage should be keep as uniform as possible so as not to cause unwanted variations in the reaction. This has proven difficult in prior constructions owing to the small radial dimension (e.g. 50-300 micrometers) and inevitable manufacturing tolerances in the bearings supporting the rotor. In apparatus of the invention the rotor is suspended within the stator passage by a flexible connection between the drive motor shaft and the rotor and uniformity is maintained by the so-called hydrodynamic effect which will become operative in such a narrow passage. Thus, if any part of the rotor surface moves radially from the central position closer to the stator surface the liquid viscosity produces a force that moves the rotor back to the central position. Preferably the flexible connection consists of two serially connected flexible connectors.
摘要翻译：管式反应器中的纺丝管具有通常的细长的横向环形横截面反应通道，反应物通过该反应通道迫使它们之间的反应; 该通道位于转子管外表面和定子管内表面之间。年度通道的径向尺寸应尽可能保持均匀，以免反应产生不必要的变化。由于小的径向尺寸（例如50-300微米）和支撑转子的轴承中的不可避免的制造公差，这在现有结构中已被证明是困难的。在本发明的装置中，转子通过驱动电动机轴和转子之间的柔性连接悬挂在定子通道内，并且通过所谓的流体动力学效应来保持均匀性，这将在这样狭窄的通道中起作用。因此，如果转子表面的任何部分从靠近定子表面的中心位置径向移动，则液体粘度产生使转子回到中心位置的力。优选地，柔性连接由两个串联连接的柔性连接器组成。

32. 发明授权

US12117390B2 Method and apparatus for monitoring production of a material in a liquid dispersion in real time 有权
公开(公告)号：US12117390B2
公开(公告)日：2024-10-15
申请号：US17630978
申请日：2020-07-27
申请人： Imperial College Innovations Limited
发明人： Camille Petit , Omar Matar , Jason Stafford
IPC分类号： G01N21/25 , B01J19/00 , B01J19/18 , C01B32/19 , C01B32/225 , G01N21/85 , G01N21/84
CPC分类号： G01N21/255 , B01J19/0006 , B01J19/1843 , C01B32/19 , C01B32/225 , G01N21/85 , B01J2219/00186 , C01B2204/04 , C01P2004/24 , C01P2006/60 , G01N2021/8411
摘要： A method for monitoring the production of a material such as graphene in a liquid dispersion in real time, comprises supplying the liquid dispersion to a fluid gap defined between a first layer and an opposed second layer, wherein the first layer is light-transmissive and wherein the second layer has a diffusely reflective surface facing the first layer. The diffusely reflective surface is illuminated with light from a light source and light reflected from the diffusely reflective surface is detected at an associated photodetector. A light path from the light source to the photodetector comprises the light passing through the transmissive layer towards the diffusely reflective surface through the fluid gap, reflecting off the diffusely reflective surface and passing back through the fluid gap towards and onwards through the transmissive layer.

33. 发明授权

US10493422B2 Fouling protection for an oligomerization reactor inlet 有权
公开(公告)号：US10493422B2
公开(公告)日：2019-12-03
申请号：US16262164
申请日：2019-01-30
申请人： Chevron Phillips Chemical Company LP
发明人： Steven M. Bischof , Orson L. Sydora , Jared T. Fern , Uriah J. Kilgore
IPC分类号： B01J19/26 , C07C2/08 , B01J23/26 , B01J19/18 , C07C2/32 , B01J4/00 , B01J8/00
CPC分类号： B01J19/1843 , B01J4/001 , B01J4/002 , B01J8/003 , B01J19/1806 , B01J19/26 , C07C2/08 , C07C2/32 , B01J23/26 , B01J2208/00902 , B01J2219/00247 , B01J2219/00252 , B01J2219/00254 , C07C2/32 , C07C11/02 , C07C2/08 , C07C11/107 , C07C2/08 , C07C11/02
摘要： Disclosed herein are systems and processes which prevent fouling of a reactor inlet of an oligomerization reactor. The systems and processes involve placement of an inlet sleeve around at least a portion of a reactor inlet such that a curtain of inert material flows through an annular space coaxially with respect to an outer surface of the end of the reactor inlet and into the reactor.

34. 发明申请

US20150352391A1 HYDROTHERMAL OXIDATION DEVICE FOR TREATING A MATERIAL IN A SUPERCRITICAL MEDIUM AND IMPLEMENTATION METHOD 有权
标题翻译：用于处理超临界介质材料和实施方法的氢氧化设备
公开(公告)号：US20150352391A1
公开(公告)日：2015-12-10
申请号：US14760567
申请日：2014-01-20
申请人： COMMISSARIAT À L 'ÉNERGIE ATOMIQUE ET AUX ÉNERGIES ALTERNATIVES
发明人： Jean Christophe RUIZ , Hubert-Alexandre TURC , Frederic CHARTON
IPC分类号： A62D3/38 , B01J19/18
CPC分类号： A62D3/38 , A62D2101/20 , B01J3/008 , B01J3/02 , B01J19/1812 , B01J19/1843 , B01J2208/00761 , B01J2219/00083 , B01J2219/00087 , B01J2219/0009 , B01J2219/00135 , B01J2219/00761 , Y02P20/544
摘要： A hydrothermal oxidation device for treatment of a material in a supercritical medium includes a main body, an internal tube installed inside the main body to form an annular zone along the main body, a stirring mechanism installed in an internal zone of the internal tube and actuated by a rotating shaft, a cooling mechanism to cool the treated material located in the internal zone of the internal tube, an inlet for water and oxidant mix, an effluents outlet, an inlet for material to be treated, located at one end of the main body, this inlet opening up into the internal tube. The oxidation device includes an inlet for a diluted effluent, located in the flange and connected to a preheating coil arranged along an internal wall of the main body and extending from its first end to its second end, the preheating coil opening up into the internal tube.
摘要翻译：用于处理超临界介质中的材料的水热氧化装置包括主体，安装在主体内部的内管，以沿着主体形成环形区域;搅拌机构，安装在内管的内部区域中并致动通过旋转轴，用于冷却位于内管内部区域中的处理材料的冷却机构，用于水和氧化剂混合物的入口，流出物出口，待处理材料的入口，位于主体的一端身体，这个入口打开进入内管。氧化装置包括用于稀释流出物的入口，其位于凸缘中并且连接到沿着主体的内壁布置并且从其第一端延伸到其第二端的预热线圈，预热线圈开口进入内管。

35. 发明授权

US08187551B2 Method and apparatus for manufacturing trichlorosilane 有权
标题翻译：制造三氯硅烷的方法和装置
公开(公告)号：US08187551B2
公开(公告)日：2012-05-29
申请号：US12461147
申请日：2009-08-03
申请人： Toshiyuki Ishii , Eiji Komai , Harumi Satoh
发明人： Toshiyuki Ishii , Eiji Komai , Harumi Satoh
IPC分类号： B01J19/00 , C01B33/107
CPC分类号： C01B33/107 , B01J19/006 , B01J19/1812 , B01J19/1843 , B01J19/2415 , B01J19/244 , B01J2219/00006 , B01J2219/00087 , B01J2219/00159 , B01J2219/00779 , C01B33/10757
摘要： An apparatus 1 for manufacturing trichlorosilane includes a decomposition furnace 2 into which polymers and hydrogen chloride are introduced, the decomposition furnace 2 includes: a heating device 11 which heats an interior of the decomposition furnace 2; a reaction chamber 4 which is formed in the decomposition furnace; a center tube 3 which is inserted in the reaction chamber 4 along a longitudinal direction of the reaction chamber and has a lower-end opening portion 3a; raw-material-supply pipes 5 and 6 which supplies the polymer and the hydrogen chloride to the reaction chamber 4 at an exterior of the center tube 3; and a gas-discharge pipe 7 which leads out reacted gas from the center tube 3, the apparatus 1 further includes a fin 14 that leads the polymer and the hydrogen chloride to the lower-end opening portion 3a of the center tube 3 so as to stir the polymer and the hydrogen chloride.
摘要翻译：用于制造三氯硅烷的装置1包括分解炉2，其中引入聚合物和氯化氢，分解炉2包括：加热分解炉2内部的加热装置11; 在分解炉中形成的反应室4; 中心管3，其沿着反应室的长度方向插入反应室4中，并具有下端开口部3a; 在中心管3的外部向反应室4供给聚合物和氯化氢的原料供给管5,6; 以及从中心管3引出反应气体的气体排出管7，装置1还包括将聚合物和氯化氢引导到中心管3的下端开口部3a的翅片14，以便搅拌聚合物和氯化氢。

36. 发明申请

US20110203995A1 Device for performing a chemical transformation in fluidic media 有权
标题翻译：用于在流体介质中进行化学转化的装置
公开(公告)号：US20110203995A1
公开(公告)日：2011-08-25
申请号：US12931829
申请日：2011-02-11
申请人： Jonas Persson , Kjell Öberg , Fredrik Almqvist , Knut Irgum
发明人： Jonas Persson , Kjell Öberg , Fredrik Almqvist , Knut Irgum
IPC分类号： B01D15/04 , B01J8/08 , B01D17/00
CPC分类号： B01J19/28 , B01D15/02 , B01D15/1892 , B01F7/00033 , B01F7/00041 , B01F7/006 , B01F7/007 , B01F7/1625 , B01F7/163 , B01F7/1635 , B01F11/0088 , B01F13/0818 , B01J4/007 , B01J8/025 , B01J8/10 , B01J19/1843 , B01J47/00 , B01J47/10 , B01J47/11 , B01J2208/00433 , B01J2208/00442 , B01J2208/00814 , B01J2208/028 , B01J2219/00139 , B01J2219/00141 , Y10T137/0318
摘要： A device is provided for performing chemical transformation in a fluid, with a flow distributor having at least one fluid medium inlet, at least one fluid medium outlet, and at least one confinement wherein the chemical transformation is performed; and a means for rotating, rocking, wagging, or oscillating the device. At least one confinement may be equipped with a provision for providing heat, cooling, sound, light or other types of radiation, such provision being contacted to an external source through an actuator shaft. The flow distributor may be provided with sectors connected with the centrally located fluid medium inlet and a designated peripheral fluid medium outlet. The means for rotating, rocking, wagging, or oscillating the device may be an element producing magnetic fields or a shaft mechanically connected to an external actuating device.
摘要翻译：提供了一种用于在流体中进行化学转化的装置，流量分配器具有至少一个流体介质入口，至少一个流体介质出口和至少一个进行化学转化的限制; 以及用于旋转，摇摆，摇摆或摆动装置的装置。至少一个限制可以配备有用于提供热，冷却，声音，光或其他类型的辐射的设备，这种设备通过致动器轴与外部源接触。流量分配器可以设置有与中心定位的流体介质入口和指定的外围流体介质出口连接的区段。用于旋转，摇摆，摆动或摆动装置的装置可以是产生磁场的元件或机械地连接到外部致动装置的轴。

37. 发明申请

US20100034721A1 Method and apparatus for manufacturing trichlorosilane 有权
标题翻译：制造三氯硅烷的方法和装置
公开(公告)号：US20100034721A1
公开(公告)日：2010-02-11
申请号：US12461147
申请日：2009-08-03
申请人： Toshiyuki Ishii , Eiji Komai , Harumi Satoh
发明人： Toshiyuki Ishii , Eiji Komai , Harumi Satoh
IPC分类号： C01B33/08 , B01J19/24
CPC分类号： C01B33/107 , B01J19/006 , B01J19/1812 , B01J19/1843 , B01J19/2415 , B01J19/244 , B01J2219/00006 , B01J2219/00087 , B01J2219/00159 , B01J2219/00779 , C01B33/10757
摘要： An apparatus 1 for manufacturing trichlorosilane includes a decomposition furnace 2 into which polymers and hydrogen chloride are introduced, the decomposition furnace 2 includes: a heating device 11 which heats an interior of the decomposition furnace 2; a reaction chamber 4 which is formed in the decomposition furnace; a center tube 3 which is inserted in the reaction chamber 4 along a longitudinal direction of the reaction chamber and has a lower-end opening portion 3a; raw-material-supply pipes 5 and 6 which supplies the polymer and the hydrogen chloride to the reaction chamber 4 at an exterior of the center tube 3; and a gas-discharge pipe 7 which leads out reacted gas from the center tube 3, the apparatus 1 further includes a fin 14 that leads the polymer and the hydrogen chloride to the lower-end opening portion 3a of the center tube 3 so as to stir the polymer and the hydrogen chloride.
摘要翻译：用于制造三氯硅烷的装置1包括分解炉2，其中引入聚合物和氯化氢，分解炉2包括：加热分解炉2内部的加热装置11; 在分解炉中形成的反应室4; 中心管3，其沿着反应室的长度方向插入反应室4中，并具有下端开口部3a; 在中心管3的外部向反应室4供给聚合物和氯化氢的原料供给管5,6; 以及从中心管3引出反应气体的气体排出管7，装置1还包括将聚合物和氯化氢引导到中心管3的下端开口部3a的翅片14，以便搅拌聚合物和氯化氢。

38. 发明申请

US20090208389A1 SPINNING TUBE IN TUBE REACTORS AND THEIR METHODS OF OPERATION 有权
标题翻译：管式反应器中的纺丝管及其操作方法
公开(公告)号：US20090208389A1
公开(公告)日：2009-08-20
申请号：US12034533
申请日：2008-02-20
申请人： Richard A. Holl
发明人： Richard A. Holl
IPC分类号： B01J8/10
CPC分类号： B01J19/1843 , B01F7/008 , B01J2219/00189
摘要： A spinning tube in tube reactor has the usual elongated transverse annular cross section reaction passage through which reactants pass to force reaction between them; the passage being between the rotor tube exterior surface and the stator tube interior surface. The radial dimension of the annual passage should be keep as uniform as possible so as not to cause unwanted variations in the reaction. This has proven difficult in prior constructions owing to the small radial dimension (e.g. 50-300 micrometers) and inevitable manufacturing tolerances in the bearings supporting the rotor. In apparatus of the invention the rotor is suspended within the stator passage by a flexible connection between the drive motor shaft and the rotor and uniformity is maintained by the so-called hydrodynamic effect which will become operative in such a narrow passage. Thus, if any part of the rotor surface moves radially from the central position closer to the stator surface the liquid viscosity produces a force that moves the rotor back to the central position. Preferably the flexible connection consists of two serially connected flexible connectors.
摘要翻译：管式反应器中的纺丝管具有通常的细长的横向环形横截面反应通道，反应物通过该反应通道迫使它们之间的反应; 该通道位于转子管外表面和定子管内表面之间。年度通道的径向尺寸应尽可能保持均匀，以免反应产生不必要的变化。由于小的径向尺寸（例如50-300微米）和支撑转子的轴承中的不可避免的制造公差，这在现有结构中已被证明是困难的。在本发明的装置中，转子通过驱动电动机轴和转子之间的柔性连接悬挂在定子通道内，并且通过所谓的流体动力学效应来保持均匀性，这将在这样狭窄的通道中起作用。因此，如果转子表面的任何部分从靠近定子表面的中心位置径向移动，则液体粘度产生使转子回到中心位置的力。优选地，柔性连接由两个串联连接的柔性连接器组成。

39. 发明申请

US20040011746A1 Method and device for oxidising materials in supercritical water 有权
标题翻译：在超临界水中氧化材料的方法和装置
公开(公告)号：US20040011746A1
公开(公告)日：2004-01-22
申请号：US10398320
申请日：2003-04-03
发明人： Christophe Joussot-Dubien , Gerard Didier , Hubert-Alexandre Turc
IPC分类号： C02F001/72
CPC分类号： A62D3/20 , A62D2101/20 , A62D2203/10 , B01F7/00908 , B01J3/008 , B01J3/042 , B01J19/006 , B01J19/0066 , B01J19/0073 , B01J19/02 , B01J19/18 , B01J19/1843 , B01J2219/00085 , B01J2219/00094 , B01J2219/00765 , B01J2219/00777 , B01J2219/00779 , B01J2219/0263 , B01J2219/0277 , B01J2219/0286 , C02F1/74 , C02F1/78 , C02F11/086 , Y02P20/544
摘要： The present invention relates to a method for oxidization of materials in supercritical water, as well as to a device which may be used for applying this invention. The method consists of a) introducing a fluid containing water and an oxidizing agent in a ring-shaped area and through a first end of a substantially tube-shaped reactor comprising an external wall and an internal tube, b) heating the fluid in the ring-shaped area, c) introducing the heated fluid into the internal tube and simultaneously introducing material to be treated into said internal tube at the second end of the reactor, d) mixing the fluid and the material to be treated in a first portion of the internal tube, followed by cooling the obtained mixture in a second portion of the internal tube, and e) isobarically discharging the fluid/oxidized material from the reactor A, from the internal tube.
摘要翻译：本发明涉及一种用于氧化超临界水中的材料的方法，以及可用于应用本发明的装置。该方法包括：a）在环形区域中引入含有水和氧化剂的流体，并通过包含外壁和内管的基本上管状的反应器的第一端，b）加热环中的流体 c）将加热的流体引入内管，同时在反应器的第二端将待处理的材料引入所述内管，d）将流体和被处理材料混合在第一部分中内管，然后在内管的第二部分中冷却所获得的混合物，以及e）从内管将来自反应器A的流体/氧化物质均匀地排出。

40. 发明授权

US11897778B2 Zeolite synthesis in a reactor with controlled velocity profile 有权
公开(公告)号：US11897778B2
公开(公告)日：2024-02-13
申请号：US16759491
申请日：2018-11-22
申请人： BASF SE
发明人： Christian Riemann , Andrei-Nicolae Parvulescu , Ralf Boehling , Ulrich Mueller , Hans-Juergen Luetzel , Stefanie Clade , Christoph Schappert
IPC分类号： C01B39/02 , B01J19/18 , B01J19/00 , B01J19/28 , C01B39/48
CPC分类号： C01B39/02 , B01J19/0053 , B01J19/1843 , B01J19/28 , C01B39/48 , B01J2219/00029 , B01J2219/00033 , B01J2219/1943
摘要： The present invention relates to a process for the preparation of a zeolitic material, as well as to a catalyst per se as obtainable or obtained according to said process. Furthermore, the present invention relates to the use of the zeolitic material, in particular as a catalyst.

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