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31. 发明授权

US5989515A Process for producing an acidic aqueous alumina sol 失效
标题翻译：酸性水性氧化铝溶胶的制造方法
公开(公告)号：US5989515A
公开(公告)日：1999-11-23
申请号：US897084
申请日：1997-07-18
申请人： Yoshitane Watanabe , Yoshiyuki Kashima , Kiyomi Ema
发明人： Yoshitane Watanabe , Yoshiyuki Kashima , Kiyomi Ema
IPC分类号： C01F7/02 , C01F7/44 , B01J20/00 , C04B35/10
CPC分类号： B82Y30/00 , C01F7/02 , C01F7/448 , C01P2002/72 , C01P2004/10 , C01P2004/20 , C01P2004/51 , C01P2004/54 , C01P2004/64 , C01P2006/22 , C01P2006/40 , C01P2006/80
摘要： A process for producing a stable acidic aqueous alumina sol containing 50 to 300 nm of elongate secondary particles which are elongated in only one plane and formed by edge-to-edge coagulation of rectangular plate-like primary particles having a length of one side of 10 to 30 nm when observed through an electron microscope, the process comprises the steps of:(A) adding an alkali to an aqueous alumina sol containing fibrous colloidal particles of an amorphous alumina hydrate to produce a reaction mixture having a pH of 9 to 12,(B) subjecting the reaction mixture obtained in the step (A) to a hydrothermal treatment at a temperature of 110 to 250.degree. C. to produce an aqueous suspension containing an alumina hydrate having a boehmite structure, and(C) desalting the aqueous suspension obtained in the step (B) by adding water and an acid by ultrafiltration to form an acidic aqueous alumina sol having a pH of 3 to 6.
摘要翻译：一种制造含有50〜300nm的细长二次粒子的稳定的酸性水溶性氧化铝溶胶的方法，所述细长二次粒子仅在一个平面上伸长，并且通过一边长度为10的矩形板状一次粒子的边缘到边缘凝固而形成至30nm，该方法包括以下步骤：（A）向含有无定形氧化铝水合物的纤维状胶体颗粒的含水氧化铝溶胶中加入碱以产生pH为9至12的反应混合物，（B）将在步骤（A）中获得的反应混合物在110-250℃的温度下进行水热处理，以制备含有勃姆石结构的水合氧化铝的水性悬浮液，和（C）将含水悬浮液在步骤（B）中通过超滤加入水和酸，形成pH为3至6的酸性水性氧化铝溶胶。

32. 发明授权

US5196177A Production of stable aqueous silica sol 失效
标题翻译：生产稳定的水性硅胶
公开(公告)号：US5196177A
公开(公告)日：1993-03-23
申请号：US641709
申请日：1991-01-15
申请人： Yoshitane Watanabe , Yoshiyuki Kashima , Kenji Tanimoto
发明人： Yoshitane Watanabe , Yoshiyuki Kashima , Kenji Tanimoto
IPC分类号： C01B33/149
CPC分类号： C01B33/149
摘要： A sol of flat silica particles (100-1000 nm in size) is produced by the following steps (a) to (d) from an acidic aqueous sol (S.sub.0) of negatively charged silica particles (7-30 nm in diameter) and an aqueous solution (B) of basic aluminum or zirconium salt.(a) mixing 100 parts by weight (as SiO.sub.2) of the sol (S.sub.0) with 0.2-10 parts by weight (as Al.sub.2 O.sub.3 or ZrO.sub.2) of the aqueous solution (B), and adjusting the resulting sol to pH 4-7, thereby yielding a sol (S.sub.1),(b) mixing 100 parts by weight (as SiO.sub.2) of the sol (S.sub.1) with 20-200 parts by weight (as SiO.sub.2) of the sol (S.sub.0), and adjusting the resulting sol to pH 4-7, thereby yielding a sol (S.sub.2),(c) mixing 100 parts by weight (as SiO.sub.2) of the sol (S.sub.2) with the aqueous solution (B) in an amount corresponding to 2-50% of the amount (as Al.sub.2 O.sub.3 or ZrO.sub.2 in parts by weight) added to 100 parts by weight (as SiO.sub.2) of the sol (S.sub.0) used in step (a), and adjusting the resulting sol to pH 4-7, thereby yielding a sol (S.sub.3), and(d) mixing 100 parts by weight (as SiO.sub.2) of the sol (S.sub.3) with the sol (S.sub.0) in an amount corresponding to 10-95% of the amount (as SiO.sub.2 in parts by weight) added to 100 parts by weight (as SiO.sub.2) of the sol (S.sub.1) in step (b), and adjusting the resulting sol to pH 4-7, thereby yielding a sol (S.sub.4).

33. 发明授权

US4840705A Papermaking method 失效
标题翻译：造纸方法
公开(公告)号：US4840705A
公开(公告)日：1989-06-20
申请号：US147851
申请日：1988-01-25
申请人： Hisao Ikeda , Fumio Suzuki , Yoshitane Watanabe , Mitsunobu Matsumura , Yasuhiro Takahashi , Hirosi Murakami , Koichi Maeda
发明人： Hisao Ikeda , Fumio Suzuki , Yoshitane Watanabe , Mitsunobu Matsumura , Yasuhiro Takahashi , Hirosi Murakami , Koichi Maeda
IPC分类号： C08B31/12 , D21H17/29
CPC分类号： D21H17/29 , C08B31/125
摘要： Disclosed are a papermaking method comprising the steps of sheet-formation of an aqueous papermaking stock which contains a cellulose fiber or the said fiber and an inorganic filler, dewatering and drying, characterized by the addition of a starch ether derivative of a general formula (I): ##STR1## where St-O represents a starch molecule residue, R.sub.1, R.sub.2 and R.sub.3 independently represent an alkyl group having from 1 to 18 carbon atoms or a benzyl group, provided that two or more of these R.sub.1, R.sub.2 and R.sub.3 must not be a benzyl group or an alkyl group having from 5 to 18 carbon atoms at the same time, and any two of these R.sub.1, R.sub.2 and R.sub.3 may be bonded to form a cyclic structure, the said derivative containing the ether bond preferably in a degree of substitution of from 0.01 to 0.1, to the said papermaking stock in an amount of from 0.05 to 5.0% by weight of the cellulose fiber or the total of the said fiber and the inorganic filler in the said stock, as well as the said starch ether derivative of the formula (I) and a method for preparation of the said derivative.

34. 发明授权

US5780201A Ultra thin photolithographically imageable organic black matrix coating material 失效
标题翻译：超薄光刻成像有机黑色基质涂料
公开(公告)号：US5780201A
公开(公告)日：1998-07-14
申请号：US721841
申请日：1996-09-27
申请人： Ram W. Sabnis , Jonathan W. Mayo , Edith G. Hays , Terry L. Brewer , Michael D. Stroder , Akira Yanagimoto , Yasuhisa Sone , Yoshitane Watanabe , Kiyomi Ema
发明人： Ram W. Sabnis , Jonathan W. Mayo , Edith G. Hays , Terry L. Brewer , Michael D. Stroder , Akira Yanagimoto , Yasuhisa Sone , Yoshitane Watanabe , Kiyomi Ema
IPC分类号： G02B5/00 , C09D179/08 , G02B5/20 , G02F1/1335 , G03C1/73 , G03F7/00 , G09F9/30 , G03F7/004
CPC分类号： G02F1/133512 , G03F7/0007
摘要： An organic black matrix having high resistivity (.gtoreq.10.sup.11 ohm/square), high optical density (.gtoreq.2.0) at ultra thin film thicknesses (.ltoreq.1.0 microns) for improved STN and TFT pixel display applications is made possible by combining polyimide/dye solutions and mixed metal oxide pigment dispersions at a weight/weight ratio of dye to pigment of 1:15 to 3:15. The need for low resistivity carbon black, as a replacement for sputtered chrome, is negated.
摘要翻译：对于改进的STN和TFT像素显示应用，超薄膜厚度（ / = 1011欧姆/平方），高光密度（> / = 2.0））的有机黑色矩阵是可以通过将聚酰亚胺/染料溶液和混合金属氧化物颜料分散体以1:15至3:15的染料与颜料的重量/重量比组合。需要低电阻率炭黑作为溅射铬的替代品被否定。

35. 发明授权

US5100581A Method of preparing high-purity aqueous silica sol 失效
标题翻译：制备高纯度水性二氧化硅溶胶的方法
公开(公告)号：US5100581A
公开(公告)日：1992-03-31
申请号：US496254
申请日：1990-03-20
申请人： Yoshitane Watanabe , Hiromi Suzuki , Mikio Ando
发明人： Yoshitane Watanabe , Hiromi Suzuki , Mikio Ando
IPC分类号： B01J13/00 , C01B33/148
CPC分类号： B01J13/0013 , C01B33/148
摘要： A high-purity stable aqueous silica sol is prepared which has an SiO.sub.2 concentration of from 30 to 50% by weight and which is substantially free from any other polyvalent metal oxides than silica and in which the colloidal silica has a mean particle size falling within the range of from 10 to 30 millimicrons. The silica sol obtained by the method of the present invention has an extremely low content of oxides of polyvalent metals such as iron or aluminum and may therefore be employed for uses which require the absence of such metals in the silica sol, for example, as an abrasive for semiconductors.
摘要翻译：制备SiO 2浓度为30〜50重量％且与二氧化硅基本上不含任何其它多价金属氧化物的高纯度稳定水溶硅溶胶，其中胶体二氧化硅的平均粒径落在范围为10至30毫微克。通过本发明的方法获得的硅溶胶具有极低的多价金属如铁或铝的氧化物含量，因此可用于在硅溶胶中不需要这种金属的用途，例如作为半导体研磨剂。

36. 发明授权

US06632489B1 Moniliform silica sol, process for producing the same, and ink-jet recording medium 有权
标题翻译：单晶硅溶胶，其制造方法和喷墨记录介质
公开(公告)号：US06632489B1
公开(公告)日：2003-10-14
申请号：US09763965
申请日：2001-02-28
申请人： Yoshitane Watanabe , Yoshiyuki Kashima , Kiyomi Ema , Yutaka Ohmori
发明人： Yoshitane Watanabe , Yoshiyuki Kashima , Kiyomi Ema , Yutaka Ohmori
IPC分类号： B32B300
CPC分类号： B41M5/5218 , B41M2205/12 , C01B33/1485
摘要： A stable silica sol having an SiO2 concentration of 1 to 50% by weight and containing liquid-medium dispersed moniliform colloidal silica particles each having 3 or more as a ratio of D1/D2 of a particle diameter (D1 nm) measured by a dynamic light scattering method to a mean particle diameter (a particle diameter measured by a nitrogen absorption method: D2 nm) where D1 is 50 to 500 nm, and which are comprised by spherical colloidal silica particles having a mean particle diameter of 10 to 80 nm and metal oxide-containing silica bonding these spherical-colloidal silica particles, and in which the spherical colloidal silica particles link in rows in only one plane, process for producing such and a coating composition for ink receiving layers containing such a silica sol and an ink jet recording medium.
摘要翻译：一种稳定的硅溶胶，其SiO 2浓度为1〜50重量％，含有液体介质分散的单状胶体二氧化硅粒子，其分别具有3个以上的D < 具有粒径（D 1 nm的HIL> 1 / D 2 ）通过动态光散射法测量为平均粒径（通过氮吸收法测量的粒径：D 2 PDAT> nm）其中D 1 为50〜500nm，由平均粒径为10〜80nm的球形胶体二氧化硅粒子和与这些球状胶体二氧化硅粒子结合的含金属氧化物的二氧化硅粒子构成，球形胶体二氧化硅颗粒仅在一个平面中成行排列，制备方法和用于含有这种二氧化硅溶胶和喷墨记录介质的油墨接收层的涂料组合物。

37. 发明授权

US5989391A Reaction product of sulfonated amino resin and amino group-containing substance and papermaking process 失效
标题翻译：磺化氨基树脂与含氨基物质的反应产物和造纸工艺
公开(公告)号：US5989391A
公开(公告)日：1999-11-23
申请号：US945270
申请日：1997-10-27
申请人： Yoshitane Watanabe , Kiyomi Ema , Takaichi Sugiyama , Hisanobu Urahata , Michie Kaneko
发明人： Yoshitane Watanabe , Kiyomi Ema , Takaichi Sugiyama , Hisanobu Urahata , Michie Kaneko
IPC分类号： C08G12/32 , C08G12/40 , D21H17/51 , D21H21/10
CPC分类号： C08G12/40 , C08G12/32 , D21H17/51 , D21H21/10
摘要： A product obtained by reacting a sulfonated amino resin and an amino group-containing substance in a weight ratio of from 1:0.05 to 1:3.
摘要翻译： PCT No.PCT / JP96 / 01043 Sec。 371日期1997年10月27日第 102（e）1997年10月27日PCT PCT 1996年4月17日PCT公布。出版物WO96 / 34027 日期：1996年10月31日通过磺化氨基树脂与含氨基物质的重量比为1:0.05至1:3的反应获得的产物。

38. 发明授权

US5221497A Elongated-shaped silica sol and method for preparing the same 失效
标题翻译：细长形硅胶及其制备方法
公开(公告)号：US5221497A
公开(公告)日：1993-06-22
申请号：US746634
申请日：1991-08-19
申请人： Yoshitane Watanabe , Mikio Ando , Kenji Tanimoto , Tsutomu Kagamimiya , Makoto Kawashima
发明人： Yoshitane Watanabe , Mikio Ando , Kenji Tanimoto , Tsutomu Kagamimiya , Makoto Kawashima
IPC分类号： C01B33/145 , C01B33/148
CPC分类号： C01B33/148 , C01B33/145
摘要： A method for preparing a stable silica sol having an SiO.sub.2 concentration of 40% or less, the colloidal particles of said silica having a particle size of 40 to 500 nm, as measured by dynamic light-scattering and having an elongated shape having a thickness of 5 to 40 nm and an elongation of 5 to 30 times the thickness in only one plane, the method comprising the steps (a), (b) and (c): (a) mixing an aqueous solution of Ca or Mg salt with an aqueous solution of active silicic acid having an SiO.sub.2 concentration of 1 to 6% and a pH value of 2 to 5, or with an aqueous acidic silica sol having a particle size of 3 to 30 nm, an SiO.sub.2 concentration of 0.5 to 25% and a pH value of 1 to 5 in a weight ratio of 1500 to 10000 ppm of (CaO or MgO)/SiO.sub.2 ; (b) mixing an alkali metal hydroxide with the solution obtained by step (a) in a molar ratio of 20 to 300 as SiO.sub.2 /M.sub.2 O, wherein M represents an alkali metal atom; and (c) heating the mixture obtained by step (b) at 60.degree. to 300.degree. C. for 0.5 to 40 hours.
摘要翻译：制备SiO 2浓度为40％以下的稳定的二氧化硅溶胶的方法，通过动态光散射测定的所述二氧化硅的粒径为40〜500nm的胶体粒子，其厚度为（a），（b）和（c）的方法：（a）将Ca或Mg盐水溶液与 SiO 2浓度为1〜6％，pH值为2〜5的活性硅酸水溶液，或粒径为3〜30nm，SiO 2浓度为0.5〜25％的酸性硅酸水溶液，以及（CaO或MgO）/ SiO 2的重量比为1500〜10000ppm的pH值为1〜5; （b）将碱金属氢氧化物与作为SiO 2 / M 2 O的摩尔比为20〜300的步骤（a）得到的溶液混合，其中M表示碱金属原子; 和（c）将步骤（b）获得的混合物在60℃至300℃下加热0.5至40小时。

39. 发明授权

US5091009A Coating composition and a process for manufacturing the same 失效
标题翻译：涂料组合物及其制造方法
公开(公告)号：US5091009A
公开(公告)日：1992-02-25
申请号：US449817
申请日：1989-12-13
申请人： Tatsuya Nogami , Kenichi Okubi , Yoshitane Watanabe
发明人： Tatsuya Nogami , Kenichi Okubi , Yoshitane Watanabe
IPC分类号： C04B41/87 , C01B33/12 , C01G23/047 , C03B19/12 , C03C8/00 , C03C17/25 , C04B41/45 , C04B41/81 , C23C18/12 , C23D5/00
CPC分类号： C23C18/1216 , C03C17/25 , C03C17/256 , C04B41/009 , C04B41/4554 , C04B41/81 , C03C2217/212 , C03C2217/213 , C03C2218/113
摘要： A coating composition for forming an inorganic film on a glass, ceramic metal or plastic surface is obtained by hydrolyzing and condensing a metal alkoxide of the general formula:M(OR).sub.nwherein M represents a metal atom, R represents an alkyl group having 1 to 5 carbon atoms, and n represents the valence number of M in an organic solvent in the presence of an aluminum salt; and adding a deposition inhibitor which prevents the separation of the aluminum salt when a film is formed. A process for preparing the composition is also disclosed.

40. 发明授权

US4904304A Chemical grout for ground injection and method for accretion 失效
标题翻译：化学灌浆用于地面注射和吸附方法
公开(公告)号：US4904304A
公开(公告)日：1990-02-27
申请号：US137940
申请日：1987-12-28
申请人： Yoshitane Watanabe , Eiji Okumura , Mikio Ando
发明人： Yoshitane Watanabe , Eiji Okumura , Mikio Ando
IPC分类号： C09K17/00 , C09K17/02 , C09K17/46 , C09K17/48 , C09K103/00
CPC分类号： C09K17/46 , C09K8/572 , Y10S106/90
摘要： A chemical grout for ground injection which is prepared by incorporating from 0.1 to 4.5 parts by weight of sulfamic acid and from 0.2 to 10.0 parts by weight of a water soluble magnesium salt into 100 parts by weight of an aqueous sol having a pH of 8 to 10.5 and containing from 5 to 25% by weight of colloidal silica (as SiO.sub.2) having a particle size of 3 to 7 m.mu., and from 0.05 to 1.5% by weight of Na.sub.2 O. This injecting grout has a gelation time not longer than 300 minutes. Soft ground can be consolidated by using the grout.

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