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31. 发明授权

US5989515A Process for producing an acidic aqueous alumina sol 失效
标题翻译：酸性水性氧化铝溶胶的制造方法
公开(公告)号：US5989515A
公开(公告)日：1999-11-23
申请号：US897084
申请日：1997-07-18
申请人： Yoshitane Watanabe , Yoshiyuki Kashima , Kiyomi Ema
发明人： Yoshitane Watanabe , Yoshiyuki Kashima , Kiyomi Ema
IPC分类号： C01F7/02 , C01F7/44 , B01J20/00 , C04B35/10
CPC分类号： B82Y30/00 , C01F7/02 , C01F7/448 , C01P2002/72 , C01P2004/10 , C01P2004/20 , C01P2004/51 , C01P2004/54 , C01P2004/64 , C01P2006/22 , C01P2006/40 , C01P2006/80
摘要： A process for producing a stable acidic aqueous alumina sol containing 50 to 300 nm of elongate secondary particles which are elongated in only one plane and formed by edge-to-edge coagulation of rectangular plate-like primary particles having a length of one side of 10 to 30 nm when observed through an electron microscope, the process comprises the steps of:(A) adding an alkali to an aqueous alumina sol containing fibrous colloidal particles of an amorphous alumina hydrate to produce a reaction mixture having a pH of 9 to 12,(B) subjecting the reaction mixture obtained in the step (A) to a hydrothermal treatment at a temperature of 110 to 250.degree. C. to produce an aqueous suspension containing an alumina hydrate having a boehmite structure, and(C) desalting the aqueous suspension obtained in the step (B) by adding water and an acid by ultrafiltration to form an acidic aqueous alumina sol having a pH of 3 to 6.
摘要翻译：一种制造含有50〜300nm的细长二次粒子的稳定的酸性水溶性氧化铝溶胶的方法，所述细长二次粒子仅在一个平面上伸长，并且通过一边长度为10的矩形板状一次粒子的边缘到边缘凝固而形成至30nm，该方法包括以下步骤：（A）向含有无定形氧化铝水合物的纤维状胶体颗粒的含水氧化铝溶胶中加入碱以产生pH为9至12的反应混合物，（B）将在步骤（A）中获得的反应混合物在110-250℃的温度下进行水热处理，以制备含有勃姆石结构的水合氧化铝的水性悬浮液，和（C）将含水悬浮液在步骤（B）中通过超滤加入水和酸，形成pH为3至6的酸性水性氧化铝溶胶。

32. 发明授权

US5196177A Production of stable aqueous silica sol 失效
标题翻译：生产稳定的水性硅胶
公开(公告)号：US5196177A
公开(公告)日：1993-03-23
申请号：US641709
申请日：1991-01-15
申请人： Yoshitane Watanabe , Yoshiyuki Kashima , Kenji Tanimoto
发明人： Yoshitane Watanabe , Yoshiyuki Kashima , Kenji Tanimoto
IPC分类号： C01B33/149
CPC分类号： C01B33/149
摘要： A sol of flat silica particles (100-1000 nm in size) is produced by the following steps (a) to (d) from an acidic aqueous sol (S.sub.0) of negatively charged silica particles (7-30 nm in diameter) and an aqueous solution (B) of basic aluminum or zirconium salt.(a) mixing 100 parts by weight (as SiO.sub.2) of the sol (S.sub.0) with 0.2-10 parts by weight (as Al.sub.2 O.sub.3 or ZrO.sub.2) of the aqueous solution (B), and adjusting the resulting sol to pH 4-7, thereby yielding a sol (S.sub.1),(b) mixing 100 parts by weight (as SiO.sub.2) of the sol (S.sub.1) with 20-200 parts by weight (as SiO.sub.2) of the sol (S.sub.0), and adjusting the resulting sol to pH 4-7, thereby yielding a sol (S.sub.2),(c) mixing 100 parts by weight (as SiO.sub.2) of the sol (S.sub.2) with the aqueous solution (B) in an amount corresponding to 2-50% of the amount (as Al.sub.2 O.sub.3 or ZrO.sub.2 in parts by weight) added to 100 parts by weight (as SiO.sub.2) of the sol (S.sub.0) used in step (a), and adjusting the resulting sol to pH 4-7, thereby yielding a sol (S.sub.3), and(d) mixing 100 parts by weight (as SiO.sub.2) of the sol (S.sub.3) with the sol (S.sub.0) in an amount corresponding to 10-95% of the amount (as SiO.sub.2 in parts by weight) added to 100 parts by weight (as SiO.sub.2) of the sol (S.sub.1) in step (b), and adjusting the resulting sol to pH 4-7, thereby yielding a sol (S.sub.4).

33. 发明授权

US4840705A Papermaking method 失效
标题翻译：造纸方法
公开(公告)号：US4840705A
公开(公告)日：1989-06-20
申请号：US147851
申请日：1988-01-25
申请人： Hisao Ikeda , Fumio Suzuki , Yoshitane Watanabe , Mitsunobu Matsumura , Yasuhiro Takahashi , Hirosi Murakami , Koichi Maeda
发明人： Hisao Ikeda , Fumio Suzuki , Yoshitane Watanabe , Mitsunobu Matsumura , Yasuhiro Takahashi , Hirosi Murakami , Koichi Maeda
IPC分类号： C08B31/12 , D21H17/29
CPC分类号： D21H17/29 , C08B31/125
摘要： Disclosed are a papermaking method comprising the steps of sheet-formation of an aqueous papermaking stock which contains a cellulose fiber or the said fiber and an inorganic filler, dewatering and drying, characterized by the addition of a starch ether derivative of a general formula (I): ##STR1## where St-O represents a starch molecule residue, R.sub.1, R.sub.2 and R.sub.3 independently represent an alkyl group having from 1 to 18 carbon atoms or a benzyl group, provided that two or more of these R.sub.1, R.sub.2 and R.sub.3 must not be a benzyl group or an alkyl group having from 5 to 18 carbon atoms at the same time, and any two of these R.sub.1, R.sub.2 and R.sub.3 may be bonded to form a cyclic structure, the said derivative containing the ether bond preferably in a degree of substitution of from 0.01 to 0.1, to the said papermaking stock in an amount of from 0.05 to 5.0% by weight of the cellulose fiber or the total of the said fiber and the inorganic filler in the said stock, as well as the said starch ether derivative of the formula (I) and a method for preparation of the said derivative.

34. 发明授权

US5780201A Ultra thin photolithographically imageable organic black matrix coating material 失效
标题翻译：超薄光刻成像有机黑色基质涂料
公开(公告)号：US5780201A
公开(公告)日：1998-07-14
申请号：US721841
申请日：1996-09-27
申请人： Ram W. Sabnis , Jonathan W. Mayo , Edith G. Hays , Terry L. Brewer , Michael D. Stroder , Akira Yanagimoto , Yasuhisa Sone , Yoshitane Watanabe , Kiyomi Ema
发明人： Ram W. Sabnis , Jonathan W. Mayo , Edith G. Hays , Terry L. Brewer , Michael D. Stroder , Akira Yanagimoto , Yasuhisa Sone , Yoshitane Watanabe , Kiyomi Ema
IPC分类号： G02B5/00 , C09D179/08 , G02B5/20 , G02F1/1335 , G03C1/73 , G03F7/00 , G09F9/30 , G03F7/004
CPC分类号： G02F1/133512 , G03F7/0007
摘要： An organic black matrix having high resistivity (.gtoreq.10.sup.11 ohm/square), high optical density (.gtoreq.2.0) at ultra thin film thicknesses (.ltoreq.1.0 microns) for improved STN and TFT pixel display applications is made possible by combining polyimide/dye solutions and mixed metal oxide pigment dispersions at a weight/weight ratio of dye to pigment of 1:15 to 3:15. The need for low resistivity carbon black, as a replacement for sputtered chrome, is negated.
摘要翻译：对于改进的STN和TFT像素显示应用，超薄膜厚度（ / = 1011欧姆/平方），高光密度（> / = 2.0））的有机黑色矩阵是可以通过将聚酰亚胺/染料溶液和混合金属氧化物颜料分散体以1:15至3:15的染料与颜料的重量/重量比组合。需要低电阻率炭黑作为溅射铬的替代品被否定。

35. 发明授权

US5100581A Method of preparing high-purity aqueous silica sol 失效
标题翻译：制备高纯度水性二氧化硅溶胶的方法
公开(公告)号：US5100581A
公开(公告)日：1992-03-31
申请号：US496254
申请日：1990-03-20
申请人： Yoshitane Watanabe , Hiromi Suzuki , Mikio Ando
发明人： Yoshitane Watanabe , Hiromi Suzuki , Mikio Ando
IPC分类号： B01J13/00 , C01B33/148
CPC分类号： B01J13/0013 , C01B33/148
摘要： A high-purity stable aqueous silica sol is prepared which has an SiO.sub.2 concentration of from 30 to 50% by weight and which is substantially free from any other polyvalent metal oxides than silica and in which the colloidal silica has a mean particle size falling within the range of from 10 to 30 millimicrons. The silica sol obtained by the method of the present invention has an extremely low content of oxides of polyvalent metals such as iron or aluminum and may therefore be employed for uses which require the absence of such metals in the silica sol, for example, as an abrasive for semiconductors.
摘要翻译：制备SiO 2浓度为30〜50重量％且与二氧化硅基本上不含任何其它多价金属氧化物的高纯度稳定水溶硅溶胶，其中胶体二氧化硅的平均粒径落在范围为10至30毫微克。通过本发明的方法获得的硅溶胶具有极低的多价金属如铁或铝的氧化物含量，因此可用于在硅溶胶中不需要这种金属的用途，例如作为半导体研磨剂。

36. 发明授权

US6093749A Anhydrous zinc antimonate sol and method for producing the same 有权
标题翻译：无水锑酸锌溶胶及其制造方法
公开(公告)号：US6093749A
公开(公告)日：2000-07-25
申请号：US168943
申请日：1998-10-09
申请人： Yoshitane Watanabe , Osamu Tanegashima
发明人： Yoshitane Watanabe , Osamu Tanegashima
IPC分类号： C01G30/00 , C01G30/02 , C09C1/00 , C09C1/04 , C09K21/02 , B01F17/00 , B05D7/00 , C04B14/00 , C09D1/00
CPC分类号： B82Y30/00 , C01G30/00 , C01G30/02 , C09C1/0096 , C09C1/04 , C09K21/02 , C01P2002/70 , C01P2002/88 , C01P2004/04 , C01P2004/50 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2006/10 , C01P2006/12 , C01P2006/22 , C01P2006/40 , C01P2006/60 , C01P2006/80 , C01P2006/82
摘要： An anhydrous zinc antimonate sol comprising a surface-modified anhydrous zinc antimonate colloid particles dispersed in a liquid, the surface-modified anhydrous zinc antimonate colloid particles comprising anhydrous zinc antimonate colloid particles as nuclei and a silicon-containing substance coating surfaces of the colloid particles, the sol containing an amine and/or an hydroxycarboxylic acid and a method for producing the same. The anhydrous zinc antimonate sol of the present invention is useful as transparent antistatic materials for resins, plastics, glasses, paper, and magnetic tapes, etc., transparent ultraviolet absorbents, transparent heat wave absorbents, high refractive index hard coating agents, antireflective agents, and the like.
摘要翻译：包含分散在液体中的表面改性无水锑酸锌胶体粒子的无水锑酸锌溶胶，包含作为核的无水锑酸锌胶体粒子的表面改性无水锑酸锌胶体粒子和胶体粒子的含硅物质被覆表面，含有胺和/或羟基羧酸的溶胶及其制备方法。本发明的无水锑酸锌溶胶可用作树脂，塑料，玻璃，纸和磁带等透明抗静电材料，透明紫外线吸收剂，透明热波吸收剂，高折射率硬涂层剂，抗反射剂，等等。

37. 发明授权

US5998090A High optical density ultra thin organic black matrix system 失效
标题翻译：高光密度超薄有机黑色矩阵系统
公开(公告)号：US5998090A
公开(公告)日：1999-12-07
申请号：US982233
申请日：1997-12-01
申请人： Ram W. Sabnis , Terry L. Brewer , Robert E. Nichols , Edith G. Hays , Michael D. Stroder , Akira Yanagimoto , Yasuhisa Sone , Yoshitane Watanabe , Kiyomi Ema
发明人： Ram W. Sabnis , Terry L. Brewer , Robert E. Nichols , Edith G. Hays , Michael D. Stroder , Akira Yanagimoto , Yasuhisa Sone , Yoshitane Watanabe , Kiyomi Ema
IPC分类号： G03F7/004 , C09D179/08 , G02B5/00 , G02B5/20 , G02F1/1335 , G03F7/00 , G03F7/11 , C08K3/04
CPC分类号： G03F7/0007 , G02F1/133512
摘要： A high optical density, i.e., .gtoreq.3.0, at 1 micron or less film thickness, black matrix is disclosed having improved stability and shelf life as a consequence of admixing Pigment Black 7 and organic dye or dye mixtures on a polyimide polymer vehicle.
摘要翻译：公开了由于将颜料黑7和有机染料或染料混合物混合在聚酰亚胺聚合物载体上而具有改进的稳定性和保质期的高光密度，即> 1微米或更小膜厚度的> / = 3.0。

38. 发明授权

US5597512A Method for preparing elongated-shaped silica sol 失效
标题翻译：制备细长形硅胶的方法
公开(公告)号：US5597512A
公开(公告)日：1997-01-28
申请号：US323119
申请日：1994-10-14
申请人： Yoshitane Watanabe , Yoshiyuki Kashima , Hiroyuki Takagi
发明人： Yoshitane Watanabe , Yoshiyuki Kashima , Hiroyuki Takagi
IPC分类号： C01B33/148 , B01J13/00 , C01B33/141 , C01B33/151
CPC分类号： C01B33/141 , B01J13/00
摘要： A method for preparing a silica sol having an elongated shape comprising a step (a) where an aqueous solution containing a water-soluble calcium salt or a water-soluble magnesium salt or a mixture of the water-soluble calcium salt or the water-soluble magnesium salt is mixed with an aqueous colloidal solution of an active silicic acid; a step (b) where an alkaline substance is mixed with the aqueous liquid obtained in the step (a); a step (c) where a part or the whole of the mixture obtained in the step (b) is heated at 60.degree. C. or higher to obtain a heel solution and a feed solution is prepared by a part of the mixture obtained in the step (b) or a mixture separately prepared by the step (b) and the feed solution is added to the heel solution; and a step where water is evaporated during said addition step so that SiO.sub.2 concentration is concentrated to 6 to 30% by weight.
摘要翻译：一种制备具有细长形状的硅溶胶的方法，包括步骤（a），其中含有水溶性钙盐或水溶性镁盐的水溶液或水溶性钙盐或水溶性钙盐的混合物镁盐与活性硅酸的水性胶体溶液混合; 步骤（b）其中将碱性物质与步骤（a）中获得的水性液体混合; 步骤（c）将步骤（b）中获得的混合物的一部分或全部加热至60℃或更高以获得脚后跟溶液，并且通过在将步骤（b）或通过步骤（b）分开制备的混合物和进料溶液加入到脚后跟溶液中; 以及在所述添加步骤中水蒸发的步骤，使SiO 2浓度浓缩至6〜30重量％。

39. 发明授权

US4769076A Binders for manufacture of precision casting molds 失效
标题翻译：用于制造精密铸造模具的粘合剂
公开(公告)号：US4769076A
公开(公告)日：1988-09-06
申请号：US881274
申请日：1986-07-02
申请人： Yoshitane Watanabe , Akira Kitajima , Keiko Tasaki , Isamu Yuuki
发明人： Yoshitane Watanabe , Akira Kitajima , Keiko Tasaki , Isamu Yuuki
IPC分类号： B22C1/18 , B22C1/20 , B28B7/28
CPC分类号： B22C1/205
摘要： Binders for manufacture of precision casting molds are provided, which are highly stable and are advantageous in that these may impart a high strength to the green molds as obtained by forming an accumulative refractory coat layer on a water-soluble pattern and then taking off the pattern from the coat layer, that no interlayer cleavage occurs in the accumulative coat layer when the pattern is taken off in the formation of the green mold, that the binders may impart a high strength to fired molds, that the castings as obtained by the use of the present fired molds are free from the surface roughness and other surface faults and that the dimension accuracy of the castings is not deteriorated at all by the use of the present binders.The binders of the present invention are characterized by containing the following components (a), (b) and (c) and optionally (d):(a) an organo-silicasol capable of providing 5-50 parts by weight of SiO.sub.2 in the binder;(b) 1-50 parts by weight of an alkyl silicate, an alkoxy-organosilane or a mixture thereof in the binder;(c) 1-30 parts by weight of a binder-soluble amine in the binder;(d) 1-30 parts by weight of an alkoxide of Ti, Zr, Sn, Al or In or a mixture thereof in the binder.
摘要翻译：提供了用于制造精密铸造模具的粘合剂，其是高度稳定的，并且有利的是这些可以赋予生坯模具高的强度，所述模具通过在水溶性图案上形成累积的耐火涂层，然后脱模在涂层形成时，当在模具的形成中取出图案时，在累积涂层中不发生层间剥离，粘合剂可赋予烧结模具高的强度，通过使用本发明的模具没有表面粗糙度和其他表面缺陷，并且通过使用本发明的粘合剂，铸件的尺寸精度根本不劣化。本发明的粘合剂的特征在于含有以下组分（a），（b）和（c）和任选的（d）：（a）能够提供5-50重量份SiO 2的有机二氧化硅粘合剂（b）1-50重量份的粘合剂中的硅酸烷基酯，烷氧基 - 有机硅烷或它们的混合物; （c）粘合剂中1-30重量份的粘合剂可溶性胺; （d）1-30重量份的Ti，Zr，Sn，Al或In的醇盐或它们在粘合剂中的混合物。

40. 发明授权

US06632489B1 Moniliform silica sol, process for producing the same, and ink-jet recording medium 有权
标题翻译：单晶硅溶胶，其制造方法和喷墨记录介质
公开(公告)号：US06632489B1
公开(公告)日：2003-10-14
申请号：US09763965
申请日：2001-02-28
申请人： Yoshitane Watanabe , Yoshiyuki Kashima , Kiyomi Ema , Yutaka Ohmori
发明人： Yoshitane Watanabe , Yoshiyuki Kashima , Kiyomi Ema , Yutaka Ohmori
IPC分类号： B32B300
CPC分类号： B41M5/5218 , B41M2205/12 , C01B33/1485
摘要： A stable silica sol having an SiO2 concentration of 1 to 50% by weight and containing liquid-medium dispersed moniliform colloidal silica particles each having 3 or more as a ratio of D1/D2 of a particle diameter (D1 nm) measured by a dynamic light scattering method to a mean particle diameter (a particle diameter measured by a nitrogen absorption method: D2 nm) where D1 is 50 to 500 nm, and which are comprised by spherical colloidal silica particles having a mean particle diameter of 10 to 80 nm and metal oxide-containing silica bonding these spherical-colloidal silica particles, and in which the spherical colloidal silica particles link in rows in only one plane, process for producing such and a coating composition for ink receiving layers containing such a silica sol and an ink jet recording medium.
摘要翻译：一种稳定的硅溶胶，其SiO 2浓度为1〜50重量％，含有液体介质分散的单状胶体二氧化硅粒子，其分别具有3个以上的D < 具有粒径（D 1 nm的HIL> 1 / D 2 ）通过动态光散射法测量为平均粒径（通过氮吸收法测量的粒径：D 2 PDAT> nm）其中D 1 为50〜500nm，由平均粒径为10〜80nm的球形胶体二氧化硅粒子和与这些球状胶体二氧化硅粒子结合的含金属氧化物的二氧化硅粒子构成，球形胶体二氧化硅颗粒仅在一个平面中成行排列，制备方法和用于含有这种二氧化硅溶胶和喷墨记录介质的油墨接收层的涂料组合物。

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