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31. 发明授权

US4950495A Tetrahydro-5-isopropyl-2-methyl-2-thiophene acetonitrile, organoleptic uses thereof and process for preparing same 失效
公开(公告)号：US4950495A
公开(公告)日：1990-08-21
申请号：US379944
申请日：1989-07-14
申请人： Richard M. Boden , Joseph A. McGhie
发明人： Richard M. Boden , Joseph A. McGhie
IPC分类号： C07C323/54 , C07C327/28 , C07C327/32 , C07D333/24 , C11B9/00
CPC分类号： C11B9/0076 , C07C323/54 , C07C327/28 , C07C327/32 , C07D333/24 , C11B9/0011
摘要： Described is the tetrahydro-5-isopropyl-2-methyl-2-thiophene acetonitrile of our invention having the structure: ##STR1## and organoleptic uses thereof in augmenting or enhancing the aroma or taste of perfume compositions, colognes, perfumed articles, foodstuffs and chewing gums.

32. 发明授权

US4634547A Organoleptic uses of bicyclononenyl alcohols 失效
标题翻译：感官用途的双环壬烯醇
公开(公告)号：US4634547A
公开(公告)日：1987-01-06
申请号：US796430
申请日：1985-11-08
申请人： Richard M. Boden , John R. Helm
发明人： Richard M. Boden , John R. Helm
IPC分类号： C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11D3/50 , C11B9/0049
摘要： Described are oxobicyclononane derivatives and mixtures of same having the generic structure: ##STR1## wherein X, Y, X' and Y' each represents the moiety having one of the structures: ##STR2## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond with the proviso that when X' and Y' are each the moiety: ##STR3## then the dashed line at the "2-3" position is a carbon-carbon double bond and the dashed line at the "6-7" position is a carbon-carbon single bond and one of X or Y has the structure: ##STR4## and the other of X or Y has the structure: ##STR5## and with the further proviso that when X and Y are the moieties: ##STR6## then the dashed line at the "6-7" position is a carbon-carbon double bond and the dashed line at the "2-3" position is a carbon-carbon single bond and one of X' or Y' has the structure: ##STR7## and the other of X' or Y' has the structure: ##STR8## and wherein R represents hydrogen, C.sub.1 -C.sub.3 acyl or C.sub.1 -C.sub.2 alkoxy carbonyl with the major portion of the mixtures defined according to the generic structure: ##STR9## wherein one of X or Y is the moiety: ##STR10## and the other of X or Y is the moiety: ##STR11## with R being one of hydrogen, C.sub.1 -C.sub.3 acyl or C.sub.1 -C.sub.2 alkoxy carbonyl and uses thereof in augmenting or enhancing the aroma of perfume compositions, perfumed articles, perfumed polymers and colognes.
摘要翻译：描述了具有以下通用结构的氧代二环壬烷衍生物及其混合物：其中X，Y，X'和Y'各自表示具有以下结构之一的部分：其中虚线之一代表碳 - 碳单键，另一个虚线表示碳 - 碳双键，条件是当X'和Y'各自为部分时：“IMAGE”，则“2-3”位的虚线是碳 - 碳双键，“6-7”位置的虚线是碳 - 碳单键，X或Y之一具有以下结构：X或Y具有以下结构：和进一步的条件是当X和Y是部分时：“IMAGE”，则“6-7”位置处的虚线是碳 - 碳双键，“2-3”位的虚线是碳碳单键和X'或Y'之一具有以下结构：X'或Y'具有以下结构：其中R表示氢，C 1-C3酰基或C1-C2烷氧基羰基，其主要部分是根据通用结构定义的混合物：其中X或Y之一为部分：X，Y中的另一个为部分：其中R为氢，C 1 -C 3酰基或C 1 -C 2烷氧基羰基之一，其用于增强或增强香料组合物，香料制品，加香聚合物和古龙水的香气。

33. 发明授权

US4605793A Methyl substituted pinyl oxopentenes, organoleptic uses thereof and process for preparing same 失效
标题翻译：甲基取代的戊基氧代戊烯，其感官用途及其制备方法
公开(公告)号：US4605793A
公开(公告)日：1986-08-12
申请号：US630727
申请日：1984-07-13
申请人： Braja D. Mookherjee , Robert W. Trenkle , Robin K. Wolff , Richard M. Boden , Takao Yoshida
发明人： Braja D. Mookherjee , Robert W. Trenkle , Robin K. Wolff , Richard M. Boden , Takao Yoshida
IPC分类号： C07C33/12 , C07C45/50 , C07C45/74 , C11B9/00 , C07C35/22
CPC分类号： C11B9/0046 , C07C33/12 , C07C45/50 , C07C45/74
摘要： Described is a process for preparing at least one secondary alcohol of the class of methyl substituted pinyl hydroxy pentenes comprising the step of:(i) reacting alpha pinene or beta pinene with a mixture of carbon monoxide and hydrogen in the presence of a hydroformalation catalyst in order to produce at least one methyl substituted pinyl carboxyaldehyde;(ii) reacting the resulting methyl substituted pinyl carboxyaldehyde with methyl ethyl ketone in the presence of a basic catalyst; and(iii) reacting the resulting product with a reducing agent selected from the group consisting of alkali metal borohydrides and lithium aluminum hydride.
摘要翻译：描述了一种制备甲基取代的戊基羟基戊烯类的至少一种仲醇的方法，其包括以下步骤：（i）在一种氢化异构化催化剂存在下，使α-蒎烯或β-蒎烯与一氧化碳和氢气的混合物反应以产生至少一种甲基取代的哌啶基羧基甲醛; （ii）在碱性催化剂存在下使所得甲基取代的吡啶甲酰甲醛与甲基乙基酮反应; 和（iii）使所得产物与选自碱金属硼氢化物和氢化铝锂的还原剂反应。

34. 发明授权

US4591451A Methyl substituted pinyl oxopentenes and organoleptic uses thereof 失效
标题翻译：甲基取代的戊基氧代戊烯及其感官用途
公开(公告)号：US4591451A
公开(公告)日：1986-05-27
申请号：US613569
申请日：1984-05-24
申请人： Braja D. Mookherjee , Robert W. Trenkle , Robin K. Wolff , Richard M. Boden , Takao Yoshida
发明人： Braja D. Mookherjee , Robert W. Trenkle , Robin K. Wolff , Richard M. Boden , Takao Yoshida
IPC分类号： A24B15/34 , C07C45/50 , C07C45/74 , C07C49/21 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0046 , A24B15/34 , A24B15/345 , C07C45/50 , C07C45/74 , C07C49/21 , C11B9/0034
摘要： Described are methyl substituted pinyl oxopentenes and mixtures of same defined according to the structure: ##STR1## wherein Z represents methylidene pinyl oxopentenes and mixtures of same defined according to the structure: ##STR2## ethylidene defined according to the structure: ##STR3## or ethylenyl defined according to the structure: ##STR4## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents no bond; wherein n is 0 or 1 and m is 0 or 1 with the sum of n+m being equal to 1; wherein X represents carbinol having the structure: ##STR5## or ketone having the structure: ##STR6## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represent hydrogen or methyl.
摘要翻译：描述的是甲基取代的戊基氧代戊烯和根据以下结构定义的相同的混合物：其中Z代表亚甲基哌啶基氧代戊烯，以及根据以下结构定义的相同的混合物：根据以下结构定义的亚乙基：根据以下结构定义：其中虚线中的一条代表碳 - 碳单键，虚线中的另一条不表示键; 其中n为0或1，m为0或1，n + m的和为1; 其中X表示具有以下结构的甲醇：具有以下结构的结构：其中R 1，R 2，R 3和R 4表示氢或甲基。

35. 发明授权

US4587981A Use of norbornyl pyridine derivatives in augmenting or enhancing the aroma of tobacco and in flavored tobacco composition 失效
标题翻译：降冰片基吡啶衍生物在增加或增强烟草香味和调味烟草组合物中的应用
公开(公告)号：US4587981A
公开(公告)日：1986-05-13
申请号：US742326
申请日：1985-06-07
申请人： Richard M. Boden , Claude Grim
发明人： Richard M. Boden , Claude Grim
IPC分类号： C07D213/16 , C11B9/00 , A24B15/38
CPC分类号： C07D213/16 , C11B9/0092
摘要： Described is the use in (a) a process for augmenting or enhancing the aroma of tobacco; and (b) a flavored tobacco composition of norbornyl pyridine derivatives defined according to the generic structure: ##STR1## wherein R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "' and R.sub.5 "" each represents hydrogen or methyl with the proviso that at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 "' and R.sub.5 "" represent hydrogen; wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond and wherein the pyridinyl moiety is bonded to the norbornyl moiety at the 2' position of the norbornyl moiety and at either the 2 or the 4 position of the pyridinyl moiety.
摘要翻译：描述了（a）增加或增强烟草香气的过程中的用途; 和（b）根据通用结构定义的降冰片基吡啶衍生物的风味烟草组合物：其中R5，R5'，R5“，R5”和R5“”各自表示氢或甲基，条件是 R5，R5'，R5“，R5”和R5“中的至少四个表示氢; 其中虚线表示碳 - 碳单键或碳 - 碳双键，其中吡啶基部分与降冰片基部分的2'位的降冰片基部分结合，并且在吡啶基的2位或4位上部分。

36. 发明授权

US4581160A 2-acetoxy-4-(2-bornyloxy) butane and organoleptic uses thereof 失效
标题翻译： 2-乙酰氧基-4-（2-苄氧基）丁烷及其感官用途
公开(公告)号：US4581160A
公开(公告)日：1986-04-08
申请号：US698853
申请日：1985-02-06
申请人： Futoshi Fujoika , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujoika , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , A61K7/46
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277
摘要： Described is the 2-acetoxy-4-(2-bornyloxy) butane of our invention defined according to the structure: ##STR1## as well as methods for augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles by adding thereto an aroma augmenting or enhancing quantity of the 2-acetoxy-4-(2-bornyloxy) butane of our invention.
摘要翻译：描述了根据以下结构定义的本发明的2-乙酰氧基-4-（2-甲氧基）丁烷：＆lt; IMAGE＆gt;以及通过添加其来增强或增强消耗材料的香气的方法，包括香料，古龙水和香料制品香气增加或增加本发明的2-乙酰氧基-4-（2-甲氧基）丁烷。

37. 发明授权

US4554385A Tertiary hydroxyl carboxaldehydes, organoleptic uses thereof, and processes for producing same 失效
标题翻译：叔羟基醛，其感官用途及其制备方法
公开(公告)号：US4554385A
公开(公告)日：1985-11-19
申请号：US709916
申请日：1985-03-08
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： C07C47/36 , C07C47/19
CPC分类号： C07C47/36
摘要： Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines ##STR2## represent covalent carbon-carbon bonds when m does not=0; and wherein the lines ##STR3## do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines ##STR4## representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line ##STR5## represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines ##STR6## represent carbon-carbon bonds and with the line ##STR7## representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR8## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).
摘要翻译：描述的是根据通用结构定义的叔羟基醛：其中当m不为0时，线和 - - - - 和/或+ + + + +代表共价碳 - 碳键; 并且当m = 0时，线+ + + + +和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个用代表碳 - 碳键的+ + + + +和 - 当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z与所述线完成环烷基环部分，并且+ + + + +代表碳 - 碳键，并且具有不代表键的线 - - - - - 。并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜和喜欢）。

38. 发明授权

US4540812A 2-Acetoxy-4-(2-bornyloxy) butane 失效
标题翻译： 2-乙酰氧基-4-（2-苄氧基）丁烷
公开(公告)号：US4540812A
公开(公告)日：1985-09-10
申请号：US578346
申请日：1984-02-09
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , C07C69/14
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277
摘要： Described is the 2-acetoxy-4-(2-bornyloxy) butane of our invention defined according to the structure: ##STR1## as well as methods for augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles by adding thereto an aroma augmenting or enhancing quantity of the 2-acetoxy-4-(2-bornyloxy) butane of our invention.
摘要翻译：描述了根据以下结构定义的本发明的2-乙酰氧基-4-（2-甲氧基）丁烷：＆lt; IMAGE＆gt;以及通过添加其来增强或增强消耗材料的香气的方法，包括香料，古龙水和香料制品香气增加或增加本发明的2-乙酰氧基-4-（2-甲氧基）丁烷。

39. 发明授权

US4539142A 4-(2-Bornyloxy)-2-butyn-1-ol and organoleptic uses thereof 失效
标题翻译： 4-（2-呋喃氧基）-2-丁炔-1-醇及其感官用途
公开(公告)号：US4539142A
公开(公告)日：1985-09-03
申请号：US604230
申请日：1984-04-26
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , A61K7/46 , C07C5/23
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C07C2102/42 , Y10S514/951
摘要： Described is the 4-(2-bornyloxy)-2-butyn-1-ol of our invention defined according to the structure: ##STR1## as well as methods for augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles by adding thereto an aroma augmenting or enhancing quantity of the 4-(2-bornyloxy)-2-butyn-1-ol of our invention.
摘要翻译：描述了根据以下结构定义的本发明的4-（2-开氧基）-2-丁炔-1-醇，以及用于增强或增强消耗材料的香气的方法，包括香料，古龙水和香料制品通过向其中加入增加或增加本发明的4-（2-甲氧基）-2-丁炔-1-醇的香味。

40. 发明授权

US4521634A Ether carbinols and process for preparing same 失效
标题翻译：醚甲醇及其制备方法
公开(公告)号：US4521634A
公开(公告)日：1985-06-04
申请号：US574150
申请日：1984-01-26
申请人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
发明人： Futoshi Fujioka , Richard M. Boden , William L. Schreiber
IPC分类号： A24B15/34 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C11B9/00 , C07C43/188 , C07C41/06
CPC分类号： C11B9/0046 , A24B15/345 , C07C43/178 , C07C43/196 , C07C43/23 , C07C45/49 , C07C47/198 , C07C47/277 , C07C2102/42
摘要： Described are ether carbinols defined according to the generic structure: ##STR1## wherein X.sub.1 represents a moiety selected from the group consisting of: ##STR2## and wherein Y.sub.1 represents C.sub.4 or C.sub.5 alkylene or C.sub.4 or C.sub.5 alkenylene or C.sub.4 or C.sub.5 alkynylene; processes for preparing such ether carbinols by means of first reacting allyl ethers with a mixture of carbon monoxide and hydrogen by means of an oxoreaction to produce ether carboxaldehydes and then reducing the thus formed ether carboxaldehydes to ether carbinols; or reacting camphene with appropriate diols; as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; and smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carbinols.Also described are two ether carboxaldehydes having one of the structures: ##STR3## processes for preparing such ether carboxaldehydes by means of reacting out an appropriate allyl ether with a mixture of carbon monoxide and hydrogen by means of an oxo-reaction as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carboxaldehydes.
摘要翻译：描述根据通用结构定义的醚甲醇：其中X 1表示选自下列的部分：其中Y 1表示C 4或C 5亚烷基或C 4或C 5亚链烯基或C 4或C 4 C5亚炔基; 通过首先使烯丙基醚与一氧化碳和氢气的混合物通过氧化反应制备这种醚甲醇的方法，以产生醚甲醛，然后将由此形成的醚甲醛还原成醚甲醇; 或使camp烯与适当的二醇反应; 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 并通过向其中加入香烟或味道来增加或增加如此生产的醚甲醇，从而吸烟烟草和烟草制品。还描述了具有以下结构之一的两种醚甲醛：通过使一种合适的烯丙基醚与一氧化碳和氢气的混合物通过氧代反应制备这种醚甲醛的方法以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 通过向其中加入香味或味道增加或增加如此制备的醚甲醛的量来吸烟烟草和烟草制品。

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