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31. 发明专利

JP2007141601A Inorganic nano-particle composite cross-linking polymer electrolyte film, manufacturing method of the same, and film-electrode assembly using the same 有权
标题翻译：无机纳米颗粒复合物交联聚合物电解质膜，其制造方法和使用其的膜电极组件
公开(公告)号：JP2007141601A
公开(公告)日：2007-06-07
申请号：JP2005332521
申请日：2005-11-17
申请人： Japan Atomic Energy Agency , Nitto Denko Corp , 日東電工株式会社 , 独立行政法人日本原子力研究開発機構
发明人： CHIN SHINKA , YOSHIDA MASARU , ASANO MASAHARU , YAMAKI TETSUYA , TACHIBANA TOSHIMITSU , NISHIYAMA SOJI , NAGAI YOZO
IPC分类号： H01B1/06 , H01B13/00 , H01M8/02 , H01M8/10
CPC分类号： C08J5/2287 , C08J2381/08 , H01M4/921 , H01M4/926 , H01M8/0289 , H01M8/1004 , H01M8/1023 , H01M8/1051 , H01M8/106 , H01M8/1072 , H01M8/1088 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide an inorganic nano-particle composite cross-linking polymer electrolyte film excellent in ion exchange capacity, dimensional stability, oxidation resistant property, and strength, suitable for using it for a fuel cell, and a manufacturing method of the same. SOLUTION: The inorganic nano-particle composite cross-linking polymer electrolyte film is constituted of a polymeric film base material, graft molecular chain bonded to main chain skeleton of the polymeric film base material, formed by graft polymerizing vinyl monomers; sulfonic acid group bonded to the graft molecular chain, and grain-shaped inorganic material of nano-scale, uniformly dispersed in the main chain skeleton of the polymeric film base material and cross-linking structure formed by the graft molecular chain, and characterized by the cross-linking structure of the main chain skeleton of the polymeric film base material, the graft molecular chain, and the inorganic nano-particles. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供一种适用于燃料电池的离子交换能力，尺寸稳定性，抗氧化性能和强度优异的无机纳米颗粒复合交联聚合物电解质膜，以及制造方法相同。解决方案：无机纳米颗粒复合交联聚合物电解质膜由聚合物膜基材，通过接枝聚合乙烯基单体形成的聚合物膜基材的主链骨架结合的接枝分子链构成; 与接枝分子链结合的磺酸基，纳米级的颗粒状无机材料均匀分散在聚合物膜基材的主链骨架中，并由接枝分子链形成的交联结构，其特征在于：聚合物膜基材的主链骨架，接枝分子链和无机纳米颗粒的交联结构。版权所有（C）2007，JPO＆INPIT

32. 发明专利

JP2014189654A Method for manufacturing porous polymer film 审中-公开
标题翻译：制造多孔聚合物薄膜的方法
公开(公告)号：JP2014189654A
公开(公告)日：2014-10-06
申请号：JP2013066942
申请日：2013-03-27
申请人： Nitto Denko Corp , 日東電工株式会社 , Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： FURUYAMA SATORU , MURAKI YUZO , NAGAI YOZO , AMINO ICHIRO , YURI YOSUKE , YUYAMA TAKAHIRO , ISHIZAKA TOMOHISA , ISHIBORI IKUO , YOSHIDA KENICHI , MAEKAWA YASUNARI , KOSHIKAWA HIROSHI , YAMAKI TETSUYA , ASANO MASAHARU
IPC分类号： C08J7/00 , C08J9/00
CPC分类号： C08J5/18 , C08J7/123 , C08J2300/20
摘要： PROBLEM TO BE SOLVED: To provide a porous polymer film manufacturing method suitable for industrial production.SOLUTION: A method for manufacturing a porous polymer film includes: a step (I) of irradiating a polymer film with an ion beam comprising ions accelerated by a cyclotron to form a polymer film with which ions in the beam collide; and a step (II) of chemically etching the polymer film formed in the step (I) to form openings and/or through holes, corresponding to loci of ion collision, in the polymer film. In the step (I), beam current values of the ion beam are detected at the upstream and/or downstream of the polymer film in an ion beam path and controls an irradiation condition of the ion beam to the polymer film on the basis of the detected beam current values so that the irradiation density of ions with respect to the polymer film becomes a set value.
摘要翻译：要解决的问题：提供一种适用于工业生产的多孔聚合物膜制造方法。解决方案：一种多孔聚合物膜的制造方法，包括：用离子束照射聚合物膜的步骤（I），所述离子束包括由回旋加速器加速的离子以形成聚合物膜，其中所述束中的离子与所述聚合物膜碰撞; 和在步骤（I）中形成的聚合物膜的化学蚀刻步骤（II），以在聚合物膜中形成对应于离子碰撞轨迹的开口和/或通孔。在步骤（I）中，在离子束路径中在聚合物膜的上游和/或下游检测离子束的束电流值，并且基于该离子束将离子束的照射条件控制在聚合物膜上检测光束电流值，使得离子相对于聚合物膜的照射密度变为设定值。

33. 发明专利

JP2013227548A Method for producing porous polymer film and porous polymer film 有权
标题翻译：用于生产多孔聚合物薄膜和多孔聚合物薄膜的方法
公开(公告)号：JP2013227548A
公开(公告)日：2013-11-07
申请号：JP2013067306
申请日：2013-03-27
申请人： Nitto Denko Corp , 日東電工株式会社 , Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： FURUYAMA SATORU , MORIYAMA JUNICHI , NAGAI YOZO , YURI YOSUKE , ISHIBORI IKUO , YUYAMA TAKAHIRO , ISHIZAKA TOMOHISA , OKUMURA SUSUMU , MAEKAWA YASUNARI , KOSHIKAWA HIROSHI , YAMAKI TETSUYA , ASANO MASAHARU
IPC分类号： C08J9/36 , C08J9/00 , G21K5/00 , G21K5/04 , G21K5/10
CPC分类号： B29C67/20 , B01D39/1692 , B29C59/16 , B29C2035/0872 , B29D7/01 , B29K2267/003 , B29L2007/00 , C08J7/123 , C08J2367/02 , H01M4/02 , H01M4/04 , H01M4/8605 , H01M4/88 , H01M2004/021
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a porous polymer film suitable for an industrial production.SOLUTION: A method for producing a porous polymer film comprises: a step (I) for irradiating a polymer film with an ion beam constituted of accelerated ions to form a polymer film that has been bombarded with the ions in the beam; and a step (II) for chemically etching the polymer film formed in the step (I) to form, in the polymer film, openings and/or through-holes corresponding to the trajectories of bombardment of the ions. The step (I) includes: arranging the polymer film in an atmosphere having a pressure of 100 Pa or greater; passing the ion beam through a beam line held at a pressure that is lower than that of the atmosphere as well as a pressure partition sheet separating the beam line and the atmosphere, the pressure barrier sheet being arranged at a terminus of the beam line; and irradiating the polymer film which is in the atmosphere.
摘要翻译：要解决的问题：提供一种适用于工业生产的多孔聚合物膜的制造方法。解决方案：一种多孔聚合物膜的制造方法，其特征在于，包括：使用离子束照射聚合物膜的工序（I），所述离子束由加速离子以形成已经用束中的离子轰击的聚合物膜; 以及用于对步骤（I）中形成的聚合物膜进行化学蚀刻以在聚合物膜中形成与离子的轰击轨迹相对应的开口和/或通孔的步骤（II）。步骤（I）包括：将聚合物膜设置在压力为100Pa以上的气氛中; 使离子束通过保持在低于大气压力的束线的束线以及分隔射束线和大气的压力分隔片，该阻挡片布置在射束线的末端; 并照射在大气中的聚合物膜。

34. 发明专利

JP2013101841A Heat resistant polymer electrolyte membrane and method for manufacturing the same 有权
标题翻译：耐热聚合物电解质膜及其制造方法
公开(公告)号：JP2013101841A
公开(公告)日：2013-05-23
申请号：JP2011245110
申请日：2011-11-09
申请人： Univ Of Tokyo , 国立大学法人東京大学 , Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： KUDO KAZUAKI , TAKAYAMA TOSHIO , PARK JUN , ASANO MASAHARU , MAEKAWA YASUNARI
IPC分类号： H01M8/02 , C08J5/22 , H01B1/06 , H01B13/00 , H01M8/10
CPC分类号： H01M8/10 , H01M8/103 , H01M8/1067 , H01M8/1072 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide: a heat resistant polymer electrolyte membrane targeted for an electrolyte membrane for a polymer fuel cell, a water electrolytic device or the like, and having high proton conductivity, low fuel permeability, high anti-oxidation properties, and excellent mechanical characteristics under high temperature operation; and a low cost and simple manufacturing process of the heat resistant polymer electrolyte membrane.SOLUTION: A heat resistant polymer electrolyte membrane of the present invention includes a main chain containing an alicyclic polybenzimidazole and a graft chain added to the main chain by radiation graft polymerization, and at least a part of the graft chain has a sulfonic acid group.
摘要翻译：要解决的问题：提供：聚合物燃料电池用电解质膜，水电解装置等的耐热性聚合物电解质膜，具有高质子传导性，低燃料透过性，高抗氧化性性能优良，机械特性优良; 以及耐热聚合物电解质膜的低成本且简单的制造工艺。解决方案：本发明的耐热聚合物电解质膜包括通过辐射接枝聚合添加到主链中的脂环族聚苯并咪唑和接枝链的主链，并且至少一部分接枝链具有磺酸组。版权所有（C）2013，JPO＆INPIT

35. 发明专利

JP2012124157A Proton-conductive polymer electrolyte membrane having excellent oxidation resistance, and method of producing the same 有权
标题翻译：具有优异耐氧化性的导电聚合物电解质膜及其制造方法
公开(公告)号：JP2012124157A
公开(公告)日：2012-06-28
申请号：JP2011250283
申请日：2011-11-16
申请人： Japan Atomic Energy Agency , Nitto Denko Corp , 日東電工株式会社 , 独立行政法人日本原子力研究開発機構
发明人： EMORI HIDEYUKI , SUZUKI HIROSE , ASANO MASAHARU , MAEKAWA YASUNARI
IPC分类号： H01B13/00 , C08J5/22 , H01B1/06 , H01M8/02 , H01M8/10
CPC分类号： C08J5/2237 , C08F259/06 , C08J2327/16 , C08J2351/00 , H01B1/122 , H01M8/1023 , H01M8/1039 , Y02P70/56 , C08F212/04 , C08F220/06
摘要： PROBLEM TO BE SOLVED: To provide a proton-conductive polymer electrolyte membrane having excellent oxidation resistance and a method capable of producing the proton-conductive polymer electrolyte membrane on an industrial scale.SOLUTION: The method of producing a proton-conductive polymer electrolyte membrane includes the steps of: irradiating resin microparticles with a radioactive ray; producing a microparticulate graft polymer by graft-polymerizing a vinyl monomer having a sulfonic acid group precursor and a vinyl monomer having a carbonyl group equivalent onto the resin microparticles in a solid-liquid dual phase system; preparing a cast solution comprising a polymer having a phosphoric acid group or a phosphonic acid group and the graft polymer and forming a cast film from the solution; drying the cast film to produce a film; converting the sulfonic acid group precursor into a sulfonic acid group; and forming a cross-liked structure between the carbonyl group equivalents. In the production method, a liquid phase of the solid-liquid dual phase system includes the vinyl monomer and a solvent for the vinyl monomer and a solid phase includes the resin microparticles.
摘要翻译：要解决的问题：提供具有优异抗氧化性的质子传导性聚合物电解质膜和能够以工业规模生产质子传导性聚合物电解质膜的方法。解决方案：制造质子传导性聚合物电解质膜的方法包括以下步骤：用放射线照射树脂微粒; 通过将具有磺酸基前体的乙烯基单体和具有羰基当量的乙烯基单体在固液二相体系中接枝聚合到树脂微粒上来生产微粒接枝聚合物; 制备包含具有磷酸基或膦酸基的聚合物的浇铸溶液和接枝聚合物，并从溶液中形成流延膜; 干燥流延膜以产生膜; 将磺酸基前体转化成磺酸基团; 并在羰基当量之间形成交叉结构。在制造方法中，固液双相体系的液相包括乙烯基单体和乙烯基单体的溶剂，固相包括树脂微粒。版权所有（C）2012，JPO＆INPIT

36. 发明专利

JP2011249093A Cross-linked aromatic polymer electrolyte membrane and producing method thereof, and polymer fuel cell using cross-linked aromatic polymer electrolyte membrane 有权
标题翻译：交联芳族聚合物电解质膜及其制备方法，以及使用交联芳族聚合物电解质膜的聚合物燃料电池
公开(公告)号：JP2011249093A
公开(公告)日：2011-12-08
申请号：JP2010119903
申请日：2010-05-25
申请人： Japan Atomic Energy Agency , 独立行政法人日本原子力研究開発機構
发明人： CHEN JINHUA , ASANO MASAHARU , MAEKAWA YASUNARI
IPC分类号： H01B13/00 , C08J7/16 , H01B1/06 , H01M8/02 , H01M8/10
CPC分类号： Y02E60/521
摘要： PROBLEM TO BE SOLVED: To produce a cross-linked aromatic polymer electrolyte membrane that achieves both ion conductivity and the mechanical strength of a membrane.SOLUTION: A portion of a graft chain formed by graft polymerization after applying a cross-linked structure by irradiation exposure to an aromatic polymer film base material and forming the graft chain by a graft polymerization process is chemically converted into a sulfonic acid group to thereby introduce the sulfonic acid group to the graft chain.
摘要翻译：要解决的问题：制备实现离子传导性和膜的机械强度两者的交联芳族聚合物电解质膜。解决方案：通过在通过辐射暴露于芳族聚合物膜基材并且通过接枝聚合方法形成接枝链来施加交联结构之后通过接枝聚合形成的接枝链的一部分被化学转化成磺酸基从而将磺酸基引入接枝链。版权所有（C）2012，JPO＆INPIT

37. 发明专利

JP2009146758A Electrolyte membrane for fuel cell, and manufacturing method thereof 审中-公开
标题翻译：燃料电池用电解质膜及其制造方法
公开(公告)号：JP2009146758A
公开(公告)日：2009-07-02
申请号：JP2007323426
申请日：2007-12-14
申请人： Japan Atomic Energy Agency , Toyota Motor Corp , トヨタ自動車株式会社 , 独立行政法人日本原子力研究開発機構
发明人： KOBAYASHI MISAKI , YAMAKI TETSUYA , ASANO MASAHARU , YOSHIDA MASARU , MAEKAWA YASUNARI
IPC分类号： H01M8/02 , H01B1/06 , H01B13/00 , H01M8/10
CPC分类号： H01B1/122 , C08J5/2218 , H01M8/1067 , H01M8/1076 , H01M8/1079 , H01M8/1086 , H01M2008/1095 , H01M2300/0082 , Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a polymer electrolyte membrane for fuel cell which has both high proton conductivity and gas barrier performance of a polymer film substrate at the same time and is superior in humidity dimension change, tensile strength, and discharge performance, and to provide a manufacturing method thereof. SOLUTION: The polymer electrolyte membrane for fuel cell which has (1) a plurality of proton conductive paths penetrated in thickness direction of a polymer film substrate and (2) a proton conduction layer formed in layers on one or both surfaces of the polymer film substrate is manufactured through a first irradiation process in which high energy heavy ions are irradiated so as to generate active species in such a way that they penetrate in thickness direction of the polymer film substrate, a second irradiation process in which electron beams or ion beams are irradiated so as to generate active species in layers in the surface layer of the substrate, and a graft polymerization process in which, after the irradiation processes, the film substrate and a monomer are graft polymerized by adding the monomer of one kind or more selected from a group of monomers having a proton conductive functional group or capable of introducing the proton conductive functional group in a later process. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供同时具有高质子传导性和高分子膜基材的气体阻隔性能的燃料电池用聚合物电解质膜，并且具有优异的湿度尺寸变化，拉伸强度和放电性能，并提供其制造方法。解决方案：一种用于燃料电池的聚合物电解质膜，其具有（1）多个质子传导路径，在聚合物膜基材的厚度方向上穿透;以及（2）在该层的一个或两个表面上形成的质子传导层通过照射高能重离子的第一照射工艺制造聚合物膜基材，以便以这样的方式产生活性物质，使得它们在聚合物膜基材的厚度方向上穿透，其中电子束或离子照射光束以在衬底的表面层中产生层中的活性物质，以及接枝聚合方法，其中在照射工艺之后，通过添加一种或更多种的单体将膜基材和单体接枝聚合选自一组具有质子传导性官能团的单体或能够在稍后的工艺中引入质子传导性官能团。版权所有（C）2009，JPO＆INPIT

38. 发明专利

JP2009014468A Manufacturing method of biological tissue hardened body 有权
标题翻译：生物组织硬化体的制备方法
公开(公告)号：JP2009014468A
公开(公告)日：2009-01-22
申请号：JP2007175814
申请日：2007-07-04
申请人： Akita Univ , Gunma Univ , Japan Atomic Energy Agency , 国立大学法人秋田大学 , 国立大学法人群馬大学 , 独立行政法人日本原子力研究開発機構
发明人： ASANO MASAHARU , YAMAKI TETSUYA , YOSHIDA MASARU , MAEKAWA YASUNARI , ABE HIROSHI , SUZUKI YOSHIKUNI , NIBE TSUNEMI , ISHIZAWA AKIMITSU , SHU AKIRA , YORIFUJI HIROSHI , SATO MASATO
IPC分类号： G01N1/36 , A01N1/02 , G01N1/30 , G01N33/48
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method of a biological tissue hardened body preservable in the state similar to the living state unaccompanied by contraction in a short time.
SOLUTION: A biological tissue is impregnated into mixed solution acquired by combining a monofunctional vinyl monomer, a polyfunctional vinyl monomer, and a solvent together, and then polymerized by being irradiated with an ionizing radiation.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供一种生物组织硬化体的制造方法，该制造方法可以在与短时间内收缩无关的生活状态相似的状态下保存。解决方案：将生物组织浸渍在通过将单官能乙烯基单体，多官能乙烯基单体和溶剂组合在一起而获得的混合溶液中，然后通过用电离辐射照射而聚合。版权所有（C）2009，JPO＆INPIT

39. 发明专利

JP2008097868A Fuel-cell polymer electrolyte membrane imparted with silane cross-linked structure and fuel-cell membrane/electrode assembly including the same 有权
标题翻译：燃料电池聚合物电解质薄膜与硅烷交联结构和燃料电池/电极组件包括其中
公开(公告)号：JP2008097868A
公开(公告)日：2008-04-24
申请号：JP2006275122
申请日：2006-10-06
申请人： Japan Atomic Energy Agency , Nitto Denko Corp , 日東電工株式会社 , 独立行政法人日本原子力研究開発機構
发明人： YOSHIDA MASARU , ASANO MASAHARU , CHIN SHINKA , MAEKAWA YASUNARI , TACHIBANA TOSHIMITSU , NAGAI YOZO , NISHIYAMA SOJI
IPC分类号： H01M8/02 , C08F291/00 , C08J5/22 , C08J7/18 , H01B1/06 , H01B13/00 , H01M8/10
CPC分类号： C08F255/00 , C08F8/00 , C08F8/12 , C08F8/36 , C08F259/08 , C08J5/2293 , C08J7/18 , C08J2323/06 , C08J2327/18 , H01B1/122 , H01M8/1027 , H01M8/1037 , H01M8/1039 , H01M8/1044 , H01M8/106 , H01M8/1072 , H01M8/1088 , H01M2300/0082 , Y02P70/56 , C08F230/08
摘要： PROBLEM TO BE SOLVED: To provide an electrolyte membrane which can maintain excellent battery characteristics for a long period of time under high temperature and low moisture retention conditions that is the most important thing in a fuel cell. SOLUTION: A manufacturing method for a fuel-cell polymer electrolyte membrane includes a step, in which a graft molecular chain is formed by graft-polymerizing a vinylsilane coupling agent having a phenyl group capable of retaining a sulfonic acid group onto a polymer film base material, a step for introducing a sulfon acid group into a phenyl group in a graft molecular chain, and a step, in which a silane bridge structure is imparted between graft molecular chains by hydrolyzing and condensing an alkoxy group in a graft molecular chain, in turn. It is devised to obtain the fuel-cell polymer electrolyte membrane manufactured by such a manufacturing method. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种电解质膜，其可以在燃料电池中最重要的高温和低保湿条件下长时间保持优异的电池特性。解决方案：燃料电池聚合物电解质膜的制造方法包括以下步骤：其中通过将具有能够保持磺酸基的苯基的乙烯基硅烷偶联剂接枝聚合到聚合物上形成接枝分子链膜基材，将磺酸基引入接枝分子链中的苯基的步骤，以及通过在接枝分子链中水解和缩合烷氧基而在接枝分子链之间施加硅烷桥结构的步骤，反过来。设计得到通过这样的制造方法制造的燃料电池用聚合物电解质膜。版权所有（C）2008，JPO＆INPIT

40. 发明专利

JP2006282969A Method for producing functional inorganic/graft polymer hybrid ion exchange membrane and electrolyte membrane for fuel cell 有权
标题翻译：生产功能无机/聚酰胺混合离子交换膜和电解槽的电解质膜的方法
公开(公告)号：JP2006282969A
公开(公告)日：2006-10-19
申请号：JP2005108561
申请日：2005-04-05
申请人： Japan Atomic Energy Agency , Nitto Denko Corp , 日東電工株式会社 , 独立行政法人日本原子力研究開発機構
发明人： YOSHIDA MASARU , YAMAKI TETSUYA , ASANO MASAHARU , MORITA YOSUKE , NISHIYAMA SOJI , TACHIBANA TOSHIMITSU , NAGAI YOZO
IPC分类号： C08J7/16 , B01D67/00 , B01D71/02 , B01D71/26 , B01D71/28 , B01D71/32 , B01D71/34 , B01D71/36 , B01D71/44 , B01D71/48 , B01D71/56 , B01D71/64 , B01D71/78 , B01D71/82 , C08F291/18 , C08L27/18 , H01B1/06 , H01M8/02 , H01M8/10
CPC分类号： C08J5/2281 , C08J2323/06 , C08J2327/18
摘要： PROBLEM TO BE SOLVED: To solve problems: defects in a polymer ion exchange membrane such as low ion exchange capacity, low electric conductivity, in addition, bad oxidation resistance of the membrane, and the like.
SOLUTION: The polymer ion exchange membrane having excellent electroconductivity, water retentivity and oxidation resistance is produced by uniformly mixing a functional inorganic material having a function for accelerating graft polymerization of a polymerizable monomer, a function for absorbing water and a function for transmitting hydrogen ions with an organic polymer to obtain a functional inorganic/polymer membrane, irradiating radioactive rays to the functional inorganic/polymer membrane to graft polymerize or co-graft polymerize the polymerizable monomer having functional groups and introducing sulfonate groups to graft chains.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：解决问题：解决问题：离子交换容量低，导电性差，聚合物离子交换膜的缺陷，膜的耐氧化性差等。解决方案：具有优异的导电性，保水性和抗氧化性的聚合物离子交换膜通过均匀混合具有促进可聚合单体的接枝聚合功能的功能性无机材料，吸水功能和发射功能而制备氢离子与有机聚合物反应获得功能性无机/聚合物膜，向功能性无机/聚合物膜照射放射线，将具有官能团的可聚合单体和引入磺酸盐基团的接枝聚合或共聚接枝聚合到接枝链上。版权所有（C）2007，JPO＆INPIT

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