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    • 21. 发明授权
    • Process and apparatus for producing high-purity nitrogen by low-temperature fractionation of air
    • 通过空气低温分馏生产高纯度氮的工艺和设备
    • US06708523B2
    • 2004-03-23
    • US10264261
    • 2002-10-04
    • Stefan LochnerRalph SpöriMichael Lauter
    • Stefan LochnerRalph SpöriMichael Lauter
    • F25J304
    • F25J3/04412F25J3/04254F25J3/04309F25J3/0486F25J2200/54F25J2200/90F25J2210/42F25J2215/44F25J2220/42F25J2245/42Y10S62/912
    • The invention relates to a process and apparatus for producing nitrogen by low-temperature fractionation of air in a rectification system which has a high-pressure column (4) and a low-pressure column (5). Feed air (1, 3) is introduced into the high-pressure column (4). An oxygen-containing liquid fraction (11) is removed from the high-pressure column (4) and fed into the low-pressure column (5). Gaseous nitrogen (18) is extracted from the low-pressure column (5) above a mass transfer section (25), which has at least one theoretical or practical plate, and is at least partially condensed in a top condenser (17) by indirect heat exchange with a refrigerant (13). High-purity nitrogen is removed from the low-pressure column below the mass transfer section (25), and is obtained as a nitrogen product (26, 27, 30). The process and apparatus have a refrigeration-supply system, in which a refrigeration fluid (31) flows. At least part of the refrigeration fluid from the refrigeration-supply system is introduced into the low-pressure column (5) above the mass transfer section (25).
    • 本发明涉及一种在具有高压塔(4)和低压塔(5)的精馏系统中通过空气的低温分馏来生产氮的方法和装置。 进料空气(1,3)被引入高压塔(4)。 从高压塔(4)除去含氧液体馏分(11)并进料到低压塔(5)中。 气体氮(18)从传质部分(25)上方的低压塔(5)中提取,该传质部分具有至少一个理论或实用的板,并且通过间接的方式在顶部冷凝器(17)中至少部分地冷凝 与制冷剂(13)进行热交换。 从质量传递部(2​​5)下方的低压塔除去高纯氮,作为氮产物(26,27,30)得到。 该方法和装置具有其中制冷流体(31)流动的制冷供应系统。 来自制冷供应系统的制冷流体的至少一部分被引入到传质部分25上方的低压塔(5)中。