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21. 发明授权

US4248910A Reverse coating textiles with polyurethane solutions 失效
标题翻译：用聚氨酯溶液反涂纺织品
公开(公告)号：US4248910A
公开(公告)日：1981-02-03
申请号：US735664
申请日：1976-10-26
申请人： Josef Pedain , Wilhelm Thoma
发明人： Josef Pedain , Wilhelm Thoma
IPC分类号： D06M15/564 , D06N3/14 , B05D5/10
CPC分类号： D06M15/564 , D06N3/14
摘要： This invention relates to the coating of sheet-form textile materials by the reverse process using polyurethanes which, for ecological and economic reasons, are dissolved in a single organic solvent.Segmented, substantially linear polyurethanes of dihydroxy polyesters and/or dihydroxy polyethers, aromatic and/or aliphatic diisocyanates and glycols and/or diamines as chain extenders, are used as surface and adhesive coatings in the form of solutions containing only a single organic solvent. To control coating properties, solutions used for adhesive coatings contain from 1 to 15% by weight based on the weight of the solution of water in addition to the organic solvent.
摘要翻译：本发明涉及通过使用聚氨酯的相反方法对片状纺织材料进行涂布，出于生态和经济原因，聚氨酯被溶解在单一的有机溶剂中。二羟基聚酯和/或二羟基聚醚，芳族和/或脂族二异氰酸酯和作为增链剂的二元醇和/或二胺的分段的基本上线性的聚氨酯用作仅含有单一有机溶剂的溶液形式的表面和粘合剂涂层。为了控制涂层性质，除了有机溶剂之外，用于粘合剂涂料的溶液含有基于水溶液重量的1至15重量％。

22. 发明授权

US3932366A Process for the production of basic modified polyamides 失效
标题翻译：碱性改性聚酰胺生产工艺
公开(公告)号：US3932366A
公开(公告)日：1976-01-13
申请号：US532671
申请日：1974-12-13
申请人： Wilhelm Thoma , Dietrich Hildebrand , Wolf-Dieter Last , Heinrich Rinke
发明人： Wilhelm Thoma , Dietrich Hildebrand , Wolf-Dieter Last , Heinrich Rinke
IPC分类号： C08G69/14 , C08G69/48
CPC分类号： C08G69/14
摘要： This invention relates to the production of basic modified polyamides produced by the polycondensation of lactams or .omega.-aminocarboxylic acids with 0.1 to 5 mol of triamines of the formulaH.sub.2 N -- (CH.sub.2).sub.n -- NH -- (CH.sub.2).sub.n -- NH.sub.2where n equals 2 to 6 per 100 mol of lactam and 2 equivalents of carboxyl groups in the form of dicarboxylic acids and monocarboxylic acids per mol of triamine, using a molar ratio of monocarboxylic acids to dicarboxylic acids of between 10 : 1 and 1 : 20, which polyamides are dyed with reactive dyes.
摘要翻译：本发明涉及通过内酰胺或ω-氨基羧酸与0.1至5mol式H 2 N - （CH 2）n -NH - （CH 2）n -NH 2的三胺缩合产生的碱性改性聚酰胺的制备，其中n等于2 使用单羧酸与二羧酸的摩尔比为10:1至1:20，每100摩尔内酰胺和2当量二羧酸和单羧酸形式的羧基/摩尔三胺的羧基为6。用活性染料染色。

23. 发明授权

US5252671A Coating compositions for coatings that are permeable to water vapor and a process for their preparation 失效
标题翻译：可渗透水蒸气的涂料涂料组合物及其制备方法
公开(公告)号：US5252671A
公开(公告)日：1993-10-12
申请号：US887213
申请日：1992-05-21
申请人： Josef Pedain , Klaus Noll , Wilhelm Thoma , Detlef-Ingo Schutze
发明人： Josef Pedain , Klaus Noll , Wilhelm Thoma , Detlef-Ingo Schutze
IPC分类号： C14C11/00 , C08L75/00 , C09D133/04 , C09D175/00 , C09D175/04 , D06M15/564 , D06N3/04 , D06N3/14 , C08F8/30
CPC分类号： D06N3/14 , C09D133/04 , C09D175/04 , C08L75/00 , Y10S528/904
摘要： The present invention relates to coating compositions containing(A) 70 to 98% by weight, based on the sum of components (A) and (B), of(a) isocyanate-free polymers of ethylenically unsaturated monomers and/or polyurethanes or blocked isocyanate prepolymers, and(b) optional organic solvents, wherein component (A) contains no significant quantities of groups capable of reacting with component (B) or starting materials thereof and has a viscosity (at 23.degree. C.) of 2000 to 100,000 mPa.s;(B) 2 to 30% by weight, based on the sum of components (A) and (B), of a polyaddition product prepared in and dispersed in component (A), wherein the polyaddition product is a polyurethane, polyurethane urea, polyurea, or mixture thereof, containing ionic groups and/or potentially ionic groups in a quantity corresponding to from 0.5 to 20 milliequivalents per 100 g of component (B) but containing substantially no free isocyanate, hydroxyl, or amino groups: and(C) optional cross-linking agents;in which component (B) is formed in situ in component (A).
摘要翻译：本发明涉及涂料组合物，其包含（A）70至98重量％，基于组分（A）和（B）的总和，（a）烯属不饱和单体和/或聚氨酯或封闭的无异氰酸酯的聚合物异氰酸酯预聚物和（b）任选的有机溶剂，其中组分（A）不含有显着量的能够与组分（B）或其原料反应的基团，并且具有2000至100,000mPa的粘度（在23℃） .s; （B）基于组分（A）和（B）的总和，制备和分散在组分（A）中的加聚产物的2-30重量％，其中所述加聚产物是聚氨酯，聚氨酯脲，聚脲或其混合物，其含有相对于每100g组分（B）0.5至20毫当量但基本上不含游离异氰酸酯，羟基或氨基的量的离子基团和/或潜在的离子基团：和（C）任选的交联剂; 其中组分（B）在组分（A）中原位形成。

24. 发明授权

US4894428A Process for coating substrates with polyurethane ureas 失效
标题翻译：用聚氨酯脲涂层基材的方法
公开(公告)号：US4894428A
公开(公告)日：1990-01-16
申请号：US292698
申请日：1989-01-03
申请人： Wilhelm Thoma , Josef Pedain , Waldemar Kling
发明人： Wilhelm Thoma , Josef Pedain , Waldemar Kling
IPC分类号： B32B27/12 , C08G18/10 , C08G18/12 , C08G18/40 , C08G18/65 , C08G18/80 , C09D175/00 , C09D175/04 , D06M15/564 , D06N3/14
CPC分类号： D06N3/14 , C08G18/10 , C08G18/12 , C08G18/4018 , Y10T428/31551 , Y10T428/31591 , Y10T442/2566
摘要： The present invention is directed to a process for coating substrates with polyurethane ureas which is characterized in that a substrate is coated with a product, which has been obtained by the reation of (A) a prepolymer based on an aromatic polyisocyanate containing on average two ketoxime-blocked NCO groups and having an average molecular weight of about 500 to 15,000 with (B) a chain-extending agent corresponding to the formulaH.sub.2 N--R'--NH.sub.2in which R' is an aliphatic or cycloaliphatic radical, in the presence of solvents at temperatures above 50.degree. C. and at an equivalent ratio of blocked NCO groups to NH.sub.2 groups of 1.43 to 1.02, wherein after about 40 to 90% of the available amino groups have reacted, the reaction is completed with crosslinking at temperatures above 120.degree. C.The present invention is also directed to the coated substrates produced by this process.
摘要翻译：本发明涉及一种用聚氨酯脲涂覆基材的方法，其特征在于基材涂覆有产品，该产品是通过（A）基于芳族多异氰酸酯的预聚物（其平均包含平均两个酮肟）（B）相应于式H2N-R'-NH2的增链剂，其中R'是脂族或脂环族基团，在溶剂存在下，具有约500至15,000的平均分子量在高于50℃的温度下，封闭的NCO基团与NH 2基团的当量比为1.43至1.02，其中约40至90％的可用氨基已经反应后，反应在120℃以上的温度下进行交联本发明还涉及通过该方法制备的涂覆基材。

25. 发明授权

US4606974A Leveller-containing high-solids polyurethane reactive coating systems and their use for reactive coating 失效
标题翻译：含水平剂的高固体聚氨酯反应涂料体系及其用于反应涂料
公开(公告)号：US4606974A
公开(公告)日：1986-08-19
申请号：US799090
申请日：1985-11-18
申请人： Wilhelm Thoma , Karl H. Pisaric , Heinrich Alberts
发明人： Wilhelm Thoma , Karl H. Pisaric , Heinrich Alberts
IPC分类号： D06N3/14 , B32B5/24 , C08G18/10 , C09D175/04 , B32B9/04
CPC分类号： C09D175/04 , C08G18/10 , Y10T428/31551 , Y10T428/31598 , Y10T428/31612 , Y10T428/31663 , Y10T428/31786
摘要： The present invention is directed to a high-solids polyurethane reactive coating system based on blocked NCO-prepolymers, polyamines and, optionally, solvents, said coating system containing a leveller agent comprising(1) a combination of from about 1 to 10% by weight of (A) vinyl polymers and copolymers based on (meth)acrylic acid esters and, optionally, other comonomers and from about 0.1 to 2% by weight of (B) polysiloxanes and/or polyalkylene oxide/polysiloxane copolymers,(2) from about 0.2 to 2.0% by weight of (C) poly(meth)acrylic acid (hydroxy)alkyl ester graft polymers on silicones,(3) mixtures of (A), (B) and (C) in the amounts specified,(4) mixtures of (A) and (C) in the amounts specified or(5) mixtures of (B) and (C) in the amounts specified.The present invention also relates to textile substrates coated on one or both sides or surface-textured sheet-form materials, particularly velour leather, coated with the above leveller-containing, high-solids polyurethane reactive coating systems.
摘要翻译：本发明涉及一种基于封闭的NCO-预聚物，多胺和任选的溶剂的高固体聚氨酯反应性涂料体系，所述涂料体系含有矫光剂，其包含（1）约1至10重量％（A）基于（甲基）丙烯酸酯和任选的其它共聚单体的乙烯基聚合物和共聚物和约0.1至2重量％的（B）聚硅氧烷和/或聚环氧烷/聚硅氧烷共聚物的共聚物，（2）（C）聚硅氧烷上的（C）聚（甲基）丙烯酸（羟基）烷基酯接枝聚合物，（3）（A），（B）和（C）的混合物中的0.2〜2.0重量％（A）和（C）的混合物按规定的数量指定的量或（5）（B）和（C）的混合物。本发明还涉及涂覆在一面或两面上的织物基材或涂有上述均化剂的高固体聚氨酯反应涂层体系的表面纹理的片状材料，特别是丝绒革。

26. 发明授权

US4035213A Soft textile coatings resembling napa leather 失效
标题翻译：柔软的纺织品涂料类似于napa皮革
公开(公告)号：US4035213A
公开(公告)日：1977-07-12
申请号：US637202
申请日：1975-12-03
申请人： Wilhelm Thoma , Josef Pedain , Jurgen Grammel , Antonio Aguado
发明人： Wilhelm Thoma , Josef Pedain , Jurgen Grammel , Antonio Aguado
IPC分类号： C08G18/00 , C08G18/10 , C08L75/00 , C09D175/04 , D06M15/423 , D06N3/14 , D06N7/04 , B32B27/12 , B32B27/40 , B32B27/42
CPC分类号： D06N3/148 , C08G18/10 , C09D175/04 , D06N3/143 , Y10S428/904 , Y10T428/31554 , Y10T428/31594
摘要： This invention relates to the coating of textile sheets with polyurethane pastes by the reversal process for producing very soft coating articles with a hand resembling that of napa leather. The particular properties of the coating are obtained by using bonding pastes which contain a mixture which can be cross-linked by the action of heat, consisting of polyurethane hydrazodicarbonamides and melamine-formaldehyde resins and/or urea-formaldehyde resins.
摘要翻译：本发明涉及通过反转方法对具有聚氨酯浆料的纺织品片材进行涂布，以用类似于napa皮革的手制造非常柔软的涂层制品。通过使用含有可通过热作用交联的混合物的粘结浆料获得涂层的特定性质，其由聚氨酯肼二酰胺和三聚氰胺 - 甲醛树脂和/或脲 - 甲醛树脂组成。

27. 发明授权

US3984607A Polyurethane coated textile sheets 失效
标题翻译：聚氨酯涂层纺织片
公开(公告)号：US3984607A
公开(公告)日：1976-10-05
申请号：US542733
申请日：1975-01-20
申请人： Wilhelm Thoma , Bernd Quiring
发明人： Wilhelm Thoma , Bernd Quiring
IPC分类号： D06M15/564 , C08G18/00 , C08L1/00 , C08L7/00 , C08L21/00 , C08L25/12 , C08L27/00 , C08L33/00 , C08L33/02 , C08L51/00 , C08L51/02 , C08L51/04 , C08L75/00 , C08L75/04 , C08L77/00 , D06M23/00 , D06N3/14 , B32B27/40 , D06N3/04
CPC分类号： D06N3/144 , C08L25/12 , C08L75/04 , C08L51/04 , Y10S428/904 , Y10T428/31554 , Y10T428/31573 , Y10T442/259
摘要： Polyurethane coated textile sheets are disclosed and a reversal process for their preparation, wherein the textile sheets are coated by means of a top coat solution with a polymer mixture comprisingI. 50 to 90% by weight, based on the total polymer, of a substantially linear polyurethane which is substantially free of reactive end groups and which has been prepared by a process which comprises reacting an organic dihyroxyl compound of molecular weight 500 to 4000 and an organic diol of molecular weight 60 to 450 with an aromatic diisocyanate,Ii. 0 to 50% by weight of a vinyl copolymer, andIii. 1 to 50% by weight of a diene graft copolymer,Said polymer mixture having been applied to a release substrate prior to said coating process.
摘要翻译：公开了聚氨酯涂覆的织物片材及其制备的反转方法，其中织物片材通过顶涂剂溶液进行涂覆，所述顶涂层溶液具有聚合物混合物，所述聚合物混合物包含按重量计约50至90％的重量，基于总共聚合物线性聚氨酯，其基本上不含反应性末端，并且由其包含反应分子量为500至4000的有机二羟基化合物和有机重量的分子量为60至450的芳族二异氰酸酯的方法制备。 0至50％的乙烯共聚物重量，III。 1％至50％的二烯酸共聚物重量，所述聚合物混合物适用于在涂覆过程之前的释放基材。

28. 发明授权

US5716676A Aqueous coating compositions and their use for the preparation of coatings that are permeable to water vapor 失效
标题翻译：水性涂料组合物及其用于制备可渗透水蒸气的涂料的用途
公开(公告)号：US5716676A
公开(公告)日：1998-02-10
申请号：US748743
申请日：1996-11-18
申请人： Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp , Josef Pedain , Reinold Schmitz
发明人： Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp , Josef Pedain , Reinold Schmitz
IPC分类号： C08G18/08 , C08G18/28 , C08G18/44 , C08G18/50 , C14C11/00 , D06N3/14 , D21H19/62 , B05D3/02 , B05D3/00 , C14C5/00 , D06M19/00
CPC分类号： C08G18/0823 , C08G18/0804 , C08G18/0828 , C08G18/283 , C08G18/3228 , C08G18/3231 , C08G18/3855 , C08G18/44 , C08G18/5072 , C08G18/73 , C14C11/006 , D06N3/14 , D21H19/62 , Y10T428/31551 , Y10T428/31558 , Y10T428/31591
摘要： The invention relates to the use of coating compositions to prepare coatings having water vapor permeabilities of at least 2500 g/m.sup.2 per day (DS 2109 TM1 method) containing (A) a polyurethane containing (1) 0.1 to 75 meq/100 g of ionic groups and (2) 11 to 50% by weight of --(CH.sub.2 CH.sub.2 O).sub.n -- units (wherein n is 2 to 25) incorporated into the main chain prepared from reactive components comprising (I) one or more polyisocyanates, (II) one or more polyols having a number average molecular weight of 350 to 5000, with the proviso that if any such polyol is a sulfonated polyether diol having the formula ##STR1## in which R is hydrogen or an organic group having 1 to 8 carbon atoms, m and n are 1 to 10, p is 0, 1, or 2, and M is ammonium or alkali metal cation, then an additional ethoxy-containing polyether polyol must also be present, and (III) one or more chain lengthening agents having a molecular weight of 32 to 349; and (B) 30 to 80% by weight, based on the sum of components (A) and (B), of an aqueous phase.
摘要翻译：本发明涉及涂料组合物用于制备具有每天至少2500g / m 2的水蒸汽渗透性（DS 2109 TM1方法）的涂层的用途，其包含（A）含有（1）0.1至75meq / 100g离子的聚氨酯基团和（2）由反应性组分制备的主链中的 - （CH 2 CH 2 O）n - 单元（其中n为2至25）的11至50重量％，其包含（I）一种或多种多异氰酸酯，（II）一种或多种更多的数均分子量为350〜5000的多元醇，条件是如果任何这样的多元醇是具有1至8个碳原子的式基的磺化聚醚二醇，则m和n为1至10，p为0,1 或2，M是铵或碱金属阳离子，则还必须含有另外的含乙氧基的聚醚多元醇，和（III）一种或多种分子量为32至349的链延长剂; 和（B）基于水相的组分（A）和（B）的总和为30至80重量％。

29. 发明授权

US5629402A Coating compositions and their use for the preparation of coatings permeable to water vapor 失效
标题翻译：涂料组合物及其用于制备可渗透水蒸汽的涂料
公开(公告)号：US5629402A
公开(公告)日：1997-05-13
申请号：US221214
申请日：1994-03-31
申请人： Josef Pedain , Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp
发明人： Josef Pedain , Detlef-Ingo Schutze , Wilhelm Thoma , Klaus Nachtkamp
IPC分类号： C09D175/04 , C08G18/08 , C08G18/12 , C08G18/40 , C08G18/42 , C08G18/44 , C08G18/48 , C09D175/00 , D06M15/564 , D06M15/568 , D06M23/00 , D06M23/10 , D06N3/14 , C08G18/38 , C08G18/80
CPC分类号： D06N3/14 , C08G18/0804 , C08G18/12 , C08G18/4018 , C08G18/4252 , C08G18/44 , C08G18/4833 , C08G18/4837 , D06M15/564 , D06M15/568 , D06M23/00 , D06M23/10
摘要： This invention relates to coating compositions containing (A) a polyurethane system containing either a polyurethane containing ionic groups and polyethylene oxide units or a precursor thereof prepared from a blocked isocyanate prepolymer and a cross-linking agent and, optionally, (B) organic solvents. This invention further relates to the use of such coating compositions to prepare coatings that are permeable to water vapor.
摘要翻译：本发明涉及包含（A）包含含有离子基团和聚环氧乙烷单元的聚氨酯的聚氨酯体系的涂料组合物或其由嵌段异氰酸酯预聚物和交联剂以及任选的（B）有机溶剂制备的前体。本发明还涉及这种涂料组合物用于制备可渗透水蒸气的涂层的用途。

30. 发明授权

US4613527A PUR-coating compositions which are cross-linkable under heat, a process for their production and their use thereof as an adhesive coat for textiles 失效
标题翻译：在加热下可交联的PUR涂料组合物，其制备方法及其作为纺织品的粘合剂涂层
公开(公告)号：US4613527A
公开(公告)日：1986-09-23
申请号：US678527
申请日：1984-12-05
申请人： Terry Potter , Wilhelm Thoma , Josef Pedain
发明人： Terry Potter , Wilhelm Thoma , Josef Pedain
IPC分类号： C08G18/38 , C09D175/04 , D06N3/14 , B05D1/36
CPC分类号： D06N3/143 , C08G18/3825 , C09D175/04
摘要： The present invention relates to coating compositions based on polyurethane polymers and melamine- and/or urea-formaldehyde resins as cross-linking agents. At least a portion of the chain lengthening agent used to prepare the polyurethane polymers is based on 2,2-bis(hydroxymethyl)propionic acid amide. By using this particular chain lengthening agent, the coating composition can be applied to textile substrates by the direct or reverse coating process and curved at lower temperatures.The present invention additionally relates to the preparation of these coating compositions and to their use as the adhesive coat in preparing coated textile substrates by the direct or reverse coating process.
摘要翻译：本发明涉及基于聚氨酯聚合物和作为交联剂的三聚氰胺和/或脲 - 甲醛树脂的涂料组合物。用于制备聚氨酯聚合物的链增长剂的至少一部分是基于2,2-双（羟甲基）丙酸酰胺。通过使用这种特殊的链延长剂，可以通过直接或反向涂布方法将涂料组合物施加到纺织品基材上，并在较低温度下弯曲。本发明还涉及这些涂料组合物的制备以及它们在通过直接或反向涂布方法制备涂布的纺织品基材中作为粘合剂涂层的用途。

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