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21. 发明申请

US20090163622A1 Copolymers Based On Unsaturated Monocarboxylic or Dicarboxylic Acid Derivatives and Oxyalkylene Glycol Alkenyl Ethers, Process for Preparing Them and Their Use 审中-公开
标题翻译：基于不饱和单羧酸或二羧酸衍生物和氧亚烷基二醇乙烯基醚的共聚物，其制备方法及其应用
公开(公告)号：US20090163622A1
公开(公告)日：2009-06-25
申请号：US12084665
申请日：2006-12-20
申请人： Gerhard Albrecht , Klaus Lorenz , Christian Scholz , Petra Wagner
发明人： Gerhard Albrecht , Klaus Lorenz , Christian Scholz , Petra Wagner
IPC分类号： C08F220/00 , C08F222/04 , C08F216/12 , C08K3/00 , C08K3/30
CPC分类号： C04B24/2605 , C04B24/2647 , C04B24/267 , C04B24/2694 , C04B2103/30 , C04B2103/408 , C08F216/1416 , C08F220/06 , C08F222/06
摘要： Copolymers based on unsaturated mono- or dicarboxylic acid derivatives, oxyalkylene glycol alkenyl ethers and optionally vinylic polyalkylene glycol or ester compounds are described and also their use as additives for aqueous suspensions based on mineral or bituminous binders, in particular cement, gypsum, lime, anhydrite, or other calcium sulphate-based binders, and based on pulverulent dispersion binders. The copolymers according to the invention impart to the aqueous binder suspensions a very good dispersing and liquefying action with, at the same time, simultaneous excellent processing properties. Moreover, the oxyalkylene glycol alkenyl ethers according to the invention are industrially relatively simple and inexpensive to prepare and need comparatively low initiator concentrations in the copolymerization.
摘要翻译：描述了基于不饱和单羧酸或二羧酸衍生物，氧亚烷基二醇烯基醚和任选的乙烯基聚亚烷基二醇或酯化合物的共聚物，也用作基于矿物或沥青粘合剂，特别是水泥，石膏，石灰，无水石膏，或其它基于硫酸钙的粘合剂，并且基于粉末分散粘合剂。根据本发明的共聚物赋予水性粘合剂悬浮液非常好的分散和液化作用，同时具有同时优异的加工性能。此外，根据本发明的氧亚烷基二醇烯基醚在工业上相对简单且制备成本低，并且在共聚中需要相对较低的引发剂浓度。

22. 发明授权

US08536285B2 Semi-continuous method for producing copolymers 有权
标题翻译：半连续共聚物的制备方法
公开(公告)号：US08536285B2
公开(公告)日：2013-09-17
申请号：US13133026
申请日：2009-11-25
申请人： Reinhard Dorfner , Klaus Lorenz , Petra Wagner , Christian Scholz
发明人： Reinhard Dorfner , Klaus Lorenz , Petra Wagner , Christian Scholz
IPC分类号： C08F216/14 , C08F2/10 , C08F224/00 , C04B16/04
CPC分类号： C08F290/00 , C08F265/00 , C08F267/00 , C08F283/06 , C08F290/062 , C08F290/142 , C08L51/003 , C08L2666/02
摘要： A process for the preparation of a copolymer in semicontinuous operation in a polymerization apparatus including a polymerization reactor connected to a metering device, acid monomer being initially taken in the metering device and polyether macromonomer and water in the polymerization reactor, acid monomer being metered from the metering device via an acid monomer metering line into the polymerization reactor, a portion of the copolymer-containing aqueous medium being passed continuously during the free radical polymerization from the polymerization reactor via a reaction mixture line which is connected via a mixing device to the acid monomer metering line, the discharged copolymer-containing aqueous medium being mixed with the acid monomer in the mixing device during the metering of the acid monomer and being recycled to the polymerization reactor after the mixing via the acid monomer metering line.
摘要翻译：一种在包括连接到计量装置的聚合反应器的聚合装置中的半连续操作中制备共聚物的方法，初始计量装置中的酸单体和聚合反应器中的聚醚大分子单体和水，酸单体从计量装置通过酸性单体计量管线进入聚合反应器，一部分含共聚物的水性介质在自由基聚合期间通过经由混合装置连接到酸单体的反应混合物线从聚合反应器中连续通过计量管线，在计量酸性单体期间将含有共聚物的含水介质与酸性单体混合在混合装置中，并通过酸性单体计量管道在混合后再循环到聚合反应器中。

23. 发明授权

US07482405B2 Cement additive 有权
标题翻译：水泥添加剂
公开(公告)号：US07482405B2
公开(公告)日：2009-01-27
申请号：US10551268
申请日：2004-03-05
申请人： Toshimi Matsumoto , Sven Asmus , Gerhard Albrecht , Klaus Lorenz , Petra Wagner , Christian Scholz
发明人： Toshimi Matsumoto , Sven Asmus , Gerhard Albrecht , Klaus Lorenz , Petra Wagner , Christian Scholz
IPC分类号： C08L35/00 , C08L33/02 , C08L33/08
CPC分类号： C04B24/2647 , C04B24/267 , C04B24/2688 , C04B40/0039 , C04B2111/34 , C04B24/06 , C04B24/121 , C04B24/122 , C04B24/18 , C04B24/32 , C04B24/38 , C04B38/10 , C04B2103/10 , C04B2103/20 , C04B2103/304 , C04B2103/44 , C04B2103/50 , C04B2103/61
摘要： The present invention concerns a cement additive containing copolymers comprising one or more constitutional units represented by formula A: (A) R1 is hydrogen, an alkyl group having 1 to 4 carbon atoms, an alkenyl group having 1 to 4 carbon atoms or an aryl group having 6 to 9 carbon atoms; R2 is hydrogen or an alkyl group having 1 to 9 carbon atoms, an alkenyl group having 1 to 9 carbon atoms or an aryl group having 6 to 9 carbon atoms; T is alkylene (including straight-chain and branched alkylene) having 1 to 4 carbon atoms or arylene having 6 to 9 carbon atoms; n is 0 or 1; S1 and S2 are, independently of one another, —OCkH2k— or —OCH2CHR3—, with the proviso that k is 2 or 3, R3 is an alkyl group having 1 to 9 carbon atoms, an aryl group having 6 to 9 carbon atoms; and 6
摘要翻译：本发明涉及包含一种或多种由式A表示的结构单元的共聚物的水泥添加剂：（A）R 1是氢，具有1至4个碳原子的烷基，具有1至4个碳原子的链烯基或芳基具有6至9个碳原子; R2是氢或碳原子数1〜9的烷基，碳原子数1〜9的烯基或碳原子数6〜9的芳基。 T是具有1至4个碳原子的亚烷基（包括直链和支链亚烷基）或具有6至9个碳原子的亚芳基; n为0或1; S 1和S 2彼此独立地为-OC k H 2k-或-OCH 2 CHR 3 - ，条件是k为2或3，R 3为具有1至9个碳原子的烷基，具有6至9个碳原子的芳基; 和6 <_m1 + m2 <_25。

24. 发明申请

US20120035300A1 Semi-Continuous Method For Producing Copolymers 有权
标题翻译：用于生产共聚物的半连续方法
公开(公告)号：US20120035300A1
公开(公告)日：2012-02-09
申请号：US13133026
申请日：2009-11-25
申请人： Reinhard Dorfner , Klaus Lorenz , Petra Wagner , Christian Scholz
发明人： Reinhard Dorfner , Klaus Lorenz , Petra Wagner , Christian Scholz
IPC分类号： C04B16/04 , C08F216/14 , C08F2/10
CPC分类号： C08F290/00 , C08F265/00 , C08F267/00 , C08F283/06 , C08F290/062 , C08F290/142 , C08L51/003 , C08L2666/02
摘要： The present invention relates to a process for the preparation of a copolymer in semicontinuous operation in a polymerization apparatus, comprising a polymerization reactor connected to a metering device, in each case acid monomer being initially taken in the metering device and polyether macromonomer and water in the polymerization reactor, acid monomer being metered from the metering device via an acid monomer metering line into the polymerization reactor, free radical polymerization initiator being passed into the polymerization reactor before and/or during the metering of the acid monomer into the polymerization reactor so that an aqueous medium in which acid monomer and polyether macromonomer are reacted with formation of the copolymer by free radical polymerization forms in the polymerization reactor, a portion of the copolymer-containing aqueous medium being passed continuously during the free radical polymerization from the polymerization reactor via a reaction mixture line which is connected via a mixing device to the acid monomer metering line, the discharged copolymer-containing aqueous medium being mixed with the acid monomer in the mixing device during the metering of the acid monomer and being recycled to the polymerization reactor after the mixing via the acid monomer metering line.
摘要翻译：本发明涉及一种在聚合设备中半连续操作中制备共聚物的方法，包括连接到计量装置的聚合反应器，在各种情况下，酸性单体最初被摄入计量装置中，聚醚大分子单体和水在聚合反应器，酸性单体通过酸单体计量管线从计量装置计量到聚合反应器中，自由基聚合引发剂在酸单体计量之前和/或期间进入聚合反应器中，使得自由基聚合引发剂其中酸性单体和聚醚大分子单体与在聚合反应器中通过自由基聚合形式形成共聚物的水性介质反应，一部分含共聚物的水性介质在自由基聚合过程中通过反应从聚合反应器中连续通过混合线 ch通过混合装置连接到酸性单体计量管线，在计量酸性单体期间，将排出的含共聚物的水性介质与酸性单体混合在混合装置中，并在经过混合之后再循环到聚合反应器中酸性单体计量线。

25. 发明申请

US20110009575A1 Semi Continuous Operational Method For Producing Copolymers 有权
标题翻译：半连续生产共聚物的连续操作方法
公开(公告)号：US20110009575A1
公开(公告)日：2011-01-13
申请号：US12920143
申请日：2009-02-10
申请人： Gerhard Albrecht , Klaus Lorenz , Christian Scholz , Petra Wagner
发明人： Gerhard Albrecht , Klaus Lorenz , Christian Scholz , Petra Wagner
IPC分类号： C08F2/04
CPC分类号： C08F220/04 , C08F220/26
摘要： The invention relates to a process for the preparation of a copolymer in a semicontinuous mode of operation in a polymerization apparatus containing a polymerization reactor connected to a metering device, in each case acid monomer being initially introduced into the metering device and polyether macromonomer and water into the polymerization reactor, acid monomer being metered from the metering device into the polymerization reactor, free radical polymerization initiator being passed into the polymerization reactor before and/or during the metering of the acid monomer into the polymerization reactor, so that an aqueous medium forms in the polymerization reactor, in which aqueous medium acid monomer and polyether macromonomer are reacted by free radical polymerization with formation of the copolymer, at least 70 mol % of the polyether macromonomer initially introduced into the polymerization reactor being converted by the free radical polymerization, the conversion of the acid monomer giving rise in the copolymer to an acid structural until which reduces the pH of the aqueous medium to a lesser extent than the acid monomer as such, the metering of the acid monomer into the polymerization reactor being effected in such a way that first a polymerization pH is established in the aqueous medium and then, until the conversion of 70 mol % of the polyether macromonomer initially introduced into the polymerization reactor, acid monomer is passed into the polymerization reactor in an amount per unit time such that the pH in the aqueous medium deviates by not more than ±0.3 from the initially established polymerization pH.
摘要翻译：本发明涉及在含有连接到计量装置的聚合反应器的聚合装置中制备半连续工作模式的共聚物的方法，每种情况下，酸性单体最初被引入计量装置和聚醚大分子单体和水中聚合反应器，酸性单体从计量装置计量到聚合反应器中，自由基聚合引发剂在酸单体计量之前和/或期间进入聚合反应器中，使得水性介质形成于其中水性介质酸性单体和聚醚大分子单体通过自由基聚合反应形成共聚物的聚合反应器，最初引入聚合反应器的至少70mol％的聚醚大分子单体通过自由基聚合转化，转化率的酸单体在共聚物中产生酸结构，直到将酸性单体的酸度降低到酸性单体的程度以下为止，将酸单体计量到聚合反应器中的方式是首先使聚合pH 在水介质中建立，然后直到最初引入聚合反应器中的70mol％的聚醚大分子单体的转化率为单位时间内将酸性单体以每单位时间的量进入聚合反应器，使得水介质中的pH偏离从最初建立的聚合pH不超过±0.3。

26. 发明授权

US09193822B2 Process for producing polyester polyols having secondary OH end groups 有权
标题翻译：制备具有次级OH端基的聚酯多元醇的方法
公开(公告)号：US09193822B2
公开(公告)日：2015-11-24
申请号：US13318157
申请日：2010-05-04
申请人： Hartmut Nefzger , Erika Bauer , Jörg Hofmann , Klaus Lorenz , Bert Klesczewski
发明人： Hartmut Nefzger , Erika Bauer , Jörg Hofmann , Klaus Lorenz , Bert Klesczewski
IPC分类号： C07C69/675 , C08G63/91 , C08G18/42 , C08G63/87
CPC分类号： C08G63/914 , C08G18/4261 , C08G63/87
摘要： The invention relates to a process for producing polyester polyols with secondary hydroxyl end groups, including the step of the reaction of a polyester including carboxyl end groups with an epoxide of the general formula (1): wherein R1 stands for an alkyl residue or an aryl residue and the reaction is carried out in the presence of a catalyst that includes at least one nitrogen atom per molecule. The process is distinguished in that the polyester including carboxyl end groups exhibits an acid value from ≧25 mg KOH/g to ≦400 mg KOH/g and a hydroxyl value from ≦5 mg KOH/g and in that the polyester including carboxyl end groups is produced by ≧1.03 mol to ≦1.90 mol carboxyl groups or carboxyl-group equivalents of an acid component being employed per mol hydroxyl groups of an alcohol. The polyester polyols obtained, including secondary hydroxyl end groups, can be used for the purpose of producing polyurethane polymers.
摘要翻译：本发明涉及一种生产具有仲羟基端基的聚酯多元醇的方法，包括包括羧基端基的聚酯与通式（1）的环氧化物反应的步骤：其中R1代表烷基或芳基残基，反应在每分子包含至少一个氮原子的催化剂存在下进行。该方法的区别在于包括羧基端基的聚酯显示出≥25mgKOH / g至≥1000的KOH值，400mg KOH / g的酸值和来自＆lt; NEE的5K KOH / g的羟值，并且包括羧基的聚酯端基是由醇的每摩尔羟基使用的≥1.03摩尔至1升; 1.90摩尔羧基或酸组分的羧基当量。得到的聚酯多元醇（包括仲羟基端基）可用于制备聚氨酯聚合物。

27. 发明授权

US09045377B2 Hardening accelerator composition containing phosphated polycondensates 有权
标题翻译：含有磷酸缩聚物的硬化促进剂组合物
公开(公告)号：US09045377B2
公开(公告)日：2015-06-02
申请号：US13392988
申请日：2010-08-12
申请人： Luc Nicoleau , Gerhard Albrecht , Klaus Lorenz , Eva Jetzlsperger , Daniel Fridrich , Thomas Wohlhaupter , Reinhard Dorfner , Hubert Leitner , Mario Vierle , Dirk Schmitt , Michael Braeu , Christoph Hesse , Sabrina Montero Pancera , Siegfried Zuern , Michael Kutschera
发明人： Luc Nicoleau , Gerhard Albrecht , Klaus Lorenz , Eva Jetzlsperger , Daniel Fridrich , Thomas Wohlhaupter , Reinhard Dorfner , Hubert Leitner , Mario Vierle , Dirk Schmitt , Michael Braeu , Christoph Hesse , Sabrina Montero Pancera , Siegfried Zuern , Michael Kutschera
IPC分类号： C04B14/04 , C04B24/32 , C08L5/00 , C08L85/02 , C04B40/00 , C04B103/14
CPC分类号： C04B40/0039 , C04B2103/14 , C04B12/04 , C04B22/085 , C04B24/122 , C04B24/246 , C04B24/383 , C04B2103/22
摘要： The invention concerns a process for the preparation of a hardening accelerator composition by reaction of a water-soluble calcium compound with a water-soluble silicate compound and by reaction of a calcium compound with a silicon dioxide containing component under alkaline conditions, in both cases the reaction being carried out in the presence of a polycondensate containing at least one structural unit consisting of an aromatic or heteroaromatic moiety bearing a polyether side chain and at least one structural unit consisting of an aromatic or heteroaromatic moiety bearing at least one phosphoric acid ester group and/or its salt. The invention concerns a composition of calcium silicate hydrate and the polycondensate, its use as hardening accelerator and for the reduction of the permeability of hardened compositions.
摘要翻译：本发明涉及通过水溶性钙化合物与水溶性硅酸盐化合物的反应以及碱性条件下钙化合物与含二氧化硅的组分的反应来制备硬化促进剂组合物的方法，在这两种情况下反应在含有至少一个结构单元的存在下进行，所述缩聚物包含至少一个由具有聚醚侧链的芳族或杂芳族部分组成的结构单元和至少一个由具有至少一个磷酸酯基团的芳族或杂芳族部分组成的结构单元，和 /或其盐。本发明涉及硅酸钙水合物和缩聚物的组合物，其用作硬化促进剂和降低硬化组合物的渗透性。

28. 发明申请

US20140142344A1 PROCESS FOR PREPARING HIGH MOLECULAR WEIGHT POLYETHER POLYOLS 有权
标题翻译：制备高分子量聚醚多元醇的方法
公开(公告)号：US20140142344A1
公开(公告)日：2014-05-22
申请号：US14125776
申请日：2012-06-26
申请人： Klaus Lorenz , Jörg Hofmann , Horst Zwick , Christian Steinlein , Edward Browne
发明人： Klaus Lorenz , Jörg Hofmann , Horst Zwick , Christian Steinlein , Edward Browne
IPC分类号： C08G65/26
CPC分类号： C08G65/2609 , C08G65/2663 , C08G65/2696
摘要： The invention relates to a process for the preparation of polyether polyols with equivalent molecular weights of from 8,000 to 20,000 g/mol from one or more H-functional starter compounds and one or more alkylene oxides in the presence of a double metal cyanide catalyst, characterized in that the alkylene oxides are metered into the reactor in the course of from 15 to 23 h.
摘要翻译：本发明涉及在双金属氰化物催化剂存在下，从一种或多种H官能起始化合物和一种或多种烯化氧制备具有8,000至20,000g / mol的当量分子量的聚醚多元醇的方法，其特征在于因为在15至23小时的过程中将环氧烷烃计量加入反应器中。

29. 发明申请

US20130204047A1 METHOD FOR PRODUCING POLYTHER POLYOLS 有权
标题翻译：生产多聚多元醇的方法
公开(公告)号：US20130204047A1
公开(公告)日：2013-08-08
申请号：US13582786
申请日：2011-03-09
申请人： Klaus Lorenz
发明人： Klaus Lorenz
IPC分类号： C07C41/02
CPC分类号： C07C41/02 , C08G18/283 , C08G18/4883 , C08G65/2609 , C08G65/2696 , C08G2650/26
摘要： The present invention relates to is coupling process for the preparation of polyether polyols starting from highly functional starter compounds that are solid or highly viscous under reaction conditions and monofunctional starter compounds that are liquid under reaction conditions with Zerewitinoff-active hydrogen atoms.
摘要翻译：本发明涉及用于制备聚醚多元醇的偶合方法，其起始于在反应条件下为固体或高粘度的高官能起始化合物，以及在具有齐来维诺 - 活性氢原子的反应条件下为液体的单官能起始化合物。

30. 发明授权

US08361678B2 Special polyether-based polyurethane formulations for the production of holographic media 有权
标题翻译：用于生产全息介质的特殊聚醚基聚氨酯配方
公开(公告)号：US08361678B2
公开(公告)日：2013-01-29
申请号：US12569344
申请日：2009-09-29
申请人： Marc-Stephan Weiser , Thomas Roelle , Friedrich-Karl Bruder , Thomas Fäcke , Dennis Hönel , Klaus Lorenz , Jörg Hofmann
发明人： Marc-Stephan Weiser , Thomas Roelle , Friedrich-Karl Bruder , Thomas Fäcke , Dennis Hönel , Klaus Lorenz , Jörg Hofmann
IPC分类号： G03H1/02 , G11B7/245 , C08G18/48
CPC分类号： C08G18/7837 , C08G18/4866 , C08G18/672 , C08G18/776 , C08G18/7887 , G03F7/001 , G03F7/027 , G03F7/035 , G11B7/24044 , G11B7/245
摘要： The present invention relates to novel polyurethane compositions which are advantageous for the production of holographic media, inter alia for data storage, but also for optical applications of different types.
摘要翻译：本发明涉及新的聚氨酯组合物，其有利于生产全息介质，特别是用于数据存储，但也适用于不同类型的光学应用。

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