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21. 发明授权

US06916854B2 Unsaturated compounds containing carbamate terminal groups or urea terminal groups 失效
标题翻译：含氨基甲酸酯末端基团或尿素末端基团的不饱和化合物
公开(公告)号：US06916854B2
公开(公告)日：2005-07-12
申请号：US10471598
申请日：2002-03-20
申请人： Reinhold Schwalm , Uwe Meisenburg
发明人： Reinhold Schwalm , Uwe Meisenburg
IPC分类号： C08G18/08 , C08G18/38 , C08G18/67 , C08G18/78 , C09D5/46 , C09D175/16 , C08G18/62
CPC分类号： C08G18/7837 , C08G18/0819 , C08G18/3831 , C08G18/672 , C09D175/16 , C08L2666/14
摘要： The invention relates to a compound containing at least one unsaturated, radically or cationically polymerizable group and at least one carbamate terminal group or urea terminal group.
摘要翻译：本发明涉及含有至少一种不饱和，自由基或阳离子聚合基团和至少一个氨基甲酸酯末端基团或脲基末端基团的化合物。

22. 发明授权

US06777458B1 Method for producing scratch-resistant coatings 失效
标题翻译：防刮涂层的制造方法
公开(公告)号：US06777458B1
公开(公告)日：2004-08-17
申请号：US10049646
申请日：2002-02-25
申请人： Thomas Jaworek , Reinhold Schwalm , Rainer Königer , Reiner Kranwetvogel
发明人： Thomas Jaworek , Reinhold Schwalm , Rainer Königer , Reiner Kranwetvogel
IPC分类号： C08F246
CPC分类号： B05D3/0486 , B05D3/067 , Y10S522/902
摘要： A process for producing scratch-resistant coatings, encompassing the following steps: applying at least one UV-curable coating composition to at least one surface of an article to be coated, said coating composition comprising at least one polymer and/or oligomer P1 containing on average at least one ethylenically unsaturated double bond per molecule, and curing the coating composition by exposure to UV radiation, which comprises conducting the curing of the coating composition under an oxygen-containing protective gas which has an oxygen partial pressure in the range from 0.2 to 18 kPa.
摘要翻译：一种制备耐刮涂层的方法，包括以下步骤：将至少一种UV可固化涂料组合物施用到待涂覆制品的至少一个表面上，所述涂料组合物包含至少一种聚合物和/或低聚物P1，其含有每分子平均至少一个烯属不饱和双键，并通过暴露于紫外线辐射固化涂料组合物，其包括在氧分压为0.2至18的含氧保护气体下进行涂料组合物的固化 kPa。

23. 发明授权

US06777090B2 Substance mixture which can be cured thermally and by using actinic radiation, and the use thereof 有权
标题翻译：能够热固化并通过使用光化辐射的物质混合物及其用途
公开(公告)号：US06777090B2
公开(公告)日：2004-08-17
申请号：US10130934
申请日：2002-06-19
申请人： Hubert Baumgart , Uwe Meisenburg , Heinz-Peter Rink , Paul J. Harris , Reinhold Schwalm
发明人： Hubert Baumgart , Uwe Meisenburg , Heinz-Peter Rink , Paul J. Harris , Reinhold Schwalm
IPC分类号： B32B3126
CPC分类号： C09D201/025 , C08G18/3831 , C08G18/672 , C09J201/025 , Y10T428/31511 , Y10T428/31551 , Y10T428/31938
摘要： Composition curable thermally and with actinic radiation (dual-cure composition) comprising A) at least one constituent containing on average per molecule at least one primary or secondary carbamate group and at least one bond which can be activated with actinic radiation and preparable by from polyfunctional compounds containing at least two isocyanate-reactive, acid-reactive or epoxide-reactive functional groups and suitable monoisocyanates, monoacids or monoepoxides or from polyisocyanates, polyacids or polyepoxides and suitable compounds which contain an isocyanate-reactive, acid-reactive or epoxide-reactive functional group; and B) at least one constituent containing on average per molecule at least one carbamate-reactive functional group and also, where appropriate, at least one bond which can be activated with actinic radiation; and its use as adhesive, sealing compound and coating material.
摘要翻译：包含可热固化和与光化辐射（双重固化组合物）组合的组合物，其包含：A）每分子平均含有至少一个伯或仲氨基甲酸酯基团和至少一个可以用光化辐射活化并可由多官能化合物制备的键的至少一种成分含有至少两种异氰酸酯反应性，酸反应性或环氧化物反应性官能团和合适的单异氰酸酯，单酸或单环氧化物或由多异氰酸酯，多元酸或聚环氧化物和含有异氰酸酯反应性，酸反应性或环氧化物反应性官能团的合适化合物 ; 和B）每分子平均含有至少一个氨基甲酸酯反应性官能团的至少一种组分，并且在适当的情况下还可以使用至少一种可用光化辐射活化的键;以及其用作粘合剂，密封剂和涂料。

24. 发明授权

US06736898B2 Method and means of producing cured coating films 失效
标题翻译：生产固化涂膜的方法和方法
公开(公告)号：US06736898B2
公开(公告)日：2004-05-18
申请号：US09977163
申请日：2001-10-15
申请人： Wolfgang Schrof , Reinhold Schwalm , Erich Beck , Uwe Meisenburg
发明人： Wolfgang Schrof , Reinhold Schwalm , Erich Beck , Uwe Meisenburg
IPC分类号： B05B1700
CPC分类号： B05D3/061
摘要： The present invention relates to a method of producing at least one coating film on at least one area of a substrate surface, which comprises at least the following steps in the following order: a) initiating at least one crosslinking reaction in at least one reactive coating formulation; b) applying said at least one reactive coating formulation before the onset of said at least one crosslinking reaction on said at least one area of said substrate surface. The present invention additionally relates to a corresponding means of producing at least one coating film on at least one area of a substrate surface, having at least the following elements: a) at least one storage container for at least one reactive coating formulation, b) at least one exposure unit, preferably a UV exposure unit, more preferably a UV laser, and c) at least one application unit having a nozzle, in particular a spraying head, and/or d) a bell for electrostatic application (ESTA bell), wherein said at least one exposure unit is designed so that the radiation generated in said at least one exposure unit is brought into contact with said at least one reactive coating formulation in said at least one application unit. Also claimed, finally, is a coating film which can be produced by the method of the invention.
摘要翻译：本发明涉及在基材表面的至少一个区域上生产至少一种涂膜的方法，该方法至少包括以下顺序的至少一个步骤：a）在至少一种反应性涂料中引发至少一种交联反应制剂; b）在所述至少一个交联反应开始之前在所述基材表面的所述至少一个区域上施用所述至少一种反应性涂料制剂。本发明还涉及相应的方法，至少一个基材表面的区域，至少具有以下元素：a）至少一个用于至少一种反应性涂料配方的储存容器，b）至少一个曝光单元，优选UV曝光单元，更优选UV激光，和c）至少一个具有喷嘴，特别是喷头的应用单元和/和用于静电施加的钟（ESTA钟）），其中所述至少一个曝光单元 t被设计成使得在所述至少一个曝光单元中产生的辐射与所述至少一个施加单元中的所述至少一个反应性涂料配方接触。最后还要求一种涂膜，其可以由本发明的方法。

25. 发明授权

US06617413B1 Coating agents which can be hardened by the addition of isocyanate groups as well as by the radiation-induced addition of activated c-c double covalent bonds 有权
标题翻译：可以通过加入异氰酸酯基团以及通过辐射诱导的活化的c-c双共价键的加成来硬化的涂层剂
公开(公告)号：US06617413B1
公开(公告)日：2003-09-09
申请号：US09868712
申请日：2001-08-29
申请人： Bernd Bruchmann , Erich Beck , Hans Renz , Rainer Königer , Reinhold Schwalm , Matthias Lokai , Wolfgang Reich
发明人： Bernd Bruchmann , Erich Beck , Hans Renz , Rainer Königer , Reinhold Schwalm , Matthias Lokai , Wolfgang Reich
IPC分类号： C08G8300
CPC分类号： C09D175/16 , A61K6/09 , B33Y70/00 , C07C265/14 , C07C275/60 , C08G18/672 , C08G18/673 , C08G18/7837 , C08G18/8175 , Y10T428/31551 , C08G18/62 , C08L75/16
摘要： Compounds having isocyanate groups with or without blocking, allophanate groups and free-radically polymerizable C—C double bonds, the C—C double bonds being in activated form by virtue of a carbonyl group attached directly to them or by virtue of an oxygen atom in ether function (activated double bonds), derived from polyisocyanates and alcohols A which in addition to the alcohol group also carry an activated double bond (compounds I). The invention additionally relates to radiation-curable formulations and coating compositions comprising the compounds I, to methods for coating using these substances, and to coated articles produced using these methods. Furthermore, the invention relates to the use of the compounds I in radiation-curable compositions such as in casting compositions, dental compounds, composite materials, sealing compounds, adhesives, troweling compounds, printing inks, in photostructurable compositions such as solder resists, photoresists, photopolymeric printing plates, and stereolithography resins.
摘要翻译：具有或不具有封闭性的异氰酸酯基团，脲基甲酸酯基和可自由基聚合的CC双键的化合物，CC双键由于直接连接到它们上的羰基或借助醚官能团中的氧原子而被活化双键），衍生自多异氰酸酯和除了醇基之外还含有活化双键的醇A（化合物I）。本发明还涉及可辐射固化的制剂和包含化合物I的涂料组合物，使用这些物质的涂覆方法以及使用这些方法制备的涂覆制品。此外，本发明涉及化合物I在可光固化组合物中的用途，所述可辐射固化组合物例如在可光致热组合物如阻焊剂，光致抗蚀剂，光致抗蚀剂等中的浇铸组合物，牙科化合物，复合材料，密封化合物，粘合剂，t刻化合物，印刷油墨，光聚合印刷版和立体光刻树脂。

26. 发明授权

US06344244B1 Method of producing cured coating films 有权
标题翻译：生产固化涂膜的方法
公开(公告)号：US06344244B1
公开(公告)日：2002-02-05
申请号：US09433547
申请日：1999-11-04
申请人： Wolfgang Schrof , Reinhold Schwalm , Erich Beck , Uwe Meisenburg
发明人： Wolfgang Schrof , Reinhold Schwalm , Erich Beck , Uwe Meisenburg
IPC分类号： C08F248
CPC分类号： B05D3/061
摘要： The present invention relates to a method of producing at cast one coating film on at least one area of a substrate surface, which comprises at least the following steps in the following order: a) initiating at least one crosslinking reaction in at least one reactive coating formulation; b) applying said at least one reactive coating formulation before the onset of said at least one crosslinking reaction on said at least one area of said substrate surface. The present invention additionally relates to a corresponding means of producing at least one coating film on at least one area of a substrate surface, having at least the following elements: a) at least one storage container for at least one reactive coating formulation, b) at least one exposure unit, preferably a UV exposure unit, more preferably a UV laser, and c) at least one application unit having a nozzle, in particular a spraying head, and/or d) a bell for electrostatic application (ESTA bell), wherein said at least one exposure unit is designed so that the radiation generated in said at least one exposure unit is brought into contact with said at least one reactive coating formulation in said at least one application unit. Also claimed, finally, is a coating film which can be produced by the method of the invention.
摘要翻译：本发明涉及一种在基材表面的至少一个区域上生产浇铸的一个涂膜的方法，该方法至少包括以下顺序的以下步骤：a）在至少一种反应性涂料中引发至少一种交联反应制剂; b）在所述至少一个交联反应开始之前，在所述基材表面的所述至少一个区域上施用所述至少一种反应性涂料制剂。本发明还涉及在衬底表面的至少一个区域上产生至少一个涂膜的相应方法，其至少具有以下元素：a）至少一个用于至少一种反应性涂料配方的储存容器，b）至少一个曝光单元，优选UV曝光单元，更优选UV激光，以及c）至少一个具有喷嘴，特别是喷头的应用单元和/或用于静电应用的钟（ESTA钟）），其中所述至少一个曝光单元被设计成使得在所述至少一个曝光单元中产生的辐射与所述至少一个应用单元中的所述至少一个反应性涂料配方接触。最后还要求的是可以通过本发明的方法生产的涂膜。

27. 发明授权

US5846689A Positive-working radiation-sensitive mixture and production of relief structures 失效
标题翻译：积极工作的辐射敏感混合物和浮雕结构的生产
公开(公告)号：US5846689A
公开(公告)日：1998-12-08
申请号：US708818
申请日：1996-09-09
申请人： Reinhold Schwalm , Dirk Funhoff , Horst Binder
发明人： Reinhold Schwalm , Dirk Funhoff , Horst Binder
IPC分类号： G03F7/004 , G03F7/039 , H01L21/027
CPC分类号： G03F7/039 , G03F7/0045 , Y10S430/106
摘要： A positive-working radiation-sensitive mixture essentially consists of (a) at least one polymer which contains acid-labile groups and is insoluble in water but becomes soluble in aqueous alkaline solutions as a result of the action of acid, (b) at least one organic compound which produces an acid under the action of actinic radiation and (c) at least one further organic compound differing from (b), where the polymer (a) contains incorporated units of the formulae (I), (II) and (III) ##STR1## and the organic compound (b) is a sulfonium salt of the formula (IV) ##STR2## The radiation-sensitive mixture is suitable for the production of relief structures having improved contrast.
摘要翻译：正面工作的辐射敏感混合物基本上由（a）至少一种含有酸不稳定基团并且不溶于水但由于酸的作用而变得可溶于碱性水溶液的聚合物，（b）至少一种在光化辐射作用下产生酸的有机化合物和（c）至少一种与（b）不同的另外的有机化合物，其中聚合物（a）含有式（I），（II）和（ III）和有机化合物（b）是式（IV）的锍盐。（IV）辐射敏感性混合物适用于生产具有改善的对比度的浮雕结构。

28. 发明授权

US5783354A Positive-working radiation-sensitive mixture 失效
标题翻译：正面工作的辐射敏感混合物
公开(公告)号：US5783354A
公开(公告)日：1998-07-21
申请号：US711016
申请日：1996-09-09
申请人： Reinhold Schwalm , Dirk Funhoff , Horst Binder
发明人： Reinhold Schwalm , Dirk Funhoff , Horst Binder
IPC分类号： G03F7/004 , G03F7/039 , H01L21/027
CPC分类号： G03F7/0045 , G03F7/039 , Y10S430/106 , Y10S430/111
摘要： A positive-working radiation-sensitive mixture essentially consists of (a.sub.1) at least one water-insoluble, organic polymeric binder which contains acid-labile groups and becomes soluble in aqueous alkaline solutions as a result of the action of acid, or (a.sub.2.1) a polymeric binder which is insoluble in water and soluble in aqueous alkaline solutions and (a.sub.2.2) a low molecular weight organic compound whose solubility and aqueous alkaline developer is increased as a result of the action of acid, and (b) at least one organic compound which produces an acid under the action of actinic radiation, and, if required, (c) one or more further organic compounds which differ from (b), at least one of the components (a.sub.1), (a.sub.2.1), (a.sub.2.2), (b) and (c) containing a bonded group of the general formula (I) --O.sup..crclbar. N.sup..sym. R.sub.4, or component (c) being of the formula (II) ##STR1## The radiation-sensitive mixture is suitable for the production of relief structures.
摘要翻译：正面工作的辐射敏感混合物基本上由（a1）至少一种含有酸不稳定基团的水不溶性有机聚合物粘合剂组成，并且由于酸的作用而变得可溶于碱性水溶液，或（a2）。 1）聚合物粘合剂，其不溶于水并且可溶于碱性水溶液，和（a2.2）由于酸的作用，其溶解度和含水碱性显影剂增加的低分子量有机化合物，和（b）在至少一种在光化辐射的作用下产生酸的有机化合物，如果需要，（c）一种或多种与（b），至少一种组分（a1），（a2.1）不同的其它有机化合物）（a）-O（ - ）N（+）R 4，或（c）成分为式（II）的键合基团的化合物（a2.2），（b）和（c）（II）辐射敏感混合物适用于浮雕结构的生产。

29. 发明授权

US5741829A Radiation-curable acrylates with built-in photoinitiators 失效
标题翻译：具有内置光引发剂的可辐射固化的丙烯酸酯
公开(公告)号：US5741829A
公开(公告)日：1998-04-21
申请号：US674832
申请日：1996-07-03
申请人： Wolfgang Reich , Erich Beck , Ulrich Jager , Reinhold Schwalm
发明人： Wolfgang Reich , Erich Beck , Ulrich Jager , Reinhold Schwalm
IPC分类号： C07C68/02 , C07C69/96 , C08F2/48 , C08F2/50 , C08F20/26 , C08F20/28 , C08G00/00 , C08F18/24
CPC分类号： C07C69/96 , Y10S522/905
摘要： Radiation-curable (meth)acrylates obtainable by reacting compounds of the formula ##STR1## in which R is C.sub.1 -C.sub.4 -alkyl, aryl or R.sup.1 and R.sup.1 is ##STR2## in which R.sup.2 to R.sup.6 independently of one another are H, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, OH, phenyl, SH, SCH.sub.3, SC.sub.2 H.sub.5, F, Cl, Br, CN, COOH, COO--(C.sub.1 -C.sub.17 -alkyl), COO--(C.sub.5 -C.sub.10 -aryl), CF.sub.3, N(alkyl).sub.2, N(alkyl)(aryl), N(aryl).sub.2, N.sup..sym. (alkyl).sub.3 A.sup..crclbar., N.sup..sym. H(alkyl).sub.2 A.sup..crclbar., A.sup..crclbar. is the anion of an acid, and alkyl or aryl, unless indicated otherwise, is C.sub.1 -C.sub.10 -alkyl or C.sub.5 -C.sub.10 -aryl, respectively, and at least one but not more than 3 of R.sup.2 to R.sup.6 are ##STR3## with hydroxy(meth)acrylates containing at least 1 free hydroxyl group and at least 2 (meth)acrylic groups in the molecule.
摘要翻译：其中R为C 1 -C 4 - 烷基，芳基或R 1和R 1的式Ⅰ'化合物是其中R 2至R 6彼此独立地为H的可辐射固化（甲基）丙烯酸酯， C 1 -C 4烷基，C 1 -C 4 - 烷氧基，OH，苯基，SH，SCH 3，SC 2 H 5，F，Cl，Br，CN，COOH，COO-（C 1 -C 17 - 烷基）），CF 3，N（烷基）2，N（烷基）（芳基），N（芳基）2，N（+）（烷基）3A（ - ），N（+）H （ - ）是酸的阴离子，除非另有说明，烷基或芳基分别为C 1 -C 10 - 烷基或C 5 -C 10 - 芳基，并且至少一个但不多于3个R 2至R 6为

30. 发明授权

US5563022A Positive-working radiation-sensitive mixture and the production of relief patterns 失效
标题翻译：正面工作的辐射敏感混合物和浮雕图案的制作
公开(公告)号：US5563022A
公开(公告)日：1996-10-08
申请号：US968408
申请日：1992-10-29
申请人： Horst Binder , Reinhold Schwalm , Dirk Funhoff
发明人： Horst Binder , Reinhold Schwalm , Dirk Funhoff
IPC分类号： G03F7/004 , G03F7/039 , H01L21/027 , G03C1/492 , G03F7/30 , G03F7/38
CPC分类号： G03F7/0045 , Y10S430/106 , Y10S430/111 , Y10S430/122
摘要： A positive-working UV-sensitive mixture containing(a1) an organic binder containing acid-labile ether, ester or carbonate groups or(a2) a polymeric binder which is insoluble in water but soluble in aqueous alkaline solutions and(a2.1) an organic compound whose solubility in an aqueous alkaline developer is increased by the action of an acid, or(a2.2) an organic compound whose solubility in an aqueous alkaline developer is increased by the action of an acid and which contains one or more acid-cleavable groups and in addition a group which forms an acid under the action of radiation, or a mixture of the organic compounds (a2.1) and (a2.2) and(b) an arylsulfonic ester, is suitable for the production of relief patterns.
摘要翻译：含有（a1）含酸不稳定醚，酯或碳酸酯基团的有机粘合剂或（a2）不溶于水但可溶于碱性水溶液的聚合物粘合剂的正性UV敏感性混合物，（a2.1）在水性碱性显影剂中的溶解度由酸的作用而增加的有机化合物，或（a2.2）其在碱性显影液中的溶解度在酸的作用下增加并且含有一种或多种酸 - 可裂解基团，另外还有在辐射作用下形成酸的基团，或有机化合物（a2.1）和（a2.2）和（b）芳基磺酸酯的混合物，适于生产浮雕模式。

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