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21. 发明授权

US06329483B1 Copolymers of carboxylic acids and quaternary ammonium compounds and the use thereof as thickeners of dispersants 失效
标题翻译：羧酸和季铵化合物的共聚物及其作为分散剂增稠剂的用途
公开(公告)号：US06329483B1
公开(公告)日：2001-12-11
申请号：US08313175
申请日：1994-09-29
申请人： Christian Schade , Axel Sanner , Hans-Ulrich Wekel , Franz Frosch , Horst Westenfelder
发明人： Christian Schade , Axel Sanner , Hans-Ulrich Wekel , Franz Frosch , Horst Westenfelder
IPC分类号： C08F22204
CPC分类号： A61Q19/00 , A61K8/817 , A61K2800/48 , C08F220/04 , C08F222/00
摘要： A copolymer obtainable by free-radical polymerization of A) 50-99.99% by weight of an olefinically unsaturated C3-C5 monocarboxylic acid, of an olefinically unsaturated C4-C8 dicarboxylic acid or the anhydride thereof or a mixture of such carboxylic acids or anhydrides with B) 0.01-50% by weight of an olefinically unsaturated quaternary ammonium compound of the formula I or II where R1 is C6-C20-alkyl, C6-C20-alkenyl, C5-C8-cycloalkyl, phenyl, phenyl(C1-C12-alkyl) or (C1-C12-alkyl)phenyl, R2 is hydrogen, methyl or phenyl, R3 and R4 are each H or C1-C4-alkyl, X is halogen, C1-C4-alkoxysulfonyloxy or C1-C4-alkanesulfonate, it also being possible for the latter to occur as R3 or R4 with the formation of a betaine structure, Y is O or NH, and A is C1-C6-alkylene, or a mixture of such ammonium compounds, C) 0 to 49.99% by weight of an acrylate or methacrylate of the formula III where R1, R2 and Y have the abovementioned meanings, R5 is hydrogen, methyl or ethyl, and n is a number from 0 to 25, D) 0-49.99% by weight of other copolymerizable monomers and E) 0-5% by weight of one or more compounds with at least two olefinically unsaturated groups in the molecule as crosslinker. The copolymers are suitable as thickeners and dispersants, especially in cosmetic compositions.
摘要翻译：可通过自由基聚合得到的共聚物，A）50-99.99重量％的烯属不饱和C 3 -C 5单羧酸，烯属不饱和C 4 -C 8二羧酸或其酸酐或这些羧酸或酸酐与B）的混合物， 0.01-50重量％的式I或II的烯属不饱和季铵化合物，其中R 1是C 6 -C 20 - 烷基，C 6 -C 20 - 烯基，C 5 -C 8 - 环烷基，苯基，苯基（C 1 -C 12 - 烷基）或（C 1 -C 12 - 烷基）苯基，R 2是氢，甲基或苯基，R 3和R 4各自为H或C 1 -C 4烷基，X为卤素，C 1 -C 4烷氧基磺酰氧基或C 1 -C 4烷基磺酸盐，也是可能的后者以R3或R4形成甜菜碱结构，Y为O或NH，A为C 1 -C 6亚烷基，或这些铵化合物的混合物，C）0至49.99重量％的丙烯酸酯或甲基丙烯酸酯，其中R 1，R 2和Y具有上述含义，R 5是氢，甲基或乙基，n是0至25的数，D）0-4 9.99重量％的其它可共聚单体和E）0-5重量％的一种或多种在分子中具有至少两个烯属不饱和基团的化合物作为交联剂。该共聚物适合用作增稠剂和分散剂，特别是在化妆品组合物中。

22. 发明授权

US5869032A Quaternized copolymers suitable as active ingredients in cosmetic formulations, such as hair styling compositions 失效
标题翻译：适合作为化妆品制剂中的活性成分的季铵化共聚物，例如头发定型组合物
公开(公告)号：US5869032A
公开(公告)日：1999-02-09
申请号：US824920
申请日：1997-03-27
申请人： Jurgen Tropsch , Axel Sanner , Peter Hossel , Hans-Jurgen Raubenheimer , Christian Schade
发明人： Jurgen Tropsch , Axel Sanner , Peter Hossel , Hans-Jurgen Raubenheimer , Christian Schade
IPC分类号： A61K8/72 , A61K8/00 , A61K8/81 , A61Q5/00 , A61Q5/06 , A61Q19/00 , C08F8/44 , C08F26/00 , C08F26/10 , C08F226/06 , C08F226/10 , A61K7/06 , A61K7/48
CPC分类号： A61Q19/00 , A61K8/817 , A61K8/8182 , A61Q5/06
摘要： Quaternized copolymers suitable as active ingredients in hair styling compositions are obtainable from N-vinylimidazoles, N-vinylcaprolactam, N-vinylpyrrolidone and, if required, further monomers.
摘要翻译：适合作为头发定型组合物中的活性成分的季铵化共聚物可从N-乙烯基咪唑，N-乙烯基己内酰胺，N-乙烯基吡咯烷酮和（如果需要的话）其它单体得到。

23. 发明授权

US5804662A Agglomerated, finely divided, crosslinked vinylimidazole copolymers, preparation thereof, and use thereof 失效
标题翻译：聚集的，细碎的，交联的乙烯基咪唑共聚物，其制备及其用途
公开(公告)号：US5804662A
公开(公告)日：1998-09-08
申请号：US894364
申请日：1997-08-19
申请人： Christian Schade , Karl-Heinrich Schneider
发明人： Christian Schade , Karl-Heinrich Schneider
IPC分类号： B01F17/00 , B01F17/52 , C08F2/24 , C08F2/32 , C08F26/06 , C08F226/06 , C11D3/00 , C11D3/37
CPC分类号： C11D3/0021 , B01F17/0042 , C08F26/06 , C11D3/3776
摘要： Agglomerated, finely divided, crosslinked vinylimidazole copolymers obtainable by free-radically initiated polymerization of N-vinylimidazoles of the formula ##STR1## where R, R.sup.1 and R.sup.2 are identical or different and each is H, C.sub.1 -C.sub.4 -alkyl or phenyl, with at least one crosslinker, optionally other water-soluble monoethylenically unsaturated monomers, and optionally water-insoluble monoethylenically unsaturated monomers in the aqueous phase of a water-in-oil emulsion in the presence of at least one emulsifier comprising block copolymers of the type AB or ABA or comb copolymers constructed from A and B, where A is a hydrophobic polymer block having a molecular weight of >500 g/mol and B is a hydrophilic polymer block having a molecular weight of >500 g/mol, to stabilize the water-in-oil monomer emulsion, azeotropic distillative removal of the water from the water-in-oil polymer suspension, and isolation of the polymers, processes for preparing said agglomerated, finely divided, crosslinked vinylimidazole copolymers, and use of the copolymers in detergents to inhibit the transfer of dye during the wash.
摘要翻译： PCT No.PCT / EP96 / 00575 Sec。 371日期1997年8月19日 102（e）日期1997年8月19日PCT提交1996年2月10日PCT公布。公开号WO96 / 26229 日期1996年8月29日通过自由基引发的式（I）的N-乙烯基咪唑聚合得到的聚集的细分交联乙烯基咪唑共聚物，其中R，R 1和R 2相同或不同，各自为H，C1- 在至少一种乳化剂的存在下，在至少一种乳化剂存在下，与至少一种交联剂，任选的其它水溶性单烯属不饱和单体和任选的水不溶性单烯属不饱和单体在油包水乳液的水相中，由A和B构成的AB型或ABA型或梳状共聚物的嵌段共聚物，其中A为分子量> 500g / mol的疏水性聚合物嵌段，B为分子量> 500g / mol，以稳定油包水单体乳液，共沸蒸馏从油包水聚合物悬浮液中除去水，并分离聚合物，制备所述附聚的精细的方法分离的交联乙烯基咪唑共聚物，以及洗涤剂中共聚物在洗涤过程中抑制染料转移的用途。

24. 发明授权

US5627151A Use of vinylpyrrolidone copolymers as detergent additives, novel polymers of vinylpyrrolidone, and preparation thereof 失效
标题翻译：使用乙烯基吡咯烷酮共聚物作为洗涤剂添加剂，乙烯基吡咯烷酮的新型聚合物及其制备
公开(公告)号：US5627151A
公开(公告)日：1997-05-06
申请号：US325177
申请日：1995-04-21
申请人： Juergen Detering , Christian Schade , Wolfgang Trieselt , Juergen Tropsch
发明人： Juergen Detering , Christian Schade , Wolfgang Trieselt , Juergen Tropsch
IPC分类号： C08F2/10 , C08F26/00 , C08F26/10 , C08F226/06 , C08F226/10 , C08F289/00 , C11D3/00 , C11D3/37 , C11D3/28
CPC分类号： C11D3/3776 , C08F289/00 , C11D3/0021 , C11D3/3788
摘要： There are described the use of copolymers obtainable by free-radically initiated copolymerization of monomer mixtures comprising(a) 60-99% by weight of 1-vinylpyrrolidone, 1-vinylimidazole or mixtures thereof,(b) 1-40% by weight of nitrogen-containing, basic ethylenically unsaturated monomers in the form of the free bases, in the form of salts or in quaternized form, and optionally(c) up to 20% by weight of other monoethylenically unsaturated monomers,as detergent additives for inhibiting dye transfer during the wash, detergents which contain such polymers, and polymers which are obtainable by free-radically initiated polymerization of(a) 1-vinylpyrrolidone, 1-vinylimidazole, 1-vinylimidazolium compounds, or mixtures thereof, and optionally(b) other nitrogen-containing, basic ethylenically unsaturated monomers in the form of the free bases, in the form of the salts or in quaternized form, and/or(c) other monoethylenically unsaturated monomers,in an aqueous medium in the presence of water-soluble proteins and a process for the preparation of the polymers by polymerising the monomers (a) and optionally (b) and/or (c) in an aqueous medium in the presence of water-soluble proteins using from 0.5 to 400 parts by weight of protein per 100 parts by weight of monomer used in the polymerization.
摘要翻译： PCT No.PCT / EP93 / 02851 Sec。 371日期1995年04月21日 102（e）日期1995年4月21日PCT 1993年10月15日PCT公布。公开号WO94 / 10281 日本1994年5月11日描述了通过自由基引发的单体混合物共聚获得的共聚物的用途，所述共聚物包含（a）60-99重量％的1-乙烯基吡咯烷酮，1-乙烯基咪唑或其混合物，（b）1-40重量％重量的游离碱形式的含氮碱性烯键式不饱和单体，以盐形式或季铵化形式，和任选地（c）最多20％重量的其它单烯属不饱和单体作为洗涤剂添加剂，用作（a）1-乙烯基吡咯烷酮，1-乙烯基咪唑，1-乙烯基咪唑鎓化合物或其混合物，和任选地（b）可通过自由基引发的聚合获得的聚合物，在盐水介质中以盐形式或季铵化形式的其它含氮的碱性烯属不饱和单体，和/或（c）其它单烯属不饱和单体在水溶性蛋白质存在下，通过在水溶性蛋白质的存在下在水溶性介质中聚合单体（a）和任选地（b）和/或（c））来制备聚合物的方法，使用相对于聚合中使用的单体100重量份，为0.5〜400重量份的蛋白质。

25. 发明授权

US08545953B2 Hollow polystyrene body obtained by injection stretch blow moulding 失效
标题翻译：空心聚苯乙烯体通过注射拉伸吹塑得到
公开(公告)号：US08545953B2
公开(公告)日：2013-10-01
申请号：US12527975
申请日：2007-12-17
申请人： Stefan Burgdörfer , Walter Heckmann , Hans-Jürgen Renner , Christian Schade , Hans-Dieter Schwaben
发明人： Stefan Burgdörfer , Walter Heckmann , Hans-Jürgen Renner , Christian Schade , Hans-Dieter Schwaben
IPC分类号： B32B1/02 , B32B1/08 , B65B25/06 , B29C49/08
CPC分类号： G11B7/2533 , C08L25/16 , C08L51/003 , C08L51/06 , C08L2205/02 , C08L2205/03 , C08L2666/24
摘要： A blow molding having capacity of at least 250 ml, having a shell which is composed of impact-resistant polystyrene and which is produced via injection stretch blow molding where an average aspect ratio of rubber particles derived from longitudinal section and an average aspect ratio of rubber particles derived from cross section measured in transmission electron micrographs is greater than 4 respectively, and a biaxial orientation of the rubber particles, given by the ratio of the aspect ratio derived from cross section to the aspect ratio derived from longitudinal section is smaller than 3.
摘要翻译：具有至少250ml容量的吹塑成型体，其具有由耐冲击聚苯乙烯构成的外壳，其通过注射拉伸吹塑法制备，其中由纵向截面的橡胶颗粒的平均纵横比和橡胶的平均纵横比衍生自透射电子显微镜照片的横截面的颗粒分别大于4，由横截面导出的纵横比与由纵截面导出的纵横比的比率给出的橡胶颗粒的双轴取向小于3。

26. 发明授权

US08206626B2 Method for producing nanoporous molded parts 有权
标题翻译：生产纳米多孔成型件的方法
公开(公告)号：US08206626B2
公开(公告)日：2012-06-26
申请号：US12307179
申请日：2007-06-27
申请人： Andre Guerin Moreira , Marc Bothe , Volker Schädler , Markus Allmendinger , Pedro Manuel Sampaio Lopes , Bernd Sowart , Timothy Francis , Erik Waβner , Christian Schade , Daniela Longo , Siljana Lietz , Volker Alstädt , Jan Sandler
发明人： Andre Guerin Moreira , Marc Bothe , Volker Schädler , Markus Allmendinger , Pedro Manuel Sampaio Lopes , Bernd Sowart , Timothy Francis , Erik Waβner , Christian Schade , Daniela Longo , Siljana Lietz , Volker Alstädt , Jan Sandler
IPC分类号： C08J9/00 , B29C44/34
CPC分类号： C08J9/0061 , B29C44/04 , B29C44/0484 , C08J9/14 , C08J2203/06 , C08J2203/12 , C08J2203/14 , C08J2203/142 , C08J2325/06 , C08J2425/00 , C08J2451/00 , C08J2453/00
摘要： Process for the production of moldings from nanoporous polymer materials, comprising the stages of a) preparation of a multiphase polymer mixture with domains in the range from 5 to 200 nm, b) impregnation of the polymer mixture with a blowing agent, where the solubility of the blowing agent in the phase forming the domains is at least twice as high as in the adjacent phases, c) expansion of the multiphase polymer mixture comprising blowing agent, by introducing the polymer mixture into a cavity and expanding it therein, thus obtaining the molding.
摘要翻译：包括以下步骤：a）制备具有5至200nm范围内的结构域的多相聚合物混合物的步骤，b）用发泡剂浸渍聚合物混合物，其中溶解度形成区域的相中的发泡剂是相邻相中的至少两倍，c）通过将聚合物混合物引入空腔并在其中膨胀从而使包含发泡剂的多相聚合物混合物膨胀，从而获得模塑。

27. 发明申请

US20100025877A1 METHOD FOR PRODUCING NANOPOROUS MOLDED PARTS 有权
标题翻译：生产纳米成型件的方法
公开(公告)号：US20100025877A1
公开(公告)日：2010-02-04
申请号：US12307179
申请日：2007-06-27
申请人： Andre Guerin Moreira , Marc Bothe , Volker Schädler , Markus Allmendinger , Pedro Manuel Sampaio Lopes , Bernd Sowart , Timothy Francis , Erik Wassner , Christian Schade , Daniela Longo , Siljana Lietz , Volker Alstädt , Jan Sandler
发明人： Andre Guerin Moreira , Marc Bothe , Volker Schädler , Markus Allmendinger , Pedro Manuel Sampaio Lopes , Bernd Sowart , Timothy Francis , Erik Wassner , Christian Schade , Daniela Longo , Siljana Lietz , Volker Alstädt , Jan Sandler
IPC分类号： C08J9/06
CPC分类号： C08J9/0061 , B29C44/04 , B29C44/0484 , C08J9/14 , C08J2203/06 , C08J2203/12 , C08J2203/14 , C08J2203/142 , C08J2325/06 , C08J2425/00 , C08J2451/00 , C08J2453/00
摘要： Process for the production of moldings from nanoporous polymer materials, comprising the stages of a) preparation of a multiphase polymer mixture with domains in the range from 5 to 200 nm, b) impregnation of the polymer mixture with a blowing agent, where the solubility of the blowing agent in the phase forming the domains is at least twice as high as in the adjacent phases, c) expansion of the multiphase polymer mixture comprising blowing agent, by introducing the polymer mixture into a cavity and expanding it therein, thus obtaining the molding.
摘要翻译：包括以下步骤：a）制备具有5至200nm范围内的结构域的多相聚合物混合物的步骤，b）用发泡剂浸渍聚合物混合物，其中溶解度形成区域的相中的发泡剂是相邻相中的至少两倍，c）通过将聚合物混合物引入空腔并在其中膨胀从而使包含发泡剂的多相聚合物混合物膨胀，从而获得模塑。

28. 发明授权

US06165969A Use of quaternized polymerizates containing units of vinyl imidazol as a color fixing and color transfer inhibiting additive to detergent post-treatment agents and detergents 有权
标题翻译：使用含有乙烯基咪唑单元的季铵化聚合物作为固色剂和颜色转移抑制添加剂到洗涤剂后处理剂和洗涤剂
公开(公告)号：US06165969A
公开(公告)日：2000-12-26
申请号：US284967
申请日：1999-05-05
申请人： Dieter Bockh , Hans-Ulrich Jager , Jurgen Alfred Lux , Stefan Stein , Jurgen Detering , Christian Schade
发明人： Dieter Bockh , Hans-Ulrich Jager , Jurgen Alfred Lux , Stefan Stein , Jurgen Detering , Christian Schade
IPC分类号： C08F226/06 , C11D3/00 , C11D3/37 , D06P1/52 , D06P5/08 , C11D10/00
CPC分类号： C08F226/06 , C11D3/0021 , C11D3/3776 , D06P1/5242 , D06P5/08
摘要： The use of polymers which comprise at least 5 mol % of quaternized 1-vinylimidazole units of the formula ##STR1## where R is C.sub.1 -C.sub.25 -alkyl, C.sub.5 -C.sub.10 -cycloalkyl or benzylR.sup.1,R.sup.2,R.sup.3 are identical or different and are H, CH.sub.3 and C.sub.2 H.sub.5, andX.sup..crclbar. is an anion,as color-fixing and color transfer-inhibiting additive to laundry aftertreatment aids and to detergents.
摘要翻译： PCT No.PCT / EP97 / 05939 Sec。 371日期1999年5月5日 102（e）日期1999年5月5日PCT 1997年10月28日PCT公布。 WO98 / 21301 PCT出版物日期1998年5月22日使用包含至少5mol％下式的季铵化1-乙烯基咪唑单元的聚合物其中R是C 1 -C 25 - 烷基，C 5 -C 10 - 环烷基或苄基R 1，R 2，R 3相同或不同，是H，CH 3和C 2 H 5，并且X（ - ）是阴离子，作为用于洗衣后处理助剂和洗涤剂的着色和转色抑制添加剂。

29. 发明授权

US5849853A Preparation of water-insoluble polymers 失效
标题翻译：水不溶性聚合物的制备
公开(公告)号：US5849853A
公开(公告)日：1998-12-15
申请号：US773310
申请日：1996-12-24
申请人： Christian Schade
发明人： Christian Schade
IPC分类号： C08L57/00 , C08F2/16 , C08F2/20 , C08F2/22 , C08F2/24 , C08F2/44
CPC分类号： C08F2/16
摘要： Water-insoluble polymers are prepared by free radical polymerization of ethylenically unsaturated monomers by a process in which the polymerization is carried out in an aqueous gel phase having a viscosity of at least 800 mPa.s and the gel former has a molecular weight of more than 20,000. The dispersions obtained have a long shelf life and the polymer can be readily precipitated.
摘要翻译：水不溶性聚合物通过烯键式不饱和单体的自由基聚合制备，其中聚合在粘度至少为800mPa.s的水凝胶相中进行，凝胶形成剂的分子量大于 20,000。获得的分散体具有长的保存期限，并且聚合物可以容易地沉淀。

30. 发明申请

US20140329100A1 THERMOPLASTIC MOULDING COMPOSITIONS FOR METAL PLATED ARTICLES WITH IMPROVED RESISTANCE AGAINST REPEATED IMPACT 有权
标题翻译：用于金属制品的热塑性成型组合物具有改善的抗重复性影响的电阻
公开(公告)号：US20140329100A1
公开(公告)日：2014-11-06
申请号：US13992602
申请日：2011-12-15
申请人： Michel Pepers , Christian Schade , Davy Roger Suwier , Norbert Niessner
发明人： Michel Pepers , Christian Schade , Davy Roger Suwier , Norbert Niessner
IPC分类号： C08L25/12 , C23C18/31 , C23C18/16
CPC分类号： C08L25/12 , C08L9/00 , C08L21/00 , C08L25/10 , C08L51/00 , C08L55/02 , C08L2205/02 , C08L2205/03 , C08L2207/04 , C23C18/1601 , C23C18/1641 , C23C18/31 , C25D5/14 , C25D5/56 , Y10T428/31696
摘要： Thermoplastic moulding composition (F), comprising: A) from 5 to 80% by weight of a graft polymer (A) having bimodal particle size distribution and a moisture content of 0 to 27% by weight, made, based on (A), a1) from 40 to 90% by weight of an elastomeric particulate graft base (a1), obtained by emulsion polymerization of based on (a1), a11) from 70 to 100% by weight of at least one conjugated diene, or of at least one C1-8-alkyl acrylate, or of mixtures of these, a12) from 0 to 30% by weight of at least one other monoethylenically unsaturated monomer and a13) from 0 to 10% by weight of at least one polyfunctional, cross linking monomer; a2) from 10 to 60% by weight of a graft a2), made, based on a2), a21) from 64 to 76% by weight of at least one vinyl aromatic monomer, a22) from 24 to 36% by weight of acrylonitrile, a23) from 0 to 30% by weight of at least one other monoethylenically unsaturated monomer, and a24) from 0 to 10% by weight of at least one polyfunctional, cross linking monomer; B) from 10 to 94% by weight of a thermoplastic polymer (B) having a viscosity number VN of from 50 to 120 ml/g, made, based on (B), b1) from 64 to 72% by weight of at least one vinyl aromatic monomer, b2) from 28 to 36% by weight of acrylonitrile, and b3) from 0 to 4% by weight of at least one other monoethylenically unsaturated monomer; whereby, the difference of the acrylonitrile content in component (B) and that in the graft shell a2) is minimal 2% by weight and maximal 6% by weight and optionally further components, have preferred optical appearance when coated with metal.
摘要翻译：热塑性成型组合物（F），其包含：A）5-80重量％的具有双峰粒径分布的接枝聚合物（A）和0-27重量％的水分含量，基于（A）， a1）40〜90重量％的通过基于（a1），a11）的乳液聚合获得的弹性体颗粒接枝基质（a1），70〜100重量％的至少一种共轭二烯，或至少一种C 1-8 - 烷基丙烯酸酯，或它们的混合物，a12）0至30重量％的至少一种其它单烯属不饱和单体和（ⅰ）0至10重量％的至少一种多官能交联单体 ; a2）10至60重量％的基于a2）制备的接枝物a2），a21）64至76重量％的至少一种乙烯基芳族单体，a22）24至36重量％的丙烯腈，a23）0至30重量％的至少一种其它单烯属不饱和单体，以及a24）0至10重量％的至少一种多官能交联单体; B）10至94重量％的基于（B），b1）的粘度VN为50至120ml / g的热塑性聚合物（B），至少64至72重量％一种乙烯基芳族单体，b2）28-36重量％的丙烯腈，和b3）0-4重量％的至少一种其它单烯属不饱和单体; 由此，组分（B）中的丙烯腈含量与接枝壳a2）中的丙烯腈含量的差异最小为2重量％，最多6重量％，任选的其它组分在涂覆金属时具有优选的光学外观。

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