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    • 23. 发明专利
    • PARTICLE MEASURING DEVICE AND PARTICLE MEASURING METHOD
    • JP2000283911A
    • 2000-10-13
    • JP9288899
    • 1999-03-31
    • TOSHIBA CORP
    • MATSUI ISAO
    • G01N27/60G01N15/02
    • PROBLEM TO BE SOLVED: To provide a particle measuring device capable of measuring a particle size number distribution easily and highly precisely under a low pressure. SOLUTION: This particle measuring device 1 is equipped with a plasma generator 11, a charged-particle counter 12, a power source 13 for generating a positive high voltage, a filter 14, a pump 15, and a particle size number distribution operation part 16 for operating a particle size. The plasma generator 11 has a positive electrode 17 and a negative electrode 18, arranged oppositely, and the charged-particle counter 12 installed on the positive electrode 17. By paying attention the fact that a particle to be measured draws a flying locus corresponding to a voltage between the electrodes 17, 18 under plasma discharge, the charged-particle counter 12 is placed on a proper position, and the voltage applied between the electrodes 17, 18 is changed, and the particle to be measured having a specific particle size is collected by the charged-particle counter 12 in each voltage. By this, a particle size number distribution of the particles to be measured can be detected easily and precisely under a low pressure.
    • 26. 发明专利
    • VAPOR GROWTH DEVICE
    • JPS6482520A
    • 1989-03-28
    • JP23884287
    • 1987-09-25
    • TOSHIBA CORP
    • MATSUI ISAO
    • H01L21/205
    • PURPOSE:To inhibit the precipitation of a solid group V substance onto a reaction pipe wall while reducing the quantity of an unreacted group V raw gas by installing fillers to a flow section lower than a crystal substrate in the direction of flow of a reaction gas and uniformly heating the fillers. CONSTITUTION:A granular filler layer 5 is heated at the point of sublimation or more of a group V substance contained in a reaction gas by a filler heating unit 7, and the reaction gas is heated at the temperature of the granular filler layer 5 when it passes through the layer 5. An undecomposed group V raw gas in the reaction gas is decomposed to a group V element by a decomposition reaction. A group V substance under a solid state in the reaction gas generated at that time generates a sublimation reaction. Since the sublimation reaction is an equilibrium reaction, sublimation pressure is determined by a temperature. All of the reaction gas heated at the point of sublimation or more are brought to a gaseous state, and discharged outside a reaction pipe from a reaction-gas discharge port 3. Accordingly, the group V substance included in the reaction gas is not precipitated into the reaction pipe under the solid state, and no undecomposed group V raw gas is contained in discharged gas from the reaction pipe.
    • 27. 发明专利
    • VAPOR GROWTH EQUIPMENT
    • JPS63278222A
    • 1988-11-15
    • JP8407987
    • 1987-04-06
    • TOSHIBA CORP
    • MATSUI ISAO
    • H01L21/205
    • PURPOSE:To obtain a crystal with a uniform film thickness and a uniform film composition by a method wherein a reflecting means which reflects a thermol radiation emitted from the surface of a sample so as to apply the reflected radiation to the sample surface is provided in a vapor growth equipment. CONSTITUTION:Eddy currents are induced in a susceptor 2 by a radio frequency current applied to a radio frequency coil 3. The susceptor 2 is heated by the induced eddy current. Substrates 6 attached to the susceptor 2 are heated by heat conduction. Heat rays are emitted from the surfaces of the substrates 6. The thermol radiation are reflected by mirrors 5 attached to the coil 3 and partially returned to the substrates 6. The end parts of the substrates 6 which have lower temperatures than the center parts are heated again by the reflected thermol radiation and the temperature of the substrate 6 becomes uniform. Reactive gas supplied from a supply inlet 1 is decomposed and made to react to make crystal growth. As the temperature of the substrate 1 is uniform, the uniformity of the film thickness and composition of the crystal made to grow can be obtained.
    • 29. 发明专利
    • METHOD AND APPARATUS FOR PRODUCING PARTICLE
    • JP2001261335A
    • 2001-09-26
    • JP2000077210
    • 2000-03-17
    • TOSHIBA CORP
    • MATSUI ISAO
    • C01G9/08B22F1/02B22F9/28
    • PROBLEM TO BE SOLVED: To provide a method and an apparatus for producing particles for restraining the particles formed in a reaction vessel from getting larger due to aggregation proceeding simultaneously with their growth. SOLUTION: This apparatus for producing particles is constituted of a reaction vessel 1, a raw gas charging unit 2 for charging a raw gas into the reaction vessel 1, a surface-adhering matter charging unit 3 for charging surface-adhering matter into the reaction vessel 1, an inert gas charging unit 4 for charging a carrier gas into the reaction vessel 1, a heater 5 equipped on the reaction vessel 1, a discharge unit 6, a cooler 7 into which microparticles formed in the reaction vessel 1 and then discharged via the unit 6 from the reaction vessel 1 and an inert gas are to be charged, a storage unit 8 for storing the particles passed through the cooler 7, a heater 9 for removing liquid component and surface-adhering matter from a solvent containing the particles stored in the storage section 8, and a filter 10 for extracting only the particles each of a desired size from particles of varying sizes.