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21. 发明申请

WO2014164614A1 METHOD FOR THE PREPARATION OF POLYMERIZATION CATALYSTS 审中-公开
标题翻译：聚合催化剂的制备方法
公开(公告)号：WO2014164614A1
公开(公告)日：2014-10-09
申请号：PCT/US2014/023009
申请日：2014-03-11
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P , COLLINS, Kathy S , SCHWERDTFEGER, Eric D , SOLENBERGER, Alan L
发明人： MCDANIEL, Max P , COLLINS, Kathy S , SCHWERDTFEGER, Eric D , SOLENBERGER, Alan L
IPC分类号： C08F10/00
CPC分类号： C08F4/22 , C08F10/00 , C08F4/24 , C08F4/025 , C08F110/02 , C08F2500/12
摘要： A method comprising contacting a support material with a transition metal compound to produce a mixture; thermally treating the mixture in the presence of oxygen at a temperature in a range of from about 100° C to about 500° C for a period of from about 1 hour to about 10 hours, wherein at least a portion of the transition metal sublimes onto the support material to produce a support material comprising a dispersed transition metal; and thermally treating the support material comprising the dispersed transition metal in an oxidizing atmosphere at a temperature in a range of from about 550° C to about 900° C for a period of from about 1 hour to about 10 hours to produce a polymerization catalyst.
摘要翻译：一种方法，包括使支撑材料与过渡金属化合物接触以产生混合物; 在氧气存在下，在约100℃至约500℃的温度范围内热处理混合物约1小时至约10小时，其中至少一部分过渡金属升华到用于生产包含分散的过渡金属的载体材料的载体材料; 并在包含分散的过渡金属的载体材料的氧化气氛中在约550℃至约900℃的温度范围内热处理约1小时至约10小时，以制备聚合催化剂。

22. 发明申请

WO2014164514A2 METHODS OF PREPARING A POLYMERIZATION CATALYST 审中-公开
标题翻译：制备聚合催化剂的方法
公开(公告)号：WO2014164514A2
公开(公告)日：2014-10-09
申请号：PCT/US2014/022663
申请日：2014-03-10
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P , COLLINS, Kathy S
发明人： MCDANIEL, Max P , COLLINS, Kathy S
IPC分类号： C08F10/00
CPC分类号： C08F10/00 , C08F4/69 , C08F4/025 , C08F110/02 , C08F2500/03 , C08F2500/12
摘要： A method comprising contacting a silica support material with a sulfating agent to form a sulfated silica support material comprising sulfate anions; thermally treating the sulfated silica support material to form a thermally treated sulfated silica support material; contacting the thermally treated sulfated silica support material with a chromium- containing compound to form a mixture; and thermally treating the mixture to form a polymerization catalyst. A method comprising thermally treating a silica support material to form a thermally-treated silica support material; contacting the thermally-treated silica support material with a sulfating agent to form a thermally treated sulfated silica support material; thermally treating the thermally treated sulfated silica support material to form a processed silica support material; contacting the processed silica support material with a chromium-containing compound to form a precursor polymerization catalyst; and thermally treating the precursor polymerization catalyst to form a polymerization catalyst.
摘要翻译：一种方法，包括使二氧化硅载体材料与硫酸化剂接触以形成包含硫酸根阴离子的硫酸化二氧化硅载体材料; 热处理硫酸化二氧化硅载体材料以形成经热处理的硫酸化二氧化硅载体材料; 使经热处理的硫酸化二氧化硅载体材料与含铬化合物接触以形成混合物; 并对该混合物进行热处理以形成聚合催化剂。一种方法，包括热处理二氧化硅载体材料以形成经热处理的二氧化硅载体材料; 使经热处理的二氧化硅载体材料与硫酸化剂接触以形成经热处理的硫酸化二氧化硅载体材料; 热处理热处理的硫酸化二氧化硅载体材料以形成加工的二氧化硅载体材料; 使经处理的二氧化硅载体材料与含铬化合物接触以形成前体聚合催化剂; 并对前体聚合催化剂进行热处理以形成聚合催化剂。

23. 发明申请

WO2014137421A1 ACTIVATOR-SUPPORTS IMPREGNATED WITH GROUP VIII TRANSITION METALS FOR POLYMER PROPERTY CONTROL 审中-公开
标题翻译：用于聚合物物质控制的第VIII组过渡金属的活化剂支持
公开(公告)号：WO2014137421A1
公开(公告)日：2014-09-12
申请号：PCT/US2013/071201
申请日：2013-11-21
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max, P , YANG, Qing , CRAIN, Tony, R , COLLINS, Kathy, S
发明人： MCDANIEL, Max, P , YANG, Qing , CRAIN, Tony, R , COLLINS, Kathy, S
IPC分类号： C08F10/00
CPC分类号： C08F10/00 , C08F4/61904 , C08F4/65927 , C08F4/65916 , C08F4/70
摘要： Methods for controlling properties of an olefin polymer using a Group VIII transition metal-modified activator-support are disclosed. The melt index of the polymer can be decreased and the molecular weight of the polymer can be increased via the addition of the transition metal-modified activator-support to the polymerization reactor system.
摘要翻译：公开了使用第VIII族过渡金属改性的活化剂 - 载体来控制烯烃聚合物性质的方法。可以降低聚合物的熔体指数，并且可以通过向聚合反应器体系中加入过渡金属改性的活化剂 - 载体来提高聚合物的分子量。

24. 发明申请

WO2013082346A3 A METHOD OF PREPARING AN OLEFIN POLYMERIZATION CATALYST, THE CATALYST AND ETHYLENE POLYMERS AND COPOLYMERS OBTAINED USING THE CATALYST 审中-公开
公开(公告)号：WO2013082346A3
公开(公告)日：2013-06-06
申请号：PCT/US2012/067175
申请日：2012-11-30
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P , COLLINS, Kathy S
发明人： MCDANIEL, Max P , COLLINS, Kathy S
IPC分类号： B01J21/06 , B01J23/26 , B01J37/03 , B01J37/08 , C08F4/02 , C08F4/22 , C08F4/24 , C08F10/00 , C08F110/00 , B01J35/10 , B01J21/08 , B01J35/00 , B01J37/06
摘要： A method of preparing a catalyst comprising contacting an acidic colloidal silica suspension with a titanium-containing compound to form a mixture, adjusting the pH of mixture to about neutral to form a catalyst support, and contacting the catalyst support with chromium- containing compound to from a chromium-supported catalyst. A catalyst support prepared by contacting a colloidal silica suspension and a titanium-containing compound under acidic conditions to form a mixture, and contacting the mixture with a basic material in an amount sufficient to increase the pH of the mixture to about 7. Ethylene polymers or copolymers made using said catalyst.

25. 发明申请

WO2013082346A2 METHODS OF PREPARING A CATALYST 审中-公开
标题翻译：制备催化剂的方法
公开(公告)号：WO2013082346A2
公开(公告)日：2013-06-06
申请号：PCT/US2012067175
申请日：2012-11-30
申请人： CHEVRON PHILLIPS CHEMICAL CO , MCDANIEL MAX P , COLLINS KATHY S
发明人： MCDANIEL MAX P , COLLINS KATHY S
IPC分类号： B01J21/06
CPC分类号： C08F110/02 , C08F2500/12 , C08F4/025 , C08F10/00 , C08F4/22 , C08F4/24 , C08F10/02 , C08F4/78
摘要： A method of preparing a catalyst comprising contacting an acidic colloidal silica suspension with a titanium-containing compound to form a mixture, adjusting the pH of mixture to about neutral to form a catalyst support, and contacting the catalyst support with chromium-containing compound to from a chromium-supported catalyst. A catalyst support prepared by contacting a colloidal silica suspension and a titanium-containing compound under acidic conditions to form a mixture, and contacting the mixture with a basic material in an amount sufficient to increase the pH of the mixture to about 7.
摘要翻译：一种制备催化剂的方法，包括使酸性胶体二氧化硅悬浮液与含钛化合物接触以形成混合物，将混合物的pH调节至约中性以形成催化剂载体，并将催化剂载体与含铬化合物接触，铬载体催化剂。通过在酸性条件下使胶体二氧化硅悬浮液和含钛化合物接触以形成混合物制备的催化剂载体，并使混合物与碱性物质接触，其量足以将混合物的pH增加至约7。

26. 发明申请

WO2013081826A1 LONG CHAIN BRANCHED POLYMERS AND METHODS OF MAKING SAME 审中-公开
标题翻译：长链分支聚合物及其制备方法
公开(公告)号：WO2013081826A1
公开(公告)日：2013-06-06
申请号：PCT/US2012/064986
申请日：2012-11-14
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , YU, Youlu , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , SOLENBERGER, Alan L , COLLINS, Kathy S
发明人： YU, Youlu , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , SOLENBERGER, Alan L , COLLINS, Kathy S
IPC分类号： C08F110/02
CPC分类号： C08F110/02 , B01J23/26 , B01J35/1009 , B01J35/1014 , B01J35/1019 , C08F10/02 , C08F210/02 , C08F2500/04 , C08F2500/09 , C08F4/69 , C08F4/025
摘要： A polymer having a long chain branching content peaking at greater than about 20 long chain branches per million carbon atoms, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 8 long chain branches per million carbon atoms, a polydispersity index of greater than about 20 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 1 long chain branches per chain, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution.
摘要翻译：具有长链支化含量高于每百万个碳原子大于约20个长支链的聚合物，多分散指数大于约10，其中长链支化在分子量的较高分子量部分下降至约零分配。具有长链支化含量高于每百万个碳原子大于约8个长链分支的聚合物，多分散指数大于约20，其中长链支化在分子量分布的较高分子量部分下降至约零。具有长链支化含量在每链大于约1个长链分支峰值的聚合物，以及多分散指数大于约10，其中长链支链在分子量分布的较高分子量部分下降至约零。

27. 发明申请

WO2009085101A8 METHODS OF PREPARING A POLYMERIZATION CATALYST 审中-公开
标题翻译：制备聚合催化剂的方法
公开(公告)号：WO2009085101A8
公开(公告)日：2010-10-07
申请号：PCT/US2008013513
申请日：2008-12-08
申请人： CHEVRON PHILLIPS CHEMICAL CO , COLLINS KATHY S , MCDANIEL MAX P
发明人： COLLINS KATHY S , MCDANIEL MAX P
IPC分类号： C08F10/00 , C08F4/69
CPC分类号： C08F10/00 , C08F110/02 , C08F4/69 , C08F2500/01 , C08F2500/12
摘要： A method comprising contacting a support with one or more chromium-containing compounds and one or more boria precursors to provide a catalyst precursor, and activating the catalyst precursor to provide a polymerization catalyst.
摘要翻译：一种方法，包括使载体与一种或多种含铬化合物和一种或多种氧化硼前体接触以提供催化剂前体，并活化催化剂前体以提供聚合催化剂。

28. 发明申请

WO2006052232A1 ORGANOCHROMIUM/ METALLOCENE COMBINATION CATALYST FOR PRODUCING BIMODAL RESINS 审中-公开
标题翻译：用于生产二元树脂的组氨酸/金属组合催化剂
公开(公告)号：WO2006052232A1
公开(公告)日：2006-05-18
申请号：PCT/US2004/036650
申请日：2004-11-04
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY, L.P. , MCDANIEL, Max, P. , BENHAM, Elizabeth, A. , JENSEN, Michael, D. , COLLINS, Kathy, S. , MARTIN, Joel, L. , HAWLEY, Gil, R.
发明人： MCDANIEL, Max, P. , BENHAM, Elizabeth, A. , JENSEN, Michael, D. , COLLINS, Kathy, S. , MARTIN, Joel, L. , HAWLEY, Gil, R.
IPC分类号： C08F10/02 , C08F4/02 , C08F4/642 , C08F4/69
CPC分类号： C08F10/02 , C08F4/63912 , C08F4/6392 , C08F4/63925 , C08F4/63927 , C08F110/02 , C08F2420/01 , C08F2420/02 , C08F4/69 , C08F4/02 , C08F4/639 , C08F4/63904 , C08F2500/04 , C08F2500/12 , C08F2500/01 , C08F10/00 , C08F4/69103 , C08F4/63916
摘要： This invention relates to the field of olefin polymerization catalyst compositions, and methods for the polymerization and copolymerization of olefins, including polymerization methods using a supported catalyst composition. In one aspect, the present invention encompasses a catalyst comprising the contact product of at least one metallocene compound, at least one organochromium compound, at least one chemically-treated solid oxide, and at least one organoaluminium compound.
摘要翻译：本发明涉及烯烃聚合催化剂组合物领域，以及烯烃聚合和共聚方法，包括使用负载催化剂组合物的聚合方法。一方面，本发明包括包含至少一种金属茂化合物，至少一种有机锡化合物，至少一种化学处理的固体氧化物和至少一种有机铝化合物的接触产物的催化剂。

29. 发明申请

WO0144308A3 ORGANOMETAL COMPOUND CATALYST 审中-公开
标题翻译：有机化合物催化剂
公开(公告)号：WO0144308A3
公开(公告)日：2002-01-10
申请号：PCT/US0042753
申请日：2000-12-12
申请人： PHILLIPS PETROLEUM CO , MCDANIEL MAX P , COLLINS KATHY S , HAWLEY GIL R , JENSEN MICHAEL D , WITTNER CHRISTOPHER E , BENHAM ELIZABETH A , EATON ANTHONY P , MARTIN JOEL L , ROHLFING DAVID C , YU YOULU
发明人： MCDANIEL MAX P , COLLINS KATHY S , HAWLEY GIL R , JENSEN MICHAEL D , WITTNER CHRISTOPHER E , BENHAM ELIZABETH A , EATON ANTHONY P , MARTIN JOEL L , ROHLFING DAVID C , YU YOULU
IPC分类号： C08F4/16 , C08F4/659 , C08F4/76 , C08F10/00 , C08F210/16 , B01J20/00 , B01J20/02 , B01J20/10 , B01J20/18 , B01J20/26
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F4/65925 , C08F4/65927 , C08F210/16 , C08F2410/02 , C08F2420/02 , C08F2420/04 , Y10S526/943 , C08F4/025 , C08F4/65904 , C08F210/14 , C08F2500/17 , C08F2500/12 , C08F2500/05 , C08F4/6546
摘要： This invention provides catalyst compositions that are useful for polymerizing at least one monomer to produce a polymer. This invention also provides catalyst compositions that are useful for polymerizing at least one monomer to produce a polymer, wherein said catalyst composition comprises contacting an organometal compound, an organoaluminum compound, and a treated solid oxide compound.
摘要翻译：本发明提供了可用于聚合至少一种单体以生产聚合物的催化剂组合物。本发明还提供了可用于聚合至少一种单体以生产聚合物的催化剂组合物，其中所述催化剂组合物包括使有机金属化合物，有机铝化合物和经处理的固体氧化物化合物接触。

30. 发明申请

WO2010107478A1 METHODS OF PREPARING A POLYMERIZATION CATALYST 审中-公开
标题翻译：制备聚合催化剂的方法
公开(公告)号：WO2010107478A1
公开(公告)日：2010-09-23
申请号：PCT/US2010/000778
申请日：2010-03-15
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , BENHAM, Elizabeth A. , MCDANIEL, Max P. , COLLINS, Kathy S. , WHARRY, Stephen M.
发明人： BENHAM, Elizabeth A. , MCDANIEL, Max P. , COLLINS, Kathy S. , WHARRY, Stephen M.
IPC分类号： C08F10/02 , C08F4/24 , C08F4/69
CPC分类号： C08F10/02 , C08F110/02 , C08F4/69 , C08F4/24 , C08F2500/10 , C08F2500/08 , C08F2500/12
摘要： A method comprising (a) contacting a support and a chromium-containing compound to form chromium-containing support, (b) heat treating the chromium-containing support in an oxidizing atmosphere to form a treated support, (c) contacting the treated support with carbon monoxide to form a CO-contacted support, and (d) contacting the CO-contacted support with hydrogen to form a catalyst. A method comprising oxidizing a chromium-treated support to form a polymerization catalyst, contacting the polymerization catalyst with carbon monoxide to form a reduced polymerization catalyst, contacting the reduced polymerization catalyst with hydrogen to form an activated polymerization catalyst, and contacting the activated polymerization catalyst with ethylene in a reaction zone under suitable reaction conditions to form a random copolymer. A method comprising reducing a polymerization catalyst comprising Cr(VI) to form a polymerization catalyst comprising Cr(II), and treating the polymerization catalyst comprising Cr(II) with hydrogen.
摘要翻译：一种方法，包括（a）使载体和含铬化合物接触以形成含铬载体，（b）在氧化气氛中热处理含铬载体以形成经处理的载体，（c）使经处理的载体与一氧化碳以形成CO-接触的载体，和（d）使CO-接触的载体与氢接触以形成催化剂。一种方法，包括氧化铬处理的载体以形成聚合催化剂，使聚合催化剂与一氧化碳接触以形成还原的聚合催化剂，使还原的聚合催化剂与氢接触以形成活化的聚合催化剂，并使活化的聚合催化剂与乙烯在合适的反应条件下在反应区中形成无规共聚物。一种包括还原包含Cr（VI）的聚合催化剂以形成包含Cr（II）的聚合催化剂并用氢气处理包含Cr（II）的聚合催化剂的方法。

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