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1. 发明申请

WO2014035875A1 VAPOR PHASE PREPARATION OF FLUORIDED SOLID OXIDES 审中-公开
标题翻译：氟化固体氧化物的蒸气相制备
公开(公告)号：WO2014035875A1
公开(公告)日：2014-03-06
申请号：PCT/US2013/056606
申请日：2013-08-26
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P , COLLINS, Kathy S , YANG, Qing , CRAIN, Tony R
发明人： MCDANIEL, Max P , COLLINS, Kathy S , YANG, Qing , CRAIN, Tony R
IPC分类号： B01J37/26 , B01J27/12 , C08F10/00
CPC分类号： B01J35/1023 , B01J21/12 , B01J35/02 , B01J35/1019 , B01J35/1047 , B01J37/26 , C08F4/65912 , C08F4/65927 , C08F110/02 , C08F4/65916
摘要： Methods for the vapor phase preparation of fluorided solid oxide activator-supports, using certain calcining temperatures and fluoriding temperatures, are disclosed.
摘要翻译：公开了使用某些煅烧温度和氟化温度来制备氟化固体氧化物活化剂 - 载体的方法。

2. 发明公开

EP2785751A1 LONG CHAIN BRANCHED POLYMERS AND METHODS OF MAKING SAME 有权转让
标题翻译： LANGKETTIGE VERZWEIGTE POLYMERE UND HERSTELLUNGSVERFAHRENDAFÜR
公开(公告)号：EP2785751A1
公开(公告)日：2014-10-08
申请号：EP12791399.4
申请日：2012-11-14
申请人： Chevron Phillips Chemical Company LP , Yu, Youlu , Schwerdtfeger, Eric D , McDaniel, Max P. , Solenberger, Alan L , Collins, Kathy S.
发明人： YU, Youlu , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , SOLENBERGER, Alan L , COLLINS, Kathy S
IPC分类号： C08F110/02
CPC分类号： C08F110/02 , B01J23/26 , B01J35/1009 , B01J35/1014 , B01J35/1019 , C08F10/02 , C08F210/02 , C08F2500/04 , C08F2500/09 , C08F4/69 , C08F4/025
摘要： A polymer having a long chain branching content peaking at greater than about 1 long chain branches per chain, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 20 long chain branches per million carbon atoms, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution.
摘要翻译：具有长链支化含量峰值达到每百万个碳原子大于约20个长支链的聚合物，并且多分散指数大于约10，其中长链支化在分子量的较高分子量部分下降至约零分配。具有长链支化含量高于每百万个碳原子大于约8个长链分支的聚合物，多分散指数大于约20，其中长链支化在分子量分布的较高分子量部分下降至约零。具有长链支化含量的聚合物，其每链长度大于约1个长链支化峰，多分散指数大于约10，其中在分子量分布的较高分子量部分，长链支链降至约零。

3. 发明申请

WO2014134028A1 DUAL ACTIVATOR-SUPPORT CATALYST SYSTEMS 审中-公开
标题翻译：双激活剂 - 支持催化剂体系
公开(公告)号：WO2014134028A1
公开(公告)日：2014-09-04
申请号：PCT/US2014/018283
申请日：2014-02-25
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , YANG, Qing , MCDANIEL, Max P , CRAIN, Tony R , COLLINS, Kathy S
发明人： YANG, Qing , MCDANIEL, Max P , CRAIN, Tony R , COLLINS, Kathy S
IPC分类号： C08F4/6592 , C08F10/02 , C08F110/02 , C08F4/02
CPC分类号： C08F10/02 , C08F110/02 , C08F4/65916 , C08F4/65925 , C08F4/65927 , C08F4/025 , C08F2500/03
摘要： Disclosed herein are polymerization processes for the production of olefin polymers. These polymerization processes use a catalyst system containing at least two activator-supports. One activator-support is a halided solid oxide, and the other activator-support is a sulfated solid oxide and/or phosphated solid oxide.
摘要翻译：本文公开了用于生产烯烃聚合物的聚合方法。这些聚合方法使用含有至少两种活化剂 - 载体的催化剂体系。一种活化剂 - 载体是一种卤化固体氧化物，另一种活化剂 - 载体是硫酸化固体氧化物和/或磷酸化固体氧化物。

4. 发明申请

WO2005107943A1 METHODS OF PREPARING ACTIVE CHROMIUM/ALUMINA CATALYSTS VIA TREATMENT WITH SULFATE AND POLYMERS PRODUCED USING THE CHROMIUM/ALUMINA CATALYSTS 审中-公开
标题翻译：通过使用铬/铝催化剂生产的硫酸钠和聚合物处理活性铬/氧化铝催化剂的制备方法
公开(公告)号：WO2005107943A1
公开(公告)日：2005-11-17
申请号：PCT/US2005/009668
申请日：2005-03-24
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P. , COLLINS, Kathy S , BENHAM, Elizabeth A. , DESLAURIERS, Paul J.
发明人： MCDANIEL, Max P. , COLLINS, Kathy S , BENHAM, Elizabeth A. , DESLAURIERS, Paul J.
IPC分类号： B01J27/053
CPC分类号： B01J27/053 , B01J23/26 , C08F10/02 , C08F110/02 , C08F4/69 , C08F2500/04 , C08F2500/12 , C08F4/025
摘要： Methods of preparing a polymerization catalyst are provided that include contacting a support comprising alumina with a sulfating agent and with chromium. The support can be calcined after loading the sulfating agent and the chromium on the support. Alternatively, the sulfating agent can be loaded on the support while calcining it. Alternatively, the support can be calcined after contacting it with the sulfating agent and before contacting it with an organochromium compound. Catalysts compositions comprising chromium and a sulfate treated alumina support that were formed by the foregoing method are provided. The catalyst compositions have increased catalyst activity. Methods of producing a polymer include contacting at least one olefin with the catalyst compositions are provided. The polymer compositions exhibit relatively low levels of long chain branching and relatively high molecular weights.
摘要翻译：提供制备聚合催化剂的方法包括使包含氧化铝的载体与硫酸化剂和铬接触。载体可以在将硫酸化剂和铬载载在载体上之后进行煅烧。或者，硫酸化剂可以在煅烧时装载到载体上。或者，支持体可以在与硫酸化剂接触之后并且在与有机铬化合物接触之前被煅烧。提供了通过上述方法形成的包含铬和硫酸盐处理的氧化铝载体的催化剂组合物。催化剂组合物具有增加的催化剂活性。制备聚合物的方法包括使至少一种烯烃与催化剂组合物接触。聚合物组合物表现出较低水平的长链支化和相对较高的分子量。

5. 发明申请

WO2014164614A1 METHOD FOR THE PREPARATION OF POLYMERIZATION CATALYSTS 审中-公开
标题翻译：聚合催化剂的制备方法
公开(公告)号：WO2014164614A1
公开(公告)日：2014-10-09
申请号：PCT/US2014/023009
申请日：2014-03-11
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P , COLLINS, Kathy S , SCHWERDTFEGER, Eric D , SOLENBERGER, Alan L
发明人： MCDANIEL, Max P , COLLINS, Kathy S , SCHWERDTFEGER, Eric D , SOLENBERGER, Alan L
IPC分类号： C08F10/00
CPC分类号： C08F4/22 , C08F10/00 , C08F4/24 , C08F4/025 , C08F110/02 , C08F2500/12
摘要： A method comprising contacting a support material with a transition metal compound to produce a mixture; thermally treating the mixture in the presence of oxygen at a temperature in a range of from about 100° C to about 500° C for a period of from about 1 hour to about 10 hours, wherein at least a portion of the transition metal sublimes onto the support material to produce a support material comprising a dispersed transition metal; and thermally treating the support material comprising the dispersed transition metal in an oxidizing atmosphere at a temperature in a range of from about 550° C to about 900° C for a period of from about 1 hour to about 10 hours to produce a polymerization catalyst.
摘要翻译：一种方法，包括使支撑材料与过渡金属化合物接触以产生混合物; 在氧气存在下，在约100℃至约500℃的温度范围内热处理混合物约1小时至约10小时，其中至少一部分过渡金属升华到用于生产包含分散的过渡金属的载体材料的载体材料; 并在包含分散的过渡金属的载体材料的氧化气氛中在约550℃至约900℃的温度范围内热处理约1小时至约10小时，以制备聚合催化剂。

6. 发明申请

WO2014164514A2 METHODS OF PREPARING A POLYMERIZATION CATALYST 审中-公开
标题翻译：制备聚合催化剂的方法
公开(公告)号：WO2014164514A2
公开(公告)日：2014-10-09
申请号：PCT/US2014/022663
申请日：2014-03-10
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P , COLLINS, Kathy S
发明人： MCDANIEL, Max P , COLLINS, Kathy S
IPC分类号： C08F10/00
CPC分类号： C08F10/00 , C08F4/69 , C08F4/025 , C08F110/02 , C08F2500/03 , C08F2500/12
摘要： A method comprising contacting a silica support material with a sulfating agent to form a sulfated silica support material comprising sulfate anions; thermally treating the sulfated silica support material to form a thermally treated sulfated silica support material; contacting the thermally treated sulfated silica support material with a chromium- containing compound to form a mixture; and thermally treating the mixture to form a polymerization catalyst. A method comprising thermally treating a silica support material to form a thermally-treated silica support material; contacting the thermally-treated silica support material with a sulfating agent to form a thermally treated sulfated silica support material; thermally treating the thermally treated sulfated silica support material to form a processed silica support material; contacting the processed silica support material with a chromium-containing compound to form a precursor polymerization catalyst; and thermally treating the precursor polymerization catalyst to form a polymerization catalyst.
摘要翻译：一种方法，包括使二氧化硅载体材料与硫酸化剂接触以形成包含硫酸根阴离子的硫酸化二氧化硅载体材料; 热处理硫酸化二氧化硅载体材料以形成经热处理的硫酸化二氧化硅载体材料; 使经热处理的硫酸化二氧化硅载体材料与含铬化合物接触以形成混合物; 并对该混合物进行热处理以形成聚合催化剂。一种方法，包括热处理二氧化硅载体材料以形成经热处理的二氧化硅载体材料; 使经热处理的二氧化硅载体材料与硫酸化剂接触以形成经热处理的硫酸化二氧化硅载体材料; 热处理热处理的硫酸化二氧化硅载体材料以形成加工的二氧化硅载体材料; 使经处理的二氧化硅载体材料与含铬化合物接触以形成前体聚合催化剂; 并对前体聚合催化剂进行热处理以形成聚合催化剂。

7. 发明申请

WO2013082346A3 A METHOD OF PREPARING AN OLEFIN POLYMERIZATION CATALYST, THE CATALYST AND ETHYLENE POLYMERS AND COPOLYMERS OBTAINED USING THE CATALYST 审中-公开
公开(公告)号：WO2013082346A3
公开(公告)日：2013-06-06
申请号：PCT/US2012/067175
申请日：2012-11-30
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P , COLLINS, Kathy S
发明人： MCDANIEL, Max P , COLLINS, Kathy S
IPC分类号： B01J21/06 , B01J23/26 , B01J37/03 , B01J37/08 , C08F4/02 , C08F4/22 , C08F4/24 , C08F10/00 , C08F110/00 , B01J35/10 , B01J21/08 , B01J35/00 , B01J37/06
摘要： A method of preparing a catalyst comprising contacting an acidic colloidal silica suspension with a titanium-containing compound to form a mixture, adjusting the pH of mixture to about neutral to form a catalyst support, and contacting the catalyst support with chromium- containing compound to from a chromium-supported catalyst. A catalyst support prepared by contacting a colloidal silica suspension and a titanium-containing compound under acidic conditions to form a mixture, and contacting the mixture with a basic material in an amount sufficient to increase the pH of the mixture to about 7. Ethylene polymers or copolymers made using said catalyst.

8. 发明申请

WO2013081826A1 LONG CHAIN BRANCHED POLYMERS AND METHODS OF MAKING SAME 审中-公开
标题翻译：长链分支聚合物及其制备方法
公开(公告)号：WO2013081826A1
公开(公告)日：2013-06-06
申请号：PCT/US2012/064986
申请日：2012-11-14
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , YU, Youlu , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , SOLENBERGER, Alan L , COLLINS, Kathy S
发明人： YU, Youlu , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , SOLENBERGER, Alan L , COLLINS, Kathy S
IPC分类号： C08F110/02
CPC分类号： C08F110/02 , B01J23/26 , B01J35/1009 , B01J35/1014 , B01J35/1019 , C08F10/02 , C08F210/02 , C08F2500/04 , C08F2500/09 , C08F4/69 , C08F4/025
摘要： A polymer having a long chain branching content peaking at greater than about 20 long chain branches per million carbon atoms, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 8 long chain branches per million carbon atoms, a polydispersity index of greater than about 20 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 1 long chain branches per chain, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution.
摘要翻译：具有长链支化含量高于每百万个碳原子大于约20个长支链的聚合物，多分散指数大于约10，其中长链支化在分子量的较高分子量部分下降至约零分配。具有长链支化含量高于每百万个碳原子大于约8个长链分支的聚合物，多分散指数大于约20，其中长链支化在分子量分布的较高分子量部分下降至约零。具有长链支化含量在每链大于约1个长链分支峰值的聚合物，以及多分散指数大于约10，其中长链支链在分子量分布的较高分子量部分下降至约零。

9. 发明申请

WO2015009484A1 METHODS FOR PRODUCING FLUORIDED-CHLORIDED SILICA-COATED ALUMINA ACTIVATOR-SUPPORTS AND CATALYST SYSTEMS CONTAINING THE SAME 审中-公开
标题翻译：用于生产氟化氯化二氧化硅氧化铝活化剂 - 载体和含有其的催化剂体系的方法
公开(公告)号：WO2015009484A1
公开(公告)日：2015-01-22
申请号：PCT/US2014/045708
申请日：2014-07-08
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP
发明人： MCDANIEL, Max P , KILGORE, Uriah J , YANG, Qing , COLLINS, Kathy S
IPC分类号： B01J31/22 , B01J31/14 , B01J37/02 , B01J37/08 , B01J37/24 , B01J37/26 , B01J21/12 , C08F110/02 , C08F110/06 , C08F10/00 , C08F4/02 , C08F4/659
CPC分类号： C08F210/16 , B01J21/04 , B01J21/12 , B01J27/053 , B01J27/08 , B01J31/143 , B01J31/1608 , B01J31/1616 , B01J31/2295 , B01J35/1019 , B01J35/1023 , B01J35/1042 , B01J35/1047 , B01J37/0203 , B01J37/0207 , B01J37/0209 , B01J37/24 , B01J37/26 , B01J2531/48 , B01J2531/49 , C08F4/02 , C08F4/025 , C08F4/65908 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F4/65925 , C08F4/65927 , C08F4/76 , C08F10/00 , C08F110/02 , C08F110/06 , C08F210/02 , Y02P20/52 , Y10S526/943 , C08F4/65904 , C08F2500/05
摘要： Methods for the preparation of fluorided-chlorided silica-coated alumina activator-supports are disclosed. These comprise (a) calcining a silica-coated alumina at a peak calcining temperature to produce a calcined silica-coated alumina; (b) contacting the calcined silica- coated alumina with a chlorine-containing compound and calcining at a peak chloriding temperature to produce a chlorided silica-coated alumina; and (c) contacting the chlorided silica-coated alumina with a fluorine-containing compound and calcining at a peak fluoriding temperature to produce the fluorided-chlorided silica-coated alumina. These activator-supports can be used in catalyst systems further comprising a metallocene compound and optionally a co-catalyst, for the production of olefin-based polymers, such as polyethylene and polypropylene.
摘要翻译：公开了制备氟化氯化二氧化硅涂覆的氧化铝活化剂 - 载体的方法。这些包括（a）在峰值煅烧温度下煅烧二氧化硅涂覆的氧化铝以产生煅烧二氧化硅涂覆的氧化铝; （b）使经煅烧的二氧化硅涂覆的氧化铝与含氯化合物接触并在峰值氯化温度下煅烧以产生氯化二氧化硅涂覆的氧化铝; 和（c）将氯化二氧化硅涂覆的氧化铝与含氟化合物接触并在峰值氟化温度下煅烧以产生氟化氯化二氧化硅涂覆的氧化铝。这些活化剂 - 载体可用于进一步包含茂金属化合物和任选的助催化剂的催化剂体系中，用于生产基于烯烃的聚合物如聚乙烯和聚丙烯。

10. 发明申请

WO2015105738A2 CHROMIUM (III) CATALYST SYSTEMS WITH ACTIVATOR-SUPPORTS 审中-公开
标题翻译：铬（III）催化剂系统与活化剂支持
公开(公告)号：WO2015105738A2
公开(公告)日：2015-07-16
申请号：PCT/US2015/010094
申请日：2015-01-05
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP
发明人： MCDANIEL, Max P , HLAVINKA, Mark L , COLLINS, Kathy S
IPC分类号： C08F4/69
CPC分类号： C08F10/02 , C08F4/63904 , C08F4/63912 , C08F4/63916 , C08F4/63927 , C08F4/69146 , C08F4/025 , C08F210/16 , C08F210/14 , C08F2500/08 , C08F2500/01 , C08F2500/04 , C08F2500/12 , C08F2500/09 , C08F110/02
摘要： Methods for preparing supported chromium catalysts containing a chromium (III) compound and an activator-support are disclosed. These supported chromium catalysts can be used in catalyst compositions for the polymerization of olefins to produce polymers having low levels of long chain branching, and with greater sensitivity to the presence of hydrogen during polymerization.
摘要翻译：公开了制备含有铬（III）化合物和活化剂 - 载体的负载型铬催化剂的方法。这些负载型铬催化剂可以用于烯烃聚合的催化剂组合物中，以生产具有低水平长链支化的聚合物，并且在聚合过程中对氢气存在的敏感性更高。

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