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11. 发明专利

JP2007153762A Method for hydrating olefin 有权
标题翻译：油脂加水方法
公开(公告)号：JP2007153762A
公开(公告)日：2007-06-21
申请号：JP2005348038
申请日：2005-12-01
申请人： Nippon Oil Corp , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 新日本石油株式会社
发明人： YANAGAWA SHINICHIRO , HARA YUKIKAZU
IPC分类号： C07C29/04 , B01J27/053 , C07B61/00 , C07C31/10
CPC分类号： C07C29/04 , C07B61/00 , C07C31/10 , C07C31/12
摘要： PROBLEM TO BE SOLVED: To provide a method for hydrating an olefin for efficiently producing the corresponding alcohol by hydration reaction of the 2-5C olefin.
SOLUTION: The method for hydrating an olefin comprises conducting a hydration reaction of the 2-5C olefin at 100-250°C in the presence of a carbon-based solid acid catalyst that is obtained by carbonizing and sulfonating an organic substance. Specifically, in this method, the organic substance is an aromatic hydrocarbon or a saccharide. More specifically, in this method, the olefin is propylene or a butene. Furthermore specifically, in this method, the temperature of the hydration reaction is equal to or higher than 120°C, and in another version of the above method, the temperature of the hydration reaction is equal to or higher than 150°C.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供通过2-5C烯烃的水合反应来有效地生产相应的醇的烯烃的水合方法。解决方案：烯烃水合方法包括在通过碳化和磺化有机物质获得的碳基固体酸催化剂存在下，在100-250℃下进行2-5C烯烃的水合反应。具体地，在该方法中，有机物质是芳族烃或糖类。更具体地，在该方法中，烯烃是丙烯或丁烯。此外，在该方法中，水合反应的温度等于或高于120℃，在上述方法的另一形式中，水合反应的温度等于或高于150℃。版权所有（C）2007，JPO＆INPIT

12. 发明专利

JP2011142894A Biomass treatment system 审中-公开
标题翻译：生物质处理系统
公开(公告)号：JP2011142894A
公开(公告)日：2011-07-28
申请号：JP2010008555
申请日：2010-01-18
申请人： Ihi Corp , Kanagawa Acad Of Sci & Technol , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 株式会社Ihi , 財団法人神奈川科学技術アカデミー
发明人： NARAI KENTARO , KANEKO NORIMITSU , KITANO MAKOTO , SATO KENJI , OKA TATSUYA , HARA YUKIKAZU , YAMAGUCHI DAIZO
IPC分类号： C13K13/00 , C07H3/02
摘要： PROBLEM TO BE SOLVED: To provide a biomass treatment system overcoming the drawbacks of insufficient monosaccharification in a solid acid catalytic reaction or deterioration and inactivation of a solid acid catalyst.
SOLUTION: The biomass treatment system includes: a pressurized hot water reactor to produce polysaccharides by passing pressurized hot water through biomass in a reaction vessel to hydrolyze the biomass; and a solid acid catalytic reactor to produce monosaccharides from the polysaccharides using a solid acid catalyst; wherein the solid acid catalytic reactor includes a control unit for setting solid acid catalytic decomposition conditions according to the hydrolysis conditions for the pressurized hot water reactor.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：解决的问题：提供一种克服固体酸催化反应中单糖化不足或固体酸催化剂劣化和失活的缺点的生物质处理体系。生物处理系统包括：加压热水反应器，通过使加压的热水通过反应容器中的生物质来生产多糖，以水解生物质; 和使用固体酸催化剂从多糖制备单糖的固体酸催化反应器; 其中固体酸催化反应器包括根据加压热水反应器的水解条件设定固体酸催化分解条件的控制单元。版权所有（C）2011，JPO＆INPIT

13. 发明专利

JP2011088827A Method for hydrolyzing polysaccharides and stirring apparatus therefor 审中-公开
标题翻译：水解多糖的方法及其制备装置
公开(公告)号：JP2011088827A
公开(公告)日：2011-05-06
申请号：JP2008028358
申请日：2008-02-08
申请人： Kanagawa Acad Of Sci & Technol , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 財団法人神奈川科学技術アカデミー
发明人： HARA YUKIKAZU , YAMAGUCHI DAIZO
IPC分类号： C07H1/00 , B01J21/18 , C07B61/00 , C07H3/02
CPC分类号： B01F7/18 , B01F7/00275 , B01F7/00633 , B01F7/20 , C13K1/02 , C13K1/06
摘要： PROBLEM TO BE SOLVED: To provide a method for hydrolyzing polysaccharides with a solid acid catalyst, whereby the hydrolysis can be more efficiently conducted than by known methods, and a stirring apparatus for the method. SOLUTION: The method for hydrolyzing the polysaccharides with the solid acid catalyst includes conducting a hydrolysis reaction under such conditions that water is used in an amount smaller than that corresponding to the proportion of the solid acid catalyst to the water, i.e., (solid acid catalyst): water, of 3:7 by weight. The stirring apparatus for the method includes a vessel and a stirrer disposed in the vessel. The stirrer includes a rotating shaft which is rotatable and a plurality of platy stirring blades fixed to the rotating shaft. The stirring blades are disposed in a plurality of stages apart from each other in the axial direction of the rotating shaft. When viewed from one end side of the rotating shaft, the stirring blade fixed in one position is disposed so as to differ in phase angle from the stirring blade fixed in an adjacent position on the rotating shaft. Both radial-direction ends of each stirring blade are bent at an angle of ±60° against an angle parallel with the inner wall of the vessel when viewed from a lateral side of the rotating shaft. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种用固体酸催化剂水解多糖的方法，由此可以比已知方法更有效地进行水解，以及该方法的搅拌装置。解决方案：用固体酸催化剂水解多糖的方法包括在水的使用量比固体酸催化剂与水的比例小的条件下进行水解反应，即（固体酸催化剂）：水，重量比为3：7。用于该方法的搅拌装置包括设置在容器中的容器和搅拌器。搅拌器包括可旋转的旋转轴和固定到旋转轴的多个板状搅拌叶片。搅拌叶片沿旋转轴的轴向彼此分开设置。当从旋转轴的一端侧观察时，固定在一个位置的搅拌叶片被设置成与固定在旋转轴上的相邻位置的搅拌叶片的相位角不同。当从旋转轴的侧面观察时，每个搅拌叶片的两个径向端部以相对于容器的内壁平行的角度以±60°的角度弯曲。版权所有（C）2011，JPO＆INPIT

14. 发明专利

JP2011011201A Carbon-based solid acid and method for producing the same 有权
标题翻译：碳基固体酸及其制造方法
公开(公告)号：JP2011011201A
公开(公告)日：2011-01-20
申请号：JP2009210531
申请日：2009-09-11
申请人： Futamura Chemical Co Ltd , Kanagawa Acad Of Sci & Technol , Nisso Engineering Co Ltd , Tokyo Institute Of Technology , フタムラ化学株式会社 , 国立大学法人東京工業大学 , 日曹エンジニアリング株式会社 , 財団法人神奈川科学技術アカデミー
发明人： KITANO MASAAKI , HARA YUKIKAZU , KODAMA ATSUSHI , KOSAKA TSUTOMU , ISHIKAWA TAKAHIRO , SUDO TOSHIYUKI , IWAKOSHI MARI , YONETANI AKIRA
IPC分类号： B01J31/26 , B01J31/02 , B01J35/10 , B01J37/08 , C07C309/28 , C07C309/62
摘要： PROBLEM TO BE SOLVED: To provide a carbon-based solid acid capable of being produced from raw materials which can be obtained at low prices and are suitable for mass production and to provide a method for producing the carbon-based solid acid, which satisfies preparation conditions suitable for producing the carbon-based solid acid and the efficiency of which is made higher than that of a method for producing the carbon-based solid acid by a reaction using strong sulfuric acid or fuming sulfuric acid.SOLUTION: The carbon-based solid acid includes porous carbon into which a sulfonate group is introduced and which has 3-1,600 m/g BET specific surface area to be defined below. The amount of the sulfonate group in the porous carbon is ≥0.2 mmol/g. The porous carbon is sulfonated by bringing sulfur trioxide or a sulfur trioxide-containing sulfonating agent into contact with a cellulose-containing raw material or a vegetable raw material. Otherwise, the porous carbon is sulfonated by impregnating the vegetable raw material with zinc chloride or phosphoric acid, heating and preliminarily carbonating the raw material thus impregnated, and heating and sulfonating the preliminarily-carbonated raw material in strong sulfuric acid or fuming sulfuric acid or in the gas or liquid of sulfur trioxide.
摘要翻译：要解决的问题：提供能够以低价格获得并适合于批量生产的原料生产的碳基固体酸，并提供满足制备的碳基固体酸的制备方法适用于生产碳基固体酸的条件，其效率高于通过使用强硫酸或发烟硫酸的反应生产碳基固体酸的方法。条件：碳基固体酸包括其中引入磺酸盐基团的多孔碳，其具有下面定义的3-1,600m 2 / g BET比表面积。多孔碳中磺酸盐基团的量为≥0.2mmol/ g。通过使三氧化硫或含三氧化硫的磺化剂与含纤维素的原料或植物原料接触来将多孔碳磺化。另外，通过用氯化锌或磷酸浸渍植物原料来对多孔碳进行磺化，对浸渍的原料进行加热并预先碳酸化，并将预先碳酸化的原料在强硫酸或发烟硫酸或三氧化硫的气体或液体。

15. 发明专利

JP2009268960A Catalyst precursor, catalyst material, and method of preparing catalyst 有权
标题翻译：催化剂前体，催化剂材料和制备催化剂的方法
公开(公告)号：JP2009268960A
公开(公告)日：2009-11-19
申请号：JP2008120817
申请日：2008-05-06
申请人： Tokyo Institute Of Technology , Toyota Industries Corp , 国立大学法人東京工業大学 , 株式会社豊田自動織機
发明人： SAGA SHOTA , SHIMO TOSHIHISA , MURAZAKI TAKANORI , HARA YUKIKAZU , NAKAJIMA KIYOTAKA
IPC分类号： B01J23/755 , B01J23/42 , B01J23/72 , B01J23/745
CPC分类号： B01J23/42 , B01J21/18 , B01J23/72 , B01J23/745 , B01J23/755 , B01J31/08 , B01J31/10 , B01J35/006 , B01J37/084 , B01J37/18
摘要： PROBLEM TO BE SOLVED: To provide a novel catalyst precursor prepared by fixing a metal species to a specific solid acid, a catalyst material derived from the catalyst precursor, and method of preparing the catalyst. SOLUTION: The catalyst precursor includes amorphous carbon to which a metal salt of an acidic group has been introduced. The precursor is synthesized by mixing the amorphous carbon to which an acidic group has been introduced with an aqueous solution comprising a metal ion and exchanging the ions. The catalyst material is prepared by reducing the catalyst precursor. The catalyst material includes a micro-support comprising graphene sheets constituting the amorphous carbon and a catalyst metal produced by reducing the metal ion and being supported by the micro-support. The catalyst material has a catalytic function different from an acid catalyst function owned by a solid acid. The growth of the catalyst metal particles in the catalyst material is suppressed because the metal ion supported by the micro-support (graphene sheets) and fixed to the carbon solid acid has a bond with the micro-support. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供通过将金属物质固定到特定固体酸，由催化剂前体衍生的催化剂材料和制备催化剂的方法制备的新型催化剂前体。解决方案：催化剂前体包括已经引入酸性基团的金属盐的无定形碳。通过将已经引入了酸性基团的无定形碳与包含金属离子的水溶液混合并交换离子来合成前体。通过还原催化剂前体制备催化剂材料。催化剂材料包括包含构成无定形碳的石墨烯片的微载体和通过还原金属离子并被微载体支持而制备的催化剂金属。催化剂材料具有与固体酸所具有的酸催化剂功能不同的催化功能。催化剂材料中的催化剂金属颗粒的生长被抑制，因为由微载体（石墨烯片）负载并固定到碳固体酸上的金属离子与微载体具有键合。版权所有（C）2010，JPO＆INPIT

16. 发明专利

JP2009215172A Production method of furfurals 审中-公开
标题翻译：芙蓉的生产方法
公开(公告)号：JP2009215172A
公开(公告)日：2009-09-24
申请号：JP2008057297
申请日：2008-03-07
申请人： Tokyo Institute Of Technology , 国立大学法人東京工業大学
发明人： HARA YUKIKAZU , NAKAJIMA KIYOTAKA , YAMASHITA SHINYA
IPC分类号： C07D307/46
摘要： PROBLEM TO BE SOLVED: To provide a means for highly selectively producing HMF (5-hydroxymethylfurfural) from glucose as a raw material.
SOLUTION: The production method of furfurals comprises causing a monosaccharide or a disaccharide to react with hydrated niobic acid and collecting furfurals from the reaction product.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供从葡萄糖作为原料高度选择性地生产HMF（5-羟甲基糠醛）的方法。解决方案：糠醛的制备方法包括使单糖或二糖与水合的铌酸反应并从反应产物中收集糠醛。版权所有（C）2009，JPO＆INPIT

17. 发明专利

JP2009067730A Method for producing anhydrosugar, organic acid and furfural 审中-公开
标题翻译：生产无机盐，有机酸和糠醛的方法
公开(公告)号：JP2009067730A
公开(公告)日：2009-04-02
申请号：JP2007238710
申请日：2007-09-14
申请人： Tokyo Institute Of Technology , 国立大学法人東京工業大学
发明人： HARA YUKIKAZU , NAKAJIMA KIYOTAKA , YAMASHITA SHINYA
IPC分类号： C07C51/00 , C07C59/185 , C07D307/48 , C07H3/10 , C13K1/00
摘要： PROBLEM TO BE SOLVED: To provide a means for efficiently producing anhydrosugars such as levoglucosan, furfurals such as HMF (hydromethylfurfural), etc., and organic acids such as levulinic acid, etc.
SOLUTION: The method for decomposing monosaccharides and disaccharides is characterized by reacting the monosaccharides or disaccharides with a sulfonic acid group-containing carbonaceous material, and a method for producing the anhydrosugars, organic acids or furfurals comprises utilizing the above method of decomposition.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供有效生产诸如左旋葡聚糖，糠醛如HMF（氢化乙基糠醛）等的脱氢葡萄糖和有机酸如乙酰丙酸等的方法。解决方案：分解方法单糖和二糖的特征在于使单糖或二糖与含磺酸基的碳质材料反应，以及制造脱水糖，有机酸或糠醛的方法包括利用上述分解方法。版权所有（C）2009，JPO＆INPIT

18. 发明专利

JP2011184568A Method for producing polymer, and use 有权
标题翻译：生产聚合物的方法和用途
公开(公告)号：JP2011184568A
公开(公告)日：2011-09-22
申请号：JP2010051339
申请日：2010-03-09
申请人： Kanagawa Acad Of Sci & Technol , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 財団法人神奈川科学技術アカデミー
发明人： HARA YUKIKAZU , KAKUNO KENJI
IPC分类号： C08F8/36 , B01J27/10 , B01J31/06 , C07B61/00 , C07C2/86 , C07C15/16 , C07C41/01 , C07C43/205 , C08F8/00
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a solid acid catalyst which exerts an excellent catalytic ability even when being used as a catalyst for a chemical reaction performed in a hydrophobic organic solvent.
SOLUTION: The method for producing a polymer which functions as the solid acid catalyst includes the steps of: reacting a vinyl aromatic polymer with a polycyclic aromatic compound; and treating the obtained polymer with chlorosulfuric acid. There are provided the new solid acid catalyst which exerts the excellent catalytic ability when being used as the acid catalyst for the chemical reaction in the hydrophobic organic solvent and the method for producing the solid acid catalyst. The solid acid catalyst exerts the chemical reaction in the hydrophobic organic solvent, particularly the high catalytic ability as the acid catalyst for alkylation.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供即使在用作疏水性有机溶剂中进行的化学反应的催化剂时也具有优异的催化能力的固体酸催化剂的制造方法。解决方案：用作固体酸催化剂的聚合物的制备方法包括以下步骤：使乙烯基芳族聚合物与多环芳族化合物反应; 并用氯磺酸处理得到的聚合物。提供了用作疏水性有机溶剂中的化学反应的酸催化剂和固体酸催化剂的制造方法时，具有优异的催化能力的新型固体酸催化剂。固体酸催化剂在疏水性有机溶剂中发挥化学反应，特别是作为烷基化用酸催化剂的高催化能力。版权所有（C）2011，JPO＆INPIT

19. 发明专利

JP2011142892A Solid acid catalyst saccharification apparatus and method 审中-公开
标题翻译：固体催化剂分离装置及方法
公开(公告)号：JP2011142892A
公开(公告)日：2011-07-28
申请号：JP2010008552
申请日：2010-01-18
申请人： Ihi Corp , Kanagawa Acad Of Sci & Technol , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 株式会社Ihi , 財団法人神奈川科学技術アカデミー
发明人： KITANO MAKOTO , SATO KENJI , NARAI KENTARO , OKA TATSUYA , HARA YUKIKAZU , YAMAGUCHI DAIZO
IPC分类号： C13K1/02 , B01F13/02 , B01J27/053 , B01J29/06 , B01J38/00
CPC分类号： B01F7/18 , B01F13/0255 , B01J27/053 , C13K1/02 , C13K13/002
摘要： PROBLEM TO BE SOLVED: To provide a solid acid catalyst saccharification apparatus which can accurately grasp the reaction state of a raw material saccharification process using a solid acid catalyst.
SOLUTION: This solid acid catalyst saccharification apparatus comprises a catalyst reaction tank 3 for receiving a polysaccharide of raw material together with water and a solid acid catalyst X2 as a mixture X3 and subjecting the polysaccharide to a monosaccharification treatment with the solid acid catalyst X2, a stirring device 4 for stirring the mixture liquid X3 in the catalyst reaction tank 3, an oxidation-reduction potentiometer 5 for measuring the oxidation-reduction potential of the mixture liquid X3 in the catalyst reaction tank 3, and a pH meter 6 for measuring the pH of the mixture liquid X3 in the catalyst reaction tank 3.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种能够精确地掌握使用固体酸催化剂的原料糖化方法的反应状态的固体酸催化剂糖化装置。该固体酸催化剂糖化装置包括：催化剂反应槽3，用于将原料的多糖与水一起接收，固体酸催化剂X2作为混合物X3，并用固体酸催化剂进行单糖化处理 X2，用于搅拌催化剂反应槽3中的混合液体X3的搅拌装置4，用于测量催化剂反应槽3中的混合液体X3的氧化还原电位的氧化还原电位计5和用于测量催化剂反应槽3中混合液体的pH值。（C）2011年，JPO＆INPIT

20. 发明专利

JP2009114273A Method of manufacturing fatty acid monoesterified product using regenerated solid acid catalyst 有权
标题翻译：使用再生固体酸催化剂制造脂肪酸单体化产品的方法
公开(公告)号：JP2009114273A
公开(公告)日：2009-05-28
申请号：JP2007286876
申请日：2007-11-05
申请人： Asahi Kasei Corp , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 旭化成株式会社
发明人： YAMASHITA KUNIHIKO , HARA YUKIKAZU
IPC分类号： C11C3/10 , C07B61/00 , C07C67/03 , C07C69/24 , C07C69/52 , C10L1/02 , C10L1/08
CPC分类号： Y02P20/584
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing a fuel for diesel engines having a low acid value from oils and fats using as a catalyst a sulfonic acid group-introduced amorphous carbon catalyst washed with water. SOLUTION: A fatty acid monoesterified product is manufactured by transesterification of an animal oil and/or a vegetable oil with an alcohol using a sulfonic acid group-introduced amorphous carbon catalyst regenerated by washing with water. The method permits continuous and inexpensive manufacture of the fatty acid monoesterified product. COPYRIGHT: (C)2009,JPO&INPIT

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