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1. 发明专利

JP2014000501A Method and apparatus for regenerating carbon-based solid acid catalyst 审中-公开
标题翻译：用于再生碳酸的固体催化剂的方法和装置
公开(公告)号：JP2014000501A
公开(公告)日：2014-01-09
申请号：JP2012136110
申请日：2012-06-15
申请人： Ihi Corp , 株式会社Ihi , Tokyo Institute Of Technology , 国立大学法人東京工業大学
发明人： NARAI KENTARO , KANEKO NORIMITSU , SATO KENJI , KITANO MAKOTO , OKA TATSUYA , HARA YUKIKAZU , NAKAJIMA KIYOTAKA
IPC分类号： B01J27/30 , B01J27/053 , B01J38/60 , C07H3/06 , C12P7/10
CPC分类号： Y02E50/16 , Y02P20/584
摘要： PROBLEM TO BE SOLVED: To provide a method for reducing an energy cost required for regenerating a carbon-based solid acid catalyst as compared with before.SOLUTION: There is provided an apparatus for regenerating a carbon-based solid acid catalyst which comprises: a sulfonation means reaction tube 3a for placing a carbon-based solid acid catalyst which has been used for treating soluble materials in a sulfonic acid atmosphere; an inlet three-way valve 3b; an outlet three-way valve 3c; a sulfuric acid tank 3d; a sulfuric acid supply pump 3e; a sulfuric acid supply valve 3f; a sulfuric acid supply pipe 3g; an ethanol tank 3h; an ethanol supply pump 3i; an ethanol supply valve 3j; a suction pump 3k; and a discharge valve 3m.
摘要翻译：要解决的问题：提供一种降低碳基固体酸催化剂再生所需的能量成本的方法。解决方案：提供一种用于再生碳基固体酸催化剂的装置，其包括：磺化是指将用于处理可溶性物质的碳系固体酸催化剂置于磺酸气氛中的反应管3a; 入口三通阀3b; 出口三通阀3c; 硫酸罐3d; 硫酸供给泵3e; 硫酸供给阀3f; 硫酸供给管3g; 乙醇罐3h; 乙醇供应泵3i; 乙醇供给阀3j; 抽水泵3k; 和排出阀3m。

2. 发明专利

JP2011068578A Apparatus and method for treating biomass 审中-公开
标题翻译：用于处理生物量的装置和方法
公开(公告)号：JP2011068578A
公开(公告)日：2011-04-07
申请号：JP2009219362
申请日：2009-09-24
申请人： Ihi Corp , Kanagawa Acad Of Sci & Technol , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 株式会社Ihi , 財団法人神奈川科学技術アカデミー
发明人： SATO KENJI , NARAI KENTARO , KITANO MAKOTO , KANEKO NORIMITSU , HARA YUKIKAZU , YAMAGUCHI DAIZO
IPC分类号： C07H3/02 , C07H1/08 , C10L1/02 , C12M1/00
CPC分类号： C13K1/02 , C12M21/12 , C12M45/06 , C13K13/00 , C13K13/002
摘要： PROBLEM TO BE SOLVED: To provide an apparatus for treating biomass, enhancing a sugar yield, the reaction speed of a solid acid catalyst, and the capability of separating a solid acid catalyst.
SOLUTION: The apparatus for treating biomass is configured to include a pressurized hydrothermal reactor that hydrolyzes biomass under a first reaction condition employed in decomposing hemicellulose, to produce a first polysaccharide solution comprising a xylooligosaccharide using pressurized hot water, and subsequently hydrolyzes the biomass under a second reaction condition employed in decomposing cellulose, to produce a second polysaccharide solution comprising a cellooligosaccharide using pressurized hot water; a first catalytic reactor that hydrolyzes the first oligosaccharide solution flowing out of the pressurized hydrothermal reactor using a solid acid catalyst to produce a first monosaccharide solution comprising xylose; and a second catalytic reactor that hydrolyzes the second polysaccharide solution flowing out of the pressurized hydrothermal reactor using a solid acid catalyst to produce a second monosaccharide solution comprising glucose.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种处理生物质的装置，提高糖产率，固体酸催化剂的反应速度和分离固体酸催化剂的能力。解决方案：用于处理生物质的装置被配置为包括在用于分解半纤维素的第一反应条件下水解生物质的加压水热反应器，以使用加压的热水产生包含低聚木糖的第一多糖溶液，随后水解生物质在用于分解纤维素的第二反应条件下，使用加压的热水产生包含纤维寡糖的第二多糖溶液; 第一催化反应器，其使用固体酸催化剂水解流出加压水热反应器的第一寡糖溶液以产生包含木糖的第一单糖溶液; 以及第二催化反应器，其使用固体酸催化剂水解流出加压水热反应器的第二多糖溶液以产生包含葡萄糖的第二单糖溶液。版权所有（C）2011，JPO＆INPIT

3. 发明专利

JP2010064941A Carbonaceous material having hetero atom-containing organic group, and method for producing the same 审中-公开
标题翻译：具有异质含有有机基团的碳质材料及其制造方法
公开(公告)号：JP2010064941A
公开(公告)日：2010-03-25
申请号：JP2008234939
申请日：2008-09-12
申请人： Nippon Oil Corp , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 新日本石油株式会社
发明人： HARA YUKIKAZU , NAKAJIMA KIYOTAKA , YANAGAWA SHINICHIRO , KONDO HIDESATO
IPC分类号： C01B31/02
摘要： PROBLEM TO BE SOLVED: To provide a new carbonaceous material obtained by introducing a predetermined group into a carbonaceous material obtained by subjecting organic matter to carbonization treatment, and to provide a method for producing the same.
SOLUTION: The carbonaceous material having a hetero atom-containing organic group is obtained by subjecting organic matter to carbonization treatment to obtain a carbonaceous material, subjecting the carbonaceous material to halogenization treatment to obtain a halogen atom-containing carbonaceous material, and substituting the halogen atoms in the halogen atom-containing carbonaceous material with a hetero atom-containing organic group.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供通过将预定基团引入通过使有机物质进行碳化处理获得的碳质材料中获得的新的碳质材料，并提供其制造方法。解决方案：具有含杂原子的有机基团的碳质材料通过使有机物进行碳化处理获得碳质材料，使碳质材料进行卤化处理以获得含卤原子的碳质材料，并代替具有含杂原子的有机基团的含卤原子的碳质材料中的卤素原子。版权所有（C）2010，JPO＆INPIT

4. 发明专利

JP2009054350A Electrolyte membrane for direct methanol fuel cell, and membrane electrode assembly as well as fuel cell using the same 审中-公开
标题翻译：用于直接甲醇燃料电池的电解质膜，以及作为使用其的燃料电池的膜电极组件
公开(公告)号：JP2009054350A
公开(公告)日：2009-03-12
申请号：JP2007218244
申请日：2007-08-24
申请人： Tokyo Institute Of Technology , Toppan Printing Co Ltd , 凸版印刷株式会社 , 国立大学法人東京工業大学
发明人： YAMAGATA SHINICHIRO , KISHI KATSUYUKI , SHIROMIZU KOHEI , HARA YUKIKAZU
IPC分类号： H01M8/02 , H01B1/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide an electrolyte membrane for a direct methanol fuel cell capable of preventing or restraining elution of solid acid from a binder, restraining swelling of an electrolyte membrane, and alleviating methanol crossover of an anode electrode, and also equipped with substantially high proton conductivity, and to provide a membrane electrode assembly as well as a direct methanol fuel cell using the electrolyte membrane. SOLUTION: The electrolyte membrane with a direct methanol fuel cell putting a composition having at least solid acid and binder under a heating treatment within a given treatment temperature and a given treatment time, and the membrane electrode assembly using the electrolyte membrane as well as the direct methanol fuel cell using the electrolyte membrane are provided. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供能够防止或抑制固体酸从粘合剂中溶出的直接甲醇燃料电池的电解质膜，抑制电解质膜的溶胀，以及减轻阳极电极的甲醇交换，以及其具有基本上高的质子传导性，并且提供膜电极组件以及使用电解质膜的直接甲醇燃料电池。解决方案：具有直接甲醇燃料电池的电解质膜在给定的处理温度和给定的处理时间内将具有至少固态酸和粘合剂的组合物在加热处理下，以及使用电解质膜的膜电极组件因为提供了使用电解质膜的直接甲醇燃料电池。版权所有（C）2009，JPO＆INPIT

5. 发明专利

JP2008287922A Solid acid having water dispersion, its process, and its utilization 审中-公开
标题翻译：具有水分散性的固体酸，其工艺及其利用
公开(公告)号：JP2008287922A
公开(公告)日：2008-11-27
申请号：JP2007129390
申请日：2007-05-15
申请人： Tokyo Institute Of Technology , Toppan Printing Co Ltd , 凸版印刷株式会社 , 国立大学法人東京工業大学
发明人： YAMAGATA SHINICHIRO , KISHI KATSUYUKI , HARA YUKIKAZU
IPC分类号： H01M8/02 , H01B1/06 , H01M8/04 , H01M8/10
CPC分类号： Y02E60/522
摘要： PROBLEM TO BE SOLVED: To provide a solid acid superior in proton conductivity and its process method.
SOLUTION: The solid acid is obtained by heat treatment of polycyclic aromatic hydrocarbons in concentrated sulfuric acid or oleum, and by condensation and sulfonation of the polycyclic aromatic hydrocarbon, and its diffraction peak on carbon (002) face of half width of 5-30° is at least detected in powder X-ray diffraction, and has a prescribed sulfonic acid density and cluster size. The membrane obtained by dispersing in binder resin or the like is excellent in dispersion of solid acid, thereby it is superior in proton conductivity and superior in stability and durability of solid acid in the membrane and can be utilized for an electrolyte membrane for fuel cell, a membrane electrode assembly, and a fuel cell.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供质子传导性优异的固体酸及其加工方法。解决方案：固体酸通过热处理浓硫酸或发烟硫酸中的多环芳烃，并通过多环芳烃的缩合和磺化得到，其半峰宽为5（002）面上的衍射峰为5 至少在粉末X射线衍射中检测到-30°，并具有规定的磺酸密度和簇尺寸。通过分散在粘合剂树脂等中获得的膜在固体酸的分散性方面是优异的，因此其质子传导性优异，膜中固体酸的稳定性和耐久性优异，可用于燃料电池用电解质膜，膜电极组件和燃料电池。版权所有（C）2009，JPO＆INPIT

6. 发明专利

JP2007273970A N-type carbon semiconductor film and semiconductor device using same 审中-公开
标题翻译： N型碳化硅半导体膜和使用相同的半导体器件
公开(公告)号：JP2007273970A
公开(公告)日：2007-10-18
申请号：JP2007056652
申请日：2007-03-07
申请人： Tokyo Institute Of Technology , 国立大学法人東京工業大学
发明人： HARA YUKIKAZU
IPC分类号： H01L51/42 , H01L51/05 , H01L51/30 , H01L51/40
CPC分类号： Y02E10/549 , Y02P70/521
摘要： PROBLEM TO BE SOLVED: To fabricate an n-type carbon semiconductor at a low cost, and to provide a high-performance and large-area semiconductor device and solar cell using it. SOLUTION: The n-type carbon semiconductor film mainly consists of an assembly of a carbon six membered ring. In spectrum by Raman spectroscopy, the integrated intensity ratio, I(D)/I(G) between D band near 1,300 cm -1 and G band near 1,600 cm -1 is 0.3 to 3.0. By X-ray photoelectron spectroscopy, the element ratio (N and/or S)/C is 0.01 to 0.40 between nitrogen or sulfur and carbon. This n-type carbon semiconductor film can be obtained by heat treatment of an organic compound containing nitrogen and/or sulfur at 200°C to 900°C after making it contact on a substrate in liquid phase, or in gaseous phase under atmospheric pressure. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：以低成本制造n型碳半导体，并提供使用它的高性能和大面积的半导体器件和太阳能电池。解决方案：n型碳半导体膜主要由碳六元环的组装构成。在通过拉曼光谱测定的光谱中，在1300cm -1附近的D波段和1600cm -1附近的G波段之间的积分强度比I（D）/ I（G）为0.3〜3.0。通过X射线光电子能谱，氮或硫与碳之间的元素比（N和/或S）/ C为0.01〜0.40。这种n型碳半导体膜可以通过在液相中或在大气压下在气相中接触后在200℃〜900℃下热处理含有氮和/或硫的有机化合物而获得。版权所有（C）2008，JPO＆INPIT

7. 发明专利

JP2012149014A Method for producing ester using carbon solid acid catalyst 审中-公开
标题翻译：使用碳酸固体催化剂生产酯的方法
公开(公告)号：JP2012149014A
公开(公告)日：2012-08-09
申请号：JP2011009741
申请日：2011-01-20
申请人： Dic Corp , Dic株式会社 , Tokyo Institute Of Technology , 国立大学法人東京工業大学
发明人： OKI HIRONOBU , OKA YASUTAKA , HARA YUKIKAZU
IPC分类号： C07C67/08 , B01J27/053 , C07B61/00 , C07C69/54
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for obtaining an ester in a high yield from polyhydric alcohol and carboxylic acid such as (meth)acrylic acid by using a solid acid catalyst which is amorphous carbon introduced with a sulfone group.SOLUTION: In the method for producing an ester, the ester is produced when, in the presence of an esterification solid acid catalyst, an alcohol selected from the group consisting of ethylene glycol, propylene glycol, 1,4-butanediol, trimethylolpropane, pentaerythritol and an ether-group-containing alcohol obtained by a ring-opening reaction between a compound having at least one hydroxy group and a compound having at least one epoxy group is reacted with a carboxylic acid. In the method, the esterification solid acid catalyst is the amorphous carbon to which a sulfone group is introduced.
摘要翻译：待解决的问题：提供一种通过使用引入了砜基的无定形碳的固体酸催化剂从多元醇和羧酸如（甲基）丙烯酸获得高收率的酯的方法。解决方案：在酯的制备方法中，当酯化固体酸催化剂存在下，选自乙二醇，丙二醇，1,4-丁二醇，三羟甲基丙烷季戊四醇和通过具有至少一个羟基的化合物和具有至少一个环氧基的化合物之间的开环反应得到的含醚基的醇与羧酸反应。在该方法中，酯化固体酸催化剂是引入砜基的无定形碳。版权所有（C）2012，JPO＆INPIT

8. 发明专利

JP2009114289A Method for producing fatty acid ester 审中-公开
标题翻译：生产脂肪酸酯的方法
公开(公告)号：JP2009114289A
公开(公告)日：2009-05-28
申请号：JP2007287572
申请日：2007-11-05
申请人： Mitsui Eng & Shipbuild Co Ltd , Tokyo Institute Of Technology , 三井造船株式会社 , 国立大学法人東京工業大学
发明人： TAKAHASHI YOICHI , TSUKUI YUTAKA , MIMACHI HIROKO , IBARAKI SHOICHI , HARA YUKIKAZU
IPC分类号： C11C3/10 , C07B61/00 , C07C67/03 , C07C67/08 , C07C69/24 , C07C69/533 , C07C69/587
摘要： PROBLEM TO BE SOLVED: To provide a method for increasing the production rate of a fatty acid ester in the process of producing a fatty acid ester from fats and oils containing free fatty acids as a source material.
SOLUTION: The method for producing a fatty acid ester comprises allowing fats and oils containing triglyceride and free fatty acids to react with alcohol in the presence of a solid acid catalyst, and is characterized in that: the oils and fats contain free fatty acids by over 0 wt.% and not more than 80 wt.%; the carbon-based solid acid catalyst comprises a carbon-based solid acid obtained by introducing a sulfonic acid group to a carbon material; and transesterification of the triglyceride and esterification of the free fatty acids are simultaneously carried out.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种在含有游离脂肪酸作为源材料的脂肪和油的脂肪酸酯的制造方法中提高脂肪酸酯的生产率的方法。解决方案：脂肪酸酯的制造方法包括使含有甘油三酯和游离脂肪酸的油脂与醇在固体酸催化剂存在下反应，其特征在于：油和脂肪含有游离脂肪超过0重量％且不大于80重量％的酸; 碳基固体酸催化剂包括通过将碳酸酯基引入磺酸基而获得的碳基固体酸; 甘油三酯的酯交换和游离脂肪酸的酯化同时进行。版权所有（C）2009，JPO＆INPIT

9. 发明专利

JP2009114272A Method of manufacturing fatty acid monoesterified product by solid acid catalyst 有权
标题翻译：通过固体酸催化剂制备脂肪酸单体化产品的方法
公开(公告)号：JP2009114272A
公开(公告)日：2009-05-28
申请号：JP2007286875
申请日：2007-11-05
申请人： Asahi Kasei Corp , Tokyo Institute Of Technology , 国立大学法人東京工業大学 , 旭化成株式会社
发明人： YAMASHITA KUNIHIKO , HARA YUKIKAZU
IPC分类号： C11C3/10 , C07B61/00 , C07C67/03 , C07C69/58 , C10L1/02
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing a fatty acid monoesterified product having a low acid value and a low total converted glycerol amount from oils and fats.
SOLUTION: The method of manufacturing a fatty acid monoesterified product includes a first step of causing an animal oil and/or a vegetable oil to react with an alcohol represented by the formula: ROH (wherein R is a 1-24C saturated or unsaturated fatty acid group) in the presence of a sulfonic acid-introduced amorphous carbon catalyst and water at a temperature of 60-200°C and a pressure of the atmospheric pressure to 5 MPa to obtain a fatty acid esterified reaction liquid having a by-produced ratio of a monoglyceride of 0-1.3 mass%. The fatty acid monoesterified product has a low total converted glycerol amount (the percentage, in the fatty acid monoesterified product, of the total of the amount of glycerol contained in the fatty acid monoesterified product and the amount of glycerol constituting all glycerides) and a low acid value and therefore is suitably employable as a fuel for diesel engines.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种从油脂中生产具有低酸值和低总转化甘油量的脂肪酸单酯化产物的方法。解决方案：制造脂肪酸单酯化产物的方法包括使动物油和/或植物油与下式表示的醇反应的第一步：ROH（其中R为1-24℃饱和或不饱和脂肪酸基团）在引入磺酸的无定形碳催化剂和水的存在下，在60-200℃的温度和大气压至5MPa的压力下，获得具有副产物的脂肪酸酯化反应液，单酸甘油酯的产率为0〜0.3质量％。脂肪酸单酯化产物具有低的总转化甘油量（脂肪酸单酯化产物中的脂肪酸单酯化产物中所含的甘油的总量和构成所有甘油酯的甘油的量的百分比）和低酸值，因此适合用作柴油发动机的燃料。版权所有（C）2009，JPO＆INPIT

10. 发明专利

JP2008138118A Fluorinated sulfonic acid group-introduced amorphous carbon-containing composition and method for producing the same composition and use of the same composition 审中-公开
标题翻译：氟化亚磺酸组引入的不含碳的含碳组合物及其制备相同组合物的方法及其组合物的使用
公开(公告)号：JP2008138118A
公开(公告)日：2008-06-19
申请号：JP2006327140
申请日：2006-12-04
申请人： Tokyo Institute Of Technology , Toppan Printing Co Ltd , 凸版印刷株式会社 , 国立大学法人東京工業大学
发明人： HARA YUKIKAZU , KISHI KATSUYUKI , SHIROMIZU KOHEI
IPC分类号： C08L101/00 , B01D71/02 , B01J27/122 , C01B31/02 , C08K5/42 , C08K9/04 , C08L27/22 , H01B1/06 , H01M4/86 , H01M4/88 , H01M8/02
CPC分类号： Y02P70/56
摘要： PROBLEM TO BE SOLVED: To provide a composition having proton conductivity, endurance and film strength and having low production cost and being utilizable for solid acid catalyst-supporting materials, electrolyte membrane, etc., for fuel cells and to provide a production method capable of readily producing such composition at low cost and to provide the use thereof. SOLUTION: The composition comprises an amorphous carbon in which a fluorine atom and a sulfonic acid group are introduced and a binder. It is preferable that an amorphous carbon in which sulfonic acid density is 0.5-14 m mol/g and proton conductivity is 0.01-0.5 S/cm and the sulfur content on the surface is 0.01-0.4, expressed in terms of the elemental ratio (S/C) of sulfur to carbon and fluorine content on the surface is 0.01-0.5, expressed in terms of the elemental ratio (F/C) of fluorine to carbon as the amorphous carbon. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供具有质子传导性，耐久性和膜强度并且具有低生产成本并且可用于燃料电池的固体酸催化剂负载材料，电解质膜等的组合物，并且提供生产能够以低成本容易地制造这种组合物并提供其用途的方法。解决方案：组合物包含其中引入氟原子和磺酸基团的无定形碳和粘合剂。优选磺酸密度为0.5〜14摩尔/克，质子传导率为0.01-0.5S / cm的无定形碳，表面上的硫含量为0.01-0.4，以元素比（ S / C）为0.01-0.5，以氟与碳的无定形碳的元素比（F / C）表示。版权所有（C）2008，JPO＆INPIT

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