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11. 发明授权

US06863708B2 Method for producing metal powder and metal powder, and electroconductive paste and monolithic ceramic capacitor 失效
标题翻译：金属粉末和金属粉末的生产方法，以及导电浆料和叠层陶瓷电容器
公开(公告)号：US06863708B2
公开(公告)日：2005-03-08
申请号：US10343936
申请日：2002-06-11
申请人： Wataru Kagohashi , Mitsugu Yoshida , Tsuyoshi Asai
发明人： Wataru Kagohashi , Mitsugu Yoshida , Tsuyoshi Asai
IPC分类号： B22F9/28 , C22B1/08 , C22B5/12 , C22B23/06 , H01G4/008 , B22F9/26
CPC分类号： C22B23/06 , B22F9/28 , C22B1/08 , C22B5/12 , H01G4/0085 , Y10T29/49165
摘要： Metal chloride vapor and reducing gas are brought into contact to form metallic powder, the metallic powder is washed in carbonic acid aqueous solution, and the metallic powder is classified in a liquid phase. In this way, metallic powder, such as nickel powder, in which the content of chloride components is extremely small and the coarse particle content is small, can be efficiently produced.
摘要翻译：使金属氯化物蒸气和还原气体接触形成金属粉末，金属粉末在碳酸水溶液中洗涤，金属粉末分级为液相。以这种方式，可以有效地制备其中氯化物组分含量极小并且粗颗粒含量小的金属粉末，如镍粉。

12. 发明授权

US06235077B1 Process for production of nickel powder 失效
标题翻译：镍粉生产工艺
公开(公告)号：US06235077B1
公开(公告)日：2001-05-22
申请号：US09381312
申请日：1999-10-12
申请人： Wataru Kagohashi , Tsuyoshi Asai , Hideo Takatori
发明人： Wataru Kagohashi , Tsuyoshi Asai , Hideo Takatori
IPC分类号： B22F928
CPC分类号： B22F9/28 , B22F2998/00 , B22F2999/00 , B22F1/0018 , B22F2201/013 , B22F2201/00
摘要： Chlorine gas from a supply nozzle is mixed with the vapor of nickel chloride and the mixed gas is supplied from a supply nozzle into a hydrogen gas atmosphere in a reduction reactor at a reduction temperature of 900 to 1100° C. The volume of chlorine gas to be mixed versus the vapor of nickel chloride is adjusted to a ratio of 0.01 to 0.5 moles per mole of the vapor of nickel chloride. The particle size of the nickel powder can be controlled appropriately, and also, uniformity of particle size, smoothability of surfaces of particles, and sphericity can be improved.
摘要翻译：来自供给喷嘴的氯气与氯化镍的蒸汽混合，混合气体在还原反应器中在900〜1100℃的还原温度下从供给喷嘴供给氢气气氛。氯气体积与氯化镍的蒸气相混合，调节成每摩尔氯化镍蒸汽为0.01〜0.5摩尔的比例。可以适当地控制镍粉的粒径，并且可以提高粒径的均匀性，颗粒表面的光滑性和球形度。

13. 发明授权

US06372015B1 Method for production of metal powder 失效
标题翻译：金属粉末生产工艺
公开(公告)号：US06372015B1
公开(公告)日：2002-04-16
申请号：US09463563
申请日：2000-01-27
申请人： Tsuyoshi Asai , Hideo Takatori , Wataru Kagohashi
发明人： Tsuyoshi Asai , Hideo Takatori , Wataru Kagohashi
IPC分类号： B22F912
CPC分类号： B22F9/28
摘要： A process for production of metallic powder comprising contacting a metallic chloride gas with a reductive gas in a temperature range for a reducing reaction to form a metallic powder and subsequently contacting the metallic powder with an inert gas such as nitrogen gas to cool the powder, wherein the rate of cooling is 30° C. or more for temperatures from the temperature range for the reducing reaction to a temperature of 800°C. or less. The metallic powder is rapidly cooled, which results in suppression of agglomeration of particles in the metallic powder and the growth of secondary particles. Growth of particles of a metallic powder formed in a reduction process into secondary particles through agglomeration after the reduction process is suppressed, and a ultrafine metallic powder having a particle diameter of, for example, 1&mgr;m or less, can be reliably produced.
摘要翻译：一种金属粉末的制造方法，其特征在于，在还原反应的温度范围内使金属氯化物气体与还原性气体接触，形成金属粉末，随后使金属粉末与氮气等惰性气体接触，使粉末冷却，对于从还原反应的温度范围到800℃的温度的温度，冷却速率为30℃以上。或更少。金属粉末被快速冷却，这导致抑制金属粉末中的颗粒附聚和二次颗粒的生长。在还原处理后，通过还原过程中的附聚将在还原过程中形成的金属粉末的颗粒生长成二次颗粒，并且可以可靠地制造具有例如1μm或更小的粒径的超细金属粉末。

14. 发明申请

US20060162496A1 Method and apparatus for producing metal powder 有权
标题翻译：金属粉末的制造方法和装置
公开(公告)号：US20060162496A1
公开(公告)日：2006-07-27
申请号：US10528372
申请日：2003-09-12
申请人： Tsuyoshi Asai , Takuya Miyagi
发明人： Tsuyoshi Asai , Takuya Miyagi
IPC分类号： B22F9/28
CPC分类号： B22F9/28
摘要： An object of the present invention is to provide a method for production of metallic powder in which aggregation of particles and growth to secondary particle after reducing process of the metallic powder particle can be prevented, to reliably obtain metallic particles containing few coarse particles and to meet requirements of thinner layer and greater number of layers in recent capacitors, and a production device therefor. The present invention includes a reducing process in which metal chloride gas and reducing gas are contacted to continuously reduce the metal chloride, and a cooling process in which a gas containing metallic powder generated in the reducing process is continuously cooled by inert gas. In the cooling process, a vortex flow is generated by blowing out the inert gas from at least one part around the flowing passage of the metallic powder. Furthermore, during the production of the metallic powder, inert gas flow is generated in the vertical direction along the inner wall of the production device (reducing process and cooling process) continuously. Aggregation of the metallic powder and growth of secondary particles can be reduced to reliably obtain metallic powder having uniform particle size containing few coarse particles.
摘要翻译：本发明的目的是提供一种金属粉末的制造方法，其中可以防止金属粉末颗粒的还原过程后的颗粒和生长到二次颗粒的聚集，以可靠地获得含有少量粗颗粒的金属颗粒并满足最近电容器中较薄层和更多层数的要求及其制造装置。本发明包括使金属氯化物气体和还原气体接触以连续地还原金属氯化物的还原过程，并且在还原过程中产生的含有金属粉末的气体通过惰性气体连续冷却的冷却过程。在冷却过程中，通过从金属粉末的流动通道周围的至少一部分吹出惰性气体而产生涡流。此外，在制造金属粉末的过程中，沿着生产装置的内壁（还原过程和冷却过程）在垂直方向上产生惰性气体流。可以减少金属粉末的聚集和二次粒子的生长，以可靠地获得具有少量粗粒子的均匀粒径的金属粉末。

15. 发明授权

US4909677A Throw away cutting tool 失效
标题翻译：丢掉刀具
公开(公告)号：US4909677A
公开(公告)日：1990-03-20
申请号：US195330
申请日：1988-05-18
申请人： Kazuo Noguchi , Nobuhiro Takahashi , Masafumi Hideshima , Tsuyoshi Asai
发明人： Kazuo Noguchi , Nobuhiro Takahashi , Masafumi Hideshima , Tsuyoshi Asai
IPC分类号： B23B27/04
CPC分类号： B23B27/04 , B23B2205/02 , B23B2222/21 , B23B2222/64 , B23B2228/28 , Y10T407/1904 , Y10T407/194 , Y10T407/22 , Y10T407/2288 , Y10T407/25 , Y10T407/27
摘要： A throw away cutting tool comprising a holder formed with a wedge groove and a throw away insert having a cutting edge at one end thereof and a wedge portion at the outer end, the wedge portion being adapted to be clamped in the wedge groove by elasticity of the material of the holder. The holder is at least partly made of cemented carbide for higher rigidity and cutting stability. Also, the radius of curvature at the deep end of the wedge groove is optimized for crack resistance. Further, the angle of the V-ridge on the holder is interrelated to the angle of the V-groove in the insert for more holding stability and crack resistance.

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