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11. 发明授权

US5034015A Process for dyeing keratin fibres with a monohydroxyindole associated with an iodide and hydrogen peroxide 失效
标题翻译：用与碘化物和过氧化氢相关的单羟基吲哚染色角蛋白纤维的方法
公开(公告)号：US5034015A
公开(公告)日：1991-07-23
申请号：US404512
申请日：1989-09-08
申请人： Alex Junino , Gerard Lang , Jean J. Vandenbossche
发明人： Alex Junino , Gerard Lang , Jean J. Vandenbossche
IPC分类号： C07D209/10 , A61K8/00 , A61K8/20 , A61K8/22 , A61K8/34 , A61K8/35 , A61K8/37 , A61K8/39 , A61K8/40 , A61K8/42 , A61K8/49 , A61Q5/10 , C07D209/42
CPC分类号： A61Q5/10 , A61K8/492
摘要： Process for dyeing keratin fibres consisting in applying on these fibres a composition (A) containing at least one indole colorant of formula: ##STR1## where R.sub.1 =H or C.sub.1 -C.sub.4 alkyl;R.sub.2 and R.sub.3, which may be identical or different, denote H, C.sub.1 -C.sub.4 alkyl, carboxyl or alkoxycarbonyl; or a salt or a precursor of a compound (I), associated, either with iodide ions, or with H.sub.2 O.sub.2 ; application of composition (A) being preceded or followed by the application of a compound (B) which contains, either H.sub.2 O.sub.2 at a pH of 2 to 12 when (A) contains iodide ions, or iodide ions at a pH of 2 to 11 when (A) contains H.sub.2 O.sub.2.This process allows particularly powerful and resistant dyes to be made.
摘要翻译：染色包含在这些纤维上施加的组合物（A）的角蛋白纤维的方法包含至少一种下式的吲哚着色剂：其中R 1 = H或C 1 -C 4烷基; R2和R3可以相同或不同，表示H，C1-C4烷基，羧基或烷氧基羰基; 或与碘离子或与H 2 O 2缔合的化合物（I）的盐或前体; 当（A）含有碘离子时，在pH为2〜12的H 2 O 2或pH为2〜11的碘离子的情况下，应用组合物（A）的施用或化合物（B）（A）含有H 2 O 2。该方法可以制造出特别强大和有效的染料。

12. 发明授权

US5536865A Process for the preparation of 5,6-dihydroxyindole and intermediate compounds 失效
公开(公告)号：US5536865A
公开(公告)日：1996-07-16
申请号：US465513
申请日：1995-06-05
申请人： Alex Junino , Jean J. Vandenbossche , Gerard Lang
发明人： Alex Junino , Jean J. Vandenbossche , Gerard Lang
IPC分类号： A61K8/49 , A61Q5/10 , B01J23/44 , B01J23/46 , C07B61/00 , C07C67/00 , C07C253/00 , C07C253/30 , C07C255/35 , C07C255/36 , C07C255/37 , C07C255/43 , C07D209/08 , D06P3/08 , C07C255/33
CPC分类号： C07C255/43 , A61K8/492 , A61Q5/10 , C07D209/08 , D06P3/08 , Y10T428/1476
摘要： Process for the preparation of 5,6-dihydroxyindole, wherein the compound of formula: ##STR1## in which R' denotes a hydrogen atom or an optionally substituted benzyl radical, is subjected either to the action of hydrogen under pressure or to a hydrogen transfer operation, in a solvent medium and in the presence of a hydrogenation catalyst.

13. 发明授权

US5364414A Tinctorial composition for keratinous fibres containing oxidation dye precursors and aminoindole couplers, methods for dyeing using these compositions and new compounds 失效
标题翻译：含有氧化染料前体和氨基吲哚成色剂的角质纤维的着色组合物，使用这些组合物染色的方法和新化合物
公开(公告)号：US5364414A
公开(公告)日：1994-11-15
申请号：US916706
申请日：1992-07-22
申请人： Gerard Lang , Alex Junino , Jean Cotteret , Jean J. Vandenbossche
发明人： Gerard Lang , Alex Junino , Jean Cotteret , Jean J. Vandenbossche
IPC分类号： C07D209/08 , A61K8/00 , A61K8/34 , A61K8/41 , A61K8/49 , A61Q5/10 , C07D209/42 , A61K7/13
CPC分类号： A61Q5/10 , A61K8/492
摘要： Oxidation tinctorial composition intended to be used for dyeing keratinous fibres, in particular human keratinous fibres and especially hair, characterized in that it contains, in a solvent medium appropriate for dyeing these fibres, at least one para oxidation dye precursor or at least one ortho oxidation dye precursor and at least one heterocyclic coupler corresponding to the formula (I): ##STR1## in which: R.sub.1 and R.sub.3, which may be identical or different, denote a hydrogen atom or a C.sub.1 -C.sub.4 alkyl group;R.sub.2 denotes a hydrogen atom, a C.sub.1 -C.sub.4 alkyl group, a carboxyl group or an alkoxycarbonyl group; at least one of the radicals R.sub.2 or R.sub.3 denotes hydrogen;R.sub.4 denotes a hydrogen atom or a C.sub.1 -C.sub.4 alkyl or C.sub.1 -C.sub.4 hydroxyalkyl or C.sub.2 -C.sub.4 polyhydroxyalkyl group;the group NHR.sub.4 occupying the positions 4, 6 or 7 of the benzene ring, as well as their salts.
摘要翻译：用于染色角质纤维，特别是人角质纤维，特别是毛发的氧化着色组合物，其特征在于，其在适于染色这些纤维的溶剂介质中含有至少一种对氧化染料前体或至少一种邻位氧化染料前体和对应于式（I）的至少一种杂环成色剂：其中：R 1和R 3可以相同或不同，表示氢原子或C 1 -C 4烷基; R2表示氢原子，C1-C4烷基，羧基或烷氧基羰基; 基团R2或R3中的至少一个表示氢; R4表示氢原子或C1-C4烷基或C1-C4羟烷基或C2-C4多羟基烷基; 占据苯环位置4,6或7的NHR4基团以及它们的盐。

14. 发明授权

US5354870A Indole derivatives for dyeing keratin materials 失效
标题翻译：用于染色角蛋白材料的吲哚衍生物
公开(公告)号：US5354870A
公开(公告)日：1994-10-11
申请号：US864410
申请日：1992-04-06
申请人： Gerard Lang , Serge Forestier , Alex Junino , Herve Richard , Jean J. Vandenbossche
发明人： Gerard Lang , Serge Forestier , Alex Junino , Herve Richard , Jean J. Vandenbossche
IPC分类号： A61K8/49 , A61Q5/10 , C07D209/08
CPC分类号： A61K8/492 , A61Q5/10 , C07D209/08
摘要： The invention concerns 4-hydroxy-5-methoxyindole and 5-ethoxy-4-hydroxy-2-methylindole which are useful as dyes for dyeing keratin materials.
摘要翻译：本发明涉及可用作染色角蛋白材料的染料的4-羟基-5-甲氧基吲哚和5-乙氧基-4-羟基-2-甲基吲哚。

15. 发明授权

US5609649A Tinctorial composition for keratinous fibers containing oxidation dye precursors and couplers derived from 4-hydroxyindole, and dyeing method using them 失效
标题翻译：含有氧化染料前体和衍生自4-羟基吲哚的成色剂的角质纤维的着色组合物和使用它们的染色方法
公开(公告)号：US5609649A
公开(公告)日：1997-03-11
申请号：US262444
申请日：1994-06-20
申请人： Alex Junino , Jean J. Vandenbossche , Herve Richard , Jean Cotteret
发明人： Alex Junino , Jean J. Vandenbossche , Herve Richard , Jean Cotteret
IPC分类号： A61K8/00 , A61K8/33 , A61K8/35 , A61K8/40 , A61K8/41 , A61K8/49 , A61Q5/10 , A61K7/13
CPC分类号： A61Q5/10 , A61K8/492
摘要： Tinctorial composition for keratinous fibers, in particular for human hair, characterized in that it contains, in a medium appropriate for dyeing these fibers, at least one para oxidation dye precursor or at least one ortho oxidation dye precursor in combination with at least one heterocyclic coupler, corresponding to the formula: ##STR1## in which R.sub.1 denotes a hydrogen atom or a C.sub.1 -C.sub.4 alkyl radical; R.sub.2 denotes a hydrogen atom, a C.sub.1 -C.sub.4 lower alkyl radical, a carboxyl radical or an alkoxycarbonyl radical; R.sub.3 denotes a hydrogen or halogen atom, a C.sub.1 -C.sub.4 lower alkyl radical, a carboxyl radical, an alkoxycarbonyl radical or a formyl radical; X denotes a hydrogen atom, a C.sub.1 -C.sub.4 alkyl radical, a halogen atom, a C.sub.1 -C.sub.4 alkoxy radical, an acetylamino group or a dialkyl(C.sub.1 -C.sub.4)aminomethyl group; at least one of the groups X, R.sub.1, R.sub.2 and R.sub.3 differing from hydrogen; as well as their salts.
摘要翻译：用于角质纤维，特别是人类头发的着色组合物，其特征在于，在适于对这些纤维进行染色的介质中含有至少一种对氧化染料前体或至少一种邻位氧化染料前体与至少一种杂环成色剂对应于下式：其中R 1表示氢原子或C 1 -C 4烷基; R2表示氢原子，C1-C4低级烷基，羧基或烷氧基羰基; R3表示氢或卤素原子，C1-C4低级烷基，羧基，烷氧基羰基或甲酰基; X表示氢原子，C1-C4烷基，卤素原子，C1-C4烷氧基，乙酰氨基或二烷基（C1-C4）氨基甲基; X，R1，R2和R3中的至少一个不同于氢; 以及它们的盐。

16. 发明授权

US5202487A 2-substituted para-aminophenols and their use for dyeing keratinous fibres 失效
标题翻译： 2-取代对氨基苯酚及其用于染色角质纤维的用途
公开(公告)号：US5202487A
公开(公告)日：1993-04-13
申请号：US933583
申请日：1992-08-24
申请人： Alex Junino , Gerard Lang , Alain Genet
发明人： Alex Junino , Gerard Lang , Alain Genet
IPC分类号： C07C217/76 , C07C323/29
CPC分类号： A61K8/415 , A61Q5/10 , C07C217/76 , C07C323/29
摘要： 2-Substituted para-aminophenols of general formula: ##STR1## where Y denotes oxygen or sulphur and R denotes a C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 hydroxyalkyl or C.sub.1 -C.sub.6 haloalkyl or a C.sub.2 -C.sub.6 polyhydroxyalkyl, provided that when Y=O, R is not methyl or ethyl and when Y=S, R is not ethyl; anddye composition containing one or more compounds of formula (I) where Y denotes an oxygen or sulphur atom and R is C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 hydroxyalkyl, C.sub.1 -C.sub.6 haloalkyl or C.sub.2 -C.sub.6 polyhydroxyalkyl.
摘要翻译： 2-取代的具有下式的对氨基苯酚：其中Y表示氧或硫，R表示C 1 -C 6烷基，C 1 -C 6羟基烷基或C 1 -C 6卤代烷基或C 2 -C 6多羟基烷基， Y = O，R不是甲基或乙基，当Y = S时，R不是乙基; 和含有一种或多种式（I）的化合物的染料组合物，其中Y表示氧或硫原子，R是C 1 -C 6烷基，C 1 -C 6羟基烷基，C 1 -C 6卤代烷基或C 2 -C 6多羟基烷基。

17. 发明授权

US5145483A Substituted ortho-aminophenols, process for preparing them and their use for the oxidatin dyeing of keratinous fibres 失效
标题翻译：取代的羟基苯丙胺，其制备方法及其用于氧化皮肤染色剂的研究
公开(公告)号：US5145483A
公开(公告)日：1992-09-08
申请号：US427474
申请日：1989-10-27
申请人： Alex Junino , Herve Andrean , Gerard Lang
发明人： Alex Junino , Herve Andrean , Gerard Lang
IPC分类号： A61K8/00 , A61K8/22 , A61K8/33 , A61K8/35 , A61K8/40 , A61K8/41 , A61K8/42 , A61K8/49 , A61Q5/10 , C07C231/12 , C07C233/43 , C07C233/44 , C07C271/28 , C07C271/58 , C09B53/00 , D06P3/08
CPC分类号： A61K8/42 , A61Q5/10 , C07C233/43 , C07C233/44 , C07C271/28
摘要： 5-Substituted ortho-aminophenols of formula: ##STR1## in which: R.sub.1 denotes a hydrogen atom, an alkyl radical having 1 to 4 carbon atoms or a hydroxyalkyl radical having 1 to 4 carbon atoms; andR.sub.2 denotes, independently of R.sub.1, an alkyl radical having 1 to 4 carbon atoms, an alkoxy radical having 1 to 4 carbon atoms or a benzyl radical;the addition salts with an acid and the phenates, anddyeing composition containing a compound of formula (I) or a salt or a phenate of such a compound.The 5-substituted ortho-aminophenols enable hair to be dyed in a rich spectrum of hues having good durability.
摘要翻译： 5-取代的下式：其中：R 1表示氢原子，具有1至4个碳原子的烷基或具有1至4个碳原子的羟烷基; 并且R 2表示与R 1独立地为具有1至4个碳原子的烷基，具有1至4个碳原子的烷氧基或苄基; 与酸和酚盐的加成盐，以及含有式（I）化合物或这种化合物的盐或酚盐的染色组合物。 5-取代的邻氨基苯酚使毛发能够在具有良好耐久性的色调丰富的色调中染色。

18. 发明授权

US5053052A 2-substituted para-aminophenols and their use for dyeing keratinous fibres 失效
标题翻译： 2-取代的对氨基苯酚及其用于染色卡介苗的用途
公开(公告)号：US5053052A
公开(公告)日：1991-10-01
申请号：US633190
申请日：1990-12-28
申请人： Alex Junino , Gerard Lang , Alain Genet
发明人： Alex Junino , Gerard Lang , Alain Genet
IPC分类号： A61K8/00 , A61K8/33 , A61K8/35 , A61K8/40 , A61K8/41 , A61K8/42 , A61K8/46 , A61K8/49 , A61Q5/10 , C07C217/76 , C07C217/84 , C07C321/06 , C07C323/29 , C09B53/00 , C09B57/00 , C09B67/42 , D06P3/08
CPC分类号： A61K8/415 , A61Q5/10 , C07C217/76 , C07C323/29
摘要： 2-Substituted para-aminophenols of general formula: ##STR1## where Y denotes oxygen or sulphur and R denotes a C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 hydroxyalkyl or C.sub.1 -C.sub.6 haloalkyl or a C.sub.2 -C.sub.6 polyhydroxyalkyl, provided that when Y=O, R is not methyl or ethyl and when Y=S, R is not ethyl; and dye composition containing one or more compounds of formula (I) where Y denotes an oxygen or sulphur atom and R is C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 hydroxyalkyl, C.sub.1 -C.sub.6 haloalkyl or C.sub.2 -C.sub.6 polyhydroxyalkyl.
摘要翻译： 2-取代的具有下式的对氨基苯酚：其中Y表示氧或硫，R表示C 1 -C 6烷基，C 1 -C 6羟基烷基或C 1 -C 6卤代烷基或C 2 -C 6多羟基烷基， Y = O，R不是甲基或乙基，当Y = S时，R不是乙基; 和含有一种或多种式（I）的化合物的染料组合物，其中Y表示氧或硫原子，R是C 1 -C 6烷基，C 1 -C 6羟基烷基，C 1 -C 6卤代烷基或C 2 -C 6多羟基烷基。

19. 发明授权

US4979961A p-phenylenediamines, process for preparation thereof, dyeing composition containing them and corresponding dyeing process 失效
标题翻译：对苯二胺，其制备方法，含有它们的染色组合物和相应的染色方法
公开(公告)号：US4979961A
公开(公告)日：1990-12-25
申请号：US342578
申请日：1989-04-24
申请人： Alex Junino , Alain Genet , Gerard Lang
发明人： Alex Junino , Alain Genet , Gerard Lang
IPC分类号： A61K8/00 , A61K8/33 , A61K8/40 , A61K8/41 , A61K8/42 , A61K8/46 , A61K8/49 , A61Q5/10 , C07C319/20 , C07C323/25 , C09B53/00 , D06P3/08
CPC分类号： A61Q5/10 , A61K8/411 , C07C323/25
摘要： The invention relates to p-phenylenediamines of formula: ##STR1## in which R.sub.1 denotes an alkyl, hydroxyalkyl or polyhydroxyalkyl radical and R.sub.2 denotes a hydrogen atom or an alkyl radical, as well as the corresponding salts with acids, and to the compositions and the process for dyeing keratinous fibers, especially hair, employing them.
摘要翻译：本发明涉及下式的对苯二胺：其中R 1表示烷基，羟烷基或多羟基烷基，R 2表示氢原子或烷基，以及与酸的相应盐，组合物和用于染色角质纤维，特别是头发的方法。

20. 发明授权

US4888445A New 2,4-dinitro- or 2-amino-4-nitro- or 2-nitro-4-amino-6-hydroxyalkylanilines, the process for preparation thereof and their use in dyeing keratinous fibres, and especially human hair 失效
标题翻译：新的2,4-二硝基或2-氨基-4-硝基 - 或2-硝基-4-氨基-6-羟基烷基苯胺，其制备方法及其在染色角质纤维，特别是人类头发中的用途
公开(公告)号：US4888445A
公开(公告)日：1989-12-19
申请号：US119083
申请日：1987-11-10
申请人： Alex Junino , Gerard Lang , Nicole Jehanno
发明人： Alex Junino , Gerard Lang , Nicole Jehanno
IPC分类号： A61K8/41 , A61Q5/06 , A61Q5/10 , C07C215/68 , C09B51/00
CPC分类号： A61K8/418 , A61Q5/065 , A61Q5/10
摘要： The invention relates to a compound of formula ##STR1## in which: X denotes a branched or unbranched alkylene radical containing 2 to 6 carbon atoms, optionally being able to be substituted with one or more hydroxyl radicals;R denotes a hydrogen atom, an alkyl or a mono- or polyhydroxyalkyl radical or an aminoalkyl radical in which the amine group can be mono- or disubstituted with an alkyl radical or with a mono- or polyhydroxyalkyl radical, the nitrogen atom also being able to form part of a heterocyclic system and the alkyl radicals containing 1 to 4 carbon atoms;R' denotes a hydrogen atom or a C.sub.1 to C.sub.4 alkyl radical;Y and Z denote a nitro and/or --NHR.sub.1 radical, R.sub.1 and R, which may be identical or different, having the meanings given above for R, with the proviso that when Y and Z are identical, they necessarily denote nitro radicals,and the cosmetically acceptable salts of the compounds containing a salifiable amine group, and also the process for preparing it and its use in dyeing keratinous fibres, and especially human hair.
摘要翻译：本发明涉及式（I）的化合物，其中：X表示含有2至6个碳原子的支链或非支链亚烷基，任选地可被一个或多个羟基取代; R表示氢原子，烷基或单羟基或多羟基烷基或氨基烷基，其中胺基可以被烷基或与单羟基或多羟基烷基单体或二取代，氮原子也可以形成杂环体系的一部分和含有1至4个碳原子的烷基; R'表示氢原子或C1〜C4烷基; Y和Z表示硝基和/或-NHR 1基团，R 1和R可以相同或不同，具有上面对R给出的含义，条件是当Y和Z相同时，它们必须表示硝基，并且含有可成胺基团的化合物的化妆品可接受的盐，以及其制备方法及其在染色角质纤维，特别是人类头发中的用途。

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