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    • 11. 发明申请
    • Organic-Solvent Dispersion of Fine Polysilsesquioxane Particle, Process for Producing the Same, Aqueous Dispersion Polysilsesquioxane Particle, and Process
    • 细聚倍半硅氧烷颗粒的有机溶剂分散体,其制备方法,水分散体倍半硅氧烷颗粒和方法
    • US20080004359A1
    • 2008-01-03
    • US11794177
    • 2005-12-27
    • Chenghuan MaMasamichi YamamotoFumio Oi
    • Chenghuan MaMasamichi YamamotoFumio Oi
    • C08J3/09
    • C08J3/09C08J2383/04
    • An organic-solvent dispersion containing fine polysilsesquioxane particles stably dispersed therein, which is obtained by adjusting the pH of an aqueous dispersion of fine polysilsesquioxane particles to 2 to 9, subsequently adding an organic solvent thereto, and then removing the water from the system; and an aqueous dispersion of fine polysilsesquioxane particles having an appropriate average particle diameter, which is obtained by adjusting the amount of a base catalyst to be used so as to be in a specific range. The process for producing an aqueous dispersion of fine polysilsesquioxane particles having a pH of 2 to 9 with an organic solvent. The process for producing an aqueous dispersion of fine polysilsesquioxane particles having an average particle diameter of 1 to 40 nm comprises mixing a dispersion stabilizer, a base catalyst, and trialkoxysilane in the presence of an aqueous solvent to produce an aqueous dispersion of fine polysilsesquioxane particles, and is characterized in that the base catalyst is used in an amount of 4 to 45 mmol/L per total amount of the aqueous solvent.
    • 通过将细聚倍半硅氧烷颗粒的水性分散体的pH调节至2〜9,然后向其中加入有机溶剂,然后从体系中除去水而获得的包含稳定分散在其中的细聚倍半硅氧烷颗粒的有机溶剂分散体。 以及通过将所使用的碱催化剂的量调整到特定范围而得到的具有适当的平均粒径的细聚倍半硅氧烷颗粒的水分散体。 用有机溶剂制备pH为2〜9的细聚倍半硅氧烷颗粒的水分散体的方法。 制备平均粒径为1〜40nm的细聚倍半硅氧烷颗粒的水性分散体的方法包括在水性溶剂的存在下混合分散稳定剂,碱催化剂和三烷氧基硅烷,以制备细聚倍半硅氧烷颗粒的水性分散体, 其特征在于,所述碱催化剂的用量为每水溶剂总量为4〜45mmol / L。
    • 18. 发明授权
    • Anisotropic conductive film
    • 各向异性导电膜
    • US08133412B2
    • 2012-03-13
    • US12918731
    • 2009-09-18
    • Masamichi YamamotoYasuhiro Okuda
    • Masamichi YamamotoYasuhiro Okuda
    • H01B1/00B32B7/12C08L29/04
    • H05K3/323C08G2650/56C08L29/14C08L71/00C09J163/00H01B1/22H05K3/361Y10T428/2857C08L2666/04
    • An anisotropic conductive film 2 contains electrically conductive particles 6 dispersed in an adhesive agent 30 for electrode connection, the adhesive agent containing an epoxy resin, which is an insulating thermosetting resin, as a main component, a phenoxy resin having a molecular weight of 30,000 or more, a latent hardener, a polyvinyl butyral resin having a glass-transition temperature of 100° C. or higher, and a polyvinyl butyral resin having a glass-transition temperature of 90° C. or lower. There is provided the high-heat-resistant anisotropic conductive film which suppresses a reduction in repairability and which can be used for electrodes having a finer pitch, i.e., having a minimum pitch of 150 μm or less, when electrodes are connected with the anisotropic conductive film.
    • 各向异性导电膜2包含分散在用于电极连接的粘合剂30中的导电颗粒6,包含作为主要成分的绝缘热固性树脂的环氧树脂的粘合剂,分子量为30,000的苯氧基树脂或 更具体地说,可以使用玻璃化转变温度为100℃以上的潜在硬化剂,聚乙烯醇缩丁醛树脂和玻璃化转变温度为90℃以下的聚乙烯醇缩丁醛树脂。 提供了抑制可修复性降低的高耐热各向异性导电膜,并且当电极与各向异性导电体连接时,可以用于具有更细间距的电极,即具有150μm或更小的最小间距的电极 电影。