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    • 5. 发明授权
    • Organic-solvent dispersion of fine polysilsesquioxane particle, process for producing the same, aqueous dispersion of fine polysilsesquioxane particle, and process for producing the same
    • 精细倍半硅氧烷颗粒的有机溶剂分散体,其制造方法,精细倍半硅氧烷颗粒的水分散体及其制造方法
    • US08088863B2
    • 2012-01-03
    • US11794177
    • 2005-12-27
    • Chenghuan MaMasamichi YamamotoFumio Oi
    • Chenghuan MaMasamichi YamamotoFumio Oi
    • C08G77/06
    • C08J3/09C08J2383/04
    • An organic-solvent dispersion containing fine polysilsesquioxane particles stably dispersed therein, which is obtained by adjusting the pH of an aqueous dispersion of fine polysilsesquioxane particles to 2 to 9, subsequently adding an organic solvent thereto, and then removing the water from the system; and an aqueous dispersion of fine polysilsesquioxane particles having an appropriate average particle diameter, which is obtained by adjusting the amount of a base catalyst to be used so as to be in a specific range. The process for producing an aqueous dispersion of fine polysilsesquioxane particles having a pH of 2 to 9 with an organic solvent. The process for producing an aqueous dispersion of fine polysilsesquioxane particles having an average particle diameter of 1 to 40 nm comprises mixing a dispersion stabilizer, a base catalyst, and trialkoxysilane in the presence of an aqueous solvent to produce an aqueous dispersion of fine polysilsesquioxane particles, and is characterized in that the base catalyst is used in an amount of 4 to 45 mmol/L per total amount of the aqueous solvent.
    • 通过将细聚倍半硅氧烷颗粒的水性分散体的pH调节至2〜9,然后向其中加入有机溶剂,然后从体系中除去水而获得的包含稳定分散在其中的细聚倍半硅氧烷颗粒的有机溶剂分散体。 以及通过将所使用的碱催化剂的量调整到特定范围而得到的具有适当的平均粒径的细聚倍半硅氧烷颗粒的水分散体。 用有机溶剂制备pH为2〜9的细聚倍半硅氧烷颗粒的水分散体的方法。 制备平均粒径为1〜40nm的细聚倍半硅氧烷颗粒的水性分散体的方法包括在水性溶剂的存在下混合分散稳定剂,碱催化剂和三烷氧基硅烷,以制备细聚倍半硅氧烷颗粒的水性分散体, 其特征在于,所述碱催化剂的用量为每水溶剂总量为4〜45mmol / L。
    • 7. 发明授权
    • Circuit connecting adhesive
    • 电路连接胶
    • US07588698B2
    • 2009-09-15
    • US11578334
    • 2005-12-02
    • Hideaki ToshiokaMasamichi YamamotoKazuhiro Kawabata
    • Hideaki ToshiokaMasamichi YamamotoKazuhiro Kawabata
    • H01B1/00H01B1/04H01B1/06H01B1/02H01B1/22
    • C09J163/00C09J9/02H01B1/22H01B1/24H01R4/04
    • A circuit coupling adhesive which is superior in heat resistance and moisture resistance is provided. The circuit coupling adhesive of the present invention can be used for purposes where high performing reliability is required, since it exhibits satisfactory electroconductive/insulative performance at connection of electrodes, etc. and the characteristics will not be varied so much even after a long period of use in a high temperature and high humidity environment. The circuit coupling adhesive comprises, as the essential ingredients, an epoxy resin, a latent curing agent, inorganic fillers having an average particle diameter of 500 nm or less, and electro-conductive particles. By mix a sufficient amount of inorganic fillers having an average particle diameter of 500 nm or less, the coefficient of thermal expansion can be decreased and the heat resistance and moisture resistance can be improved.
    • 提供了耐热性和耐湿性优异的电路耦合粘合剂。 本发明的电路耦合粘合剂可以用于需要高性能可靠性的目的,因为它在电极连接时表现出令人满意的导电/绝缘性能,并且特性即使在长时间 在高温高湿环境下使用。 电路耦合粘合剂包括环氧树脂,潜伏性固化剂,平均粒径为500nm以下的无机填料和导电性颗粒作为必要成分。 通过混合足量的平均粒径为500nm以下的无机填料,能够降低热膨胀系数,提高耐热性和耐湿性。