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111. 发明授权

US07566480B2 Fluorochemical composition for treating porous stone 失效
标题翻译：用于处理多孔石的含氟化合物
公开(公告)号：US07566480B2
公开(公告)日：2009-07-28
申请号：US11192940
申请日：2005-07-29
申请人： Rudolf J. Dams
发明人： Rudolf J. Dams
IPC分类号： B05D3/02
CPC分类号： C04B41/4842 , C04B41/009 , C04B41/83 , C04B41/4922 , C04B41/49 , C04B33/00
摘要： The present invention relates to a method of treating porous stone, comprising contacting porous stone with a composition comprising: (i) a fluorinated oligomer having a weight average molecular weight of not more than 70,000 g/mol and comprising repeating units derived from one or more hydrocarbon monomers and one or more fluorinated monomers represented by the formula: Rf—Xt-E1 wherein Rf represents a perfluorinated aliphatic group having 3 or 4 carbon atoms, X represents a non-fluorinated organic linking group, t is 0 or 1 and E1 represents an ethylenically unsaturated group; and wherein the amount of repeating units derived from said fluorinated monomers is more than 50 mole % of the total amount of repeating units; (ii) a liquid dispersing or dissolving said fluorinated oligomer, said liquid comprising an organic solvent in an amount of at least 70% by weight based on the total amount of liquid; and wherein said fluorinated oligomer is contained in said composition in an amount of 1 to 20% by weight based on the total weight of the composition.
摘要翻译：本发明涉及一种处理多孔石的方法，包括使多孔石与以下组合物接触的组合物：（i）重均分子量不超过70,000g / mol的氟化低聚物，并且包含衍生自一种或多种烃单体和一种或多种由下式表示的氟化单体：<？in-line-formula description =“In-line formula”end =“lead”？> Rf-Xt-E1 <？in-line-formula description =“ 其中Rf表示具有3或4个碳原子的全氟化脂族基团，X表示非氟化有机连接基团，t表示0或1，E1表示烯属不饱和基团; 并且其中衍生自所述氟化单体的重复单元的量大于重复单元总量的50摩尔％（ii）分散或溶解所述氟化低聚物的液体，所述液体包含基于液体总量至少70重量％的有机溶剂; 并且其中所述氟化低聚物以所述组合物的总重量计含有1至20重量％的所述组合物。

112. 发明申请

US20090149616A1 FLUORINATED SURFACTANTS 审中-公开
标题翻译：氟化表面活性剂
公开(公告)号：US20090149616A1
公开(公告)日：2009-06-11
申请号：US12095205
申请日：2006-11-22
申请人： Frans A. Audenaert , Rudolf J. Dams
发明人： Frans A. Audenaert , Rudolf J. Dams
IPC分类号： C08F14/18
CPC分类号： C08F214/18 , C08F290/062 , C08J3/03 , C08J2351/08
摘要： The present invention provides a fluorinated surfactant comprising fluorinated units and hydrophilic non-fluorinated units wherein said fluorinated surfactant can be obtained by(i) a free radical polymerization of: (a) one or more fluorinated monomers having the general formula (I): (Rf)n—X—C(R1)═CH2 (I) wherein Rf represents a perfluorinated polyether group, X represents a bond or a linking group, R1 represents a hydrogen atom or an alkyl group of 1 to 4 carbon atoms, and n is 1 or 2; and (b) at least one non-fluorinated monomer having at least one hydrophilic group or a precursor thereof; and (ii) conversion of said precursor when present, into a corresponding hydrophilic group.
摘要翻译：本发明提供含氟单体和亲水性非氟化单元的含氟表面活性剂，其中所述氟化表面活性剂可以通过以下方法获得：（i）自由基聚合：（a）一种或多种具有通式（I）的氟化单体：（在线公式）end =“lead”？>（Rf）nXC（R1）-CH2（I）<？in-line-formula description =“In-line Formulas”end = “尾”→其中Rf表示全氟化聚醚基团，X表示键或连接基团，R 1表示氢原子或碳原子数1〜4的烷基，n为1或2; 和（b）至少一种具有至少一个亲水基团的非氟化单体或其前体; 和（ii）当存在时所述前体的转化成相应的亲水基团。

113. 发明申请

US20080008891A1 COMPOSITIONS CONTAINING SILANES 失效
标题翻译：含硅烷的组合物
公开(公告)号：US20080008891A1
公开(公告)日：2008-01-10
申请号：US11466620
申请日：2006-08-23
申请人： Rudolf J. Dams , George G.I. Moore
发明人： Rudolf J. Dams , George G.I. Moore
IPC分类号： B32B13/04 , C07F7/10
CPC分类号： C09D4/00 , C07F7/1804
摘要： Perfluoro lower alkanesulfonamide-derived silanes which in an organic solvent are useful in treating siliceous substrates are described. The compositions may optionally contain an additional non-fluorinated compound in a mixture or condensation product. Methods for preparing perfluoro lower alkanesulfonamide-derived silanes are also described.
摘要翻译：描述了在有机溶剂中可用于处理硅质底物的全氟低级链烷磺酰胺衍生的硅烷。组合物可任选地在混合物或缩合产物中含有另外的非氟化化合物。还描述了制备全氟低级链烷磺酰胺衍生的硅烷的方法。

114. 发明授权

US07166329B2 Method of rendering substrates oil and water repellent with a fluorochemical oligomeric silane 失效
标题翻译：用含氟低聚硅烷生产底漆油和防水剂的方法
公开(公告)号：US07166329B2
公开(公告)日：2007-01-23
申请号：US10053396
申请日：2002-01-17
申请人： Rudolf J. Dams
发明人： Rudolf J. Dams
IPC分类号： B05D3/10 , B32B27/28 , C08L27/12
CPC分类号： C04B41/4842 , C04B41/009 , C04B41/83 , C08F8/42 , C08F220/22 , C08F220/38 , C08F230/08 , C08F2220/387 , C09D4/00 , C09D133/16 , C04B41/463 , C04B33/00 , C08G77/24 , C08F2220/1891 , C08F2220/1825
摘要： A fluorochemical composition comprising of organic solvent and fluorochemical oligomer represented by the general formula: X-MfnMhmMar-G wherein X represents the residue of an initiator or hydrogen; Mf represents units derived from fluorinated monomers; Mh represents units derived from a non-fluorinated monomers; Ma represents units having a silyl group represented by the formula: wherein each of Y4, Y5 and Y6 independently represents an alkyl group, an aryl group or a hydrolyzable group; G is a monovalent organic group comprising the residue of a chain transfer agent; n represents a value of 1 to 100; m represents a value of 0 to 100; r represents a value of 0 to 100; and n+m+r is at least 2.
摘要翻译：由有机溶剂和由以下通式表示的含氟低聚物组成的含氟化合物组合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> XM n = r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r = = = = = = = = = = = = = = = = “In-line Formulas”end =“tail”？>其中X表示引发剂或氢的残基; M代表来自氟化单体的单元; M h表示源自非氟化单体的单元; 表示具有由下式表示的甲硅烷基的单元：其中Y 4，Y 5和Y 6各自表示， SUP>独立地表示烷基，芳基或可水解基团; G是包含链转移剂残基的一价有机基团; n表示1〜100的数值。 m表示0〜100的值。 r表示0〜100的值。 n + m + r为2以上。

115. 发明授权

US06716534B2 Coating composition comprising a fluorochemical polyether silane partial condensate and use thereof 失效
公开(公告)号：US06716534B2
公开(公告)日：2004-04-06
申请号：US10007556
申请日：2001-11-08
申请人： George G. I. Moore , Rudolf J. Dams , Franceska M. Fieuws , Guido P. Piessens
发明人： George G. I. Moore , Rudolf J. Dams , Franceska M. Fieuws , Guido P. Piessens
IPC分类号： B32B2520
CPC分类号： C09D183/12 , C08G65/007 , C08G65/336 , C09D183/08 , Y10S528/901 , Y10T428/31663 , C08L83/00
摘要： A composition comprising a least one fluorochemical polyether silane compound having a polyfluoropolyether segment and at least two hydrolysable silane groups per molecule, one or more non-fluorinated compounds having at least two hydrolysable groups per molecule, and/or a partial condensate thereof, is disclosed. The composition provides durable water, oil and stain repellency to a substrate.

116. 发明授权

US06592659B1 Compositions for aqueous delivery of fluorinated silanes 失效
标题翻译：氟化硅烷水性输送组合物
公开(公告)号：US06592659B1
公开(公告)日：2003-07-15
申请号：US10002543
申请日：2001-11-15
申请人： Michael S. Terrazas , Mark J. Pellerite , Rudolf J. Dams
发明人： Michael S. Terrazas , Mark J. Pellerite , Rudolf J. Dams
IPC分类号： C09D18308
CPC分类号： C08G65/336 , C08G65/007 , C09D4/00 , Y10T428/3154 , Y10T428/31663 , C08G77/00
摘要： The invention relates to a dilutable, non-aqueous concentrate and an aqueous dilution used for aqueous delivery of fluorinated silanes to a substrate, a method of treating a substrate with the aqueous dilution composition to render it oil and water repellent, and articles having coatings made from the aqueous dilution.
摘要翻译：本发明涉及一种可稀释的非水浓缩物和用于将氟化硅烷水性递送至基材的水性稀释液，用水稀释组合物处理底物以使其具有防水和防水性的方法，以及制备具有涂层的制品从水稀释液中。

117. 发明授权

US06440321B1 Mixed fluorochemical hydrocarbon condensates to impart oil and water repellency to a substrate 失效
标题翻译：混合的含氟烃缩合物以赋予基底油和拒水性
公开(公告)号：US06440321B1
公开(公告)日：2002-08-27
申请号：US09381572
申请日：1999-09-17
申请人： Frans A. Audenaert , Dirk M. Coppens , Rudolf J. Dams
发明人： Frans A. Audenaert , Dirk M. Coppens , Rudolf J. Dams
IPC分类号： C08G1240
CPC分类号： D06M15/437 , C08G12/40 , D06M15/423 , D06M15/429 , D06M2200/11 , D06M2200/12
摘要： A fluorochemical composition to impart water repellency and/or oil repellency to a substrate, the composition comprising one or more condensates of (i) a methylolated amine or a C1-C4 alkoxylated derivative thereof, (ii) a hydrocarbon compound represented by formula (II) and (iii) a fluorinated compound represented by formula (I): Rf—(X1)n—Z1 (I) wherein: Rf is a fluorinated aliphatic group; X1 is an organic divalent linking group; Z1 is selected from the group consisting of hydroxy, thiol, amide or acid groups; and n is 0 or 1; and Rh—Z2 (II) wherein: Rh is a hydrocarbon group having at least 6 carbon atoms and optionally being substituted with 1 to 3 subsituents; Z2 is selected from the group consisting of hydroxy, thiol, amide or acid groups. The invention further provides a method of treatment of a substrate with the fluorochemical composition and a treated substrate.
摘要翻译：一种含氟化合物，其对基质赋予拒水性和/或拒油性，所述组合物包含一种或多种（i）羟甲基化胺或其C1-C4烷氧基化衍生物的缩合物，（ii）由式（II）表示的烃化合物）和（iii）由式（I）表示的氟化化合物：其中：Rf是氟化脂肪族基团; X1是有机二价连接基团; Z1选自羟基，硫醇，酰胺或酸基; 并且n为0或1; 并且其中：Rh是具有至少6个碳原子并且任选地被1至3个取代基取代的烃基; Z2选自羟基，硫醇，酰胺或酸基。本发明还提供了一种用含氟化合物组合物和经处理的底物处理底物的方法。

118. 发明授权

US06365769B1 Perfluoroalkyl halides and derivatives 失效
标题翻译：全氟烷基卤化物及其衍生物
公开(公告)号：US06365769B1
公开(公告)日：2002-04-02
申请号：US09504483
申请日：2000-02-15
申请人： Frederick E. Behr , Rudolf J. Dams , Johan E. DeWitte , Donald F. Hagen
发明人： Frederick E. Behr , Rudolf J. Dams , Johan E. DeWitte , Donald F. Hagen
IPC分类号： C07C32100
CPC分类号： C08G18/8077 , C07C17/00 , C07C17/25 , C07C19/10 , C07C19/14 , C07C19/16 , C07C31/40 , C07C51/285 , C07C53/21 , C07C69/653 , C07C305/06 , C07C309/13 , C07C309/17 , C07C323/03 , C07C323/12 , C07C323/14 , C07C323/50 , C07C323/60 , C07D303/08 , C08G18/0866 , C08G18/095 , C08G18/2885 , C08G63/682 , C07C19/01 , C07C21/18
摘要： Novel mixtures of perfluoroalkyl halides and derivatives thereof are described. These mixtures contain some compounds with a straight perfluoroalkyl group and some with a branched perfluoroalkyl group. Methods of preparation and use are also described.
摘要翻译：描述了全氟烷基卤化物及其衍生物的新型混合物。这些混合物含有一些具有直链全氟烷基的化合物，一些具有支链全氟烷基的化合物。还描述了制备和使用的方法。

119. 发明授权

US06309752B1 Substrate having high initial water repellency and a laundry durable water repellency 失效
标题翻译：基材具有较高的起始防水性和耐洗涤性
公开(公告)号：US06309752B1
公开(公告)日：2001-10-30
申请号：US09231028
申请日：1999-01-14
申请人： Rudolf J. Dams , Johan E. DeWitte , Christoffel C. Maes
发明人： Rudolf J. Dams , Johan E. DeWitte , Christoffel C. Maes
IPC分类号： B32B2712
CPC分类号： D06M15/277 , D06M15/263 , D06M15/564 , Y10T428/2964 , Y10T428/2967 , Y10T428/3154 , Y10T428/31573 , Y10T428/3158 , Y10T428/31743 , Y10T428/31797 , Y10T428/31935 , Y10T428/31993 , Y10T442/2213 , Y10T442/2262
摘要： Compositions comprising a fluorochemical agent, a copolymer extender, and a blocked isocyanate extender and substrates treated with such compositions that possess high initial water repellency and laundry durable water repellency.
摘要翻译：包含含氟化合物，共聚物增量剂和封端的异氰酸酯增量剂的组合物和用这种组合物处理的底物，其具有高的起始拒水性和耐洗涤的耐水性。

120. 发明授权

US06239247B1 Fluorochemical composition comprising a urethane having a fluorochemical oligomer and a hydrophilic segment to impart stain release properties to a substrate 有权
标题翻译：含氟化合物组合物包含具有含氟低聚物和亲水链段的氨基甲酸酯，以赋予基材去污性能
公开(公告)号：US06239247B1
公开(公告)日：2001-05-29
申请号：US09381865
申请日：1999-09-24
申请人： Kathy E. M. L. A. Allewaert , Rudolf J. Dams , Pierre J. Vander Elst
发明人： Kathy E. M. L. A. Allewaert , Rudolf J. Dams , Pierre J. Vander Elst
IPC分类号： C08G1848
CPC分类号： C08G18/4063 , C08G18/4825 , C08G18/6279 , C08G18/6295 , C08G18/672 , C08G18/8077
摘要： The present invention provides a method for preparing a fluorochemical composition comprising a urethane by reacting: (A) fluorochemical oligomer of the formula (I): MfmMn—Q1—T1 wherein MfmMn represents a fluorochemical oligomer comprising m units derived from fluorinated monomer and n units derived from fluorine-free monomer and wherein the fluorinated monomers and fluorine-free monomers may be the same or different; m is a value of about 2 to 40; n is a value of about 0 to 20; T1 is an —OH or —NH2 moiety; Q1 and T1 together represent an organic residue obtained by removing a hydrogen atom from a chain transfer agent that is functionalized with T1; (B) monofunctional compound capable of reacting with an isocyanate and comprising a poly(oxyalkylene) group; (C) isocyanate blocking agent or a fluorine-free oligomer; and (D) isocyanate-reactive compound other than said fluorochemical oligomer, said isocyanate blocking agent, said fluorine-free oligomer and said monofunctional compound; with (E) diisocyanate or a triisocyanate, wherein 33% to 67% of the number of isocyanate groups are reacted with the fluorochemical oligomer according to the formula (I), 33% to 67% of the number of isocyanate groups are reacted with said monofunctional compound, 0 to 33% of the number of isocyanate groups are reacted with an isocyanate blocking agent or a fluorine-free oligomer and 0 to 10% of the number of isocyanate groups are reacted with said isocyanate-reactive compound.
摘要翻译：本发明提供一种制备含有氨基甲酸酯的含氟化合物组合物的方法，该方法包括：（A）式（I）的氟化物低聚物：MfmMn-Q1-T1，其中MfmMn表示含有源自氟化单体的m个单元和n个单元的含氟低聚物衍生自无氟单体，其中氟化单体和无氟单体可以相同或不同; m为约2〜40的值; n为约0〜20的值; T1是-OH或-NH2部分; Q1和T1一起表示通过用T1官能化的链转移剂除去氢原子获得的有机残基; （B）能够与异氰酸酯反应并且包含聚（氧化烯）基团的单官能化合物; （C）异氰酸酯封端剂或无氟低聚物; 和（D）除所述含氟低聚物以外的异氰酸酯反应性化合物，所述异氰酸酯封端剂，所述无氟低聚物和所述单官能化合物; 与（E）二异氰酸酯或三异氰酸酯反应，其中33％至67％的异氰酸酯基数与根据式（I）的含氟低聚物反应，33％至67％的异氰酸酯基数与所述使异氰酸酯基数为0〜33％与异氰酸酯封端剂或无氟低聚物反应，0〜10％的异氰酸酯基与异氰酸酯反应性化合物反应。

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