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91. 发明授权

US08034969B2 Synthesis of N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester using 3,3-dimethylbutyraldehyde precursors 有权
标题翻译：使用3,3-二甲基丁醛前体合成N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸1-甲基酯
公开(公告)号：US08034969B2
公开(公告)日：2011-10-11
申请号：US12778306
申请日：2010-05-12
申请人： Indra Prakash , Kenneth E. Furlong , Handley E. Jackson, III
发明人： Indra Prakash , Kenneth E. Furlong , Handley E. Jackson, III
IPC分类号： C07K5/06
CPC分类号： C07K5/06113
摘要： N—[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester is produced by hydrogenation of L-α-aspartyl-L-phenylalanine 1-methyl ester and 3,3-dimethylbutyraldehyde produced in situ by the hydrolysis or cleavage of a 3,3-dimethylbutyraldehyde precursor. The production method is efficient and low cost, as compared with conventional N—[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester synthesis.
摘要翻译： N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸1-甲酯通过L-α-天冬氨酰基-L-苯丙氨酸1-甲基酯和3,3- 通过3,3-二甲基丁醛前体的水解或裂解原位产生的二甲基丁醛。与常规的N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸1-甲酯合成相比，制备方法是有效且低成本的。

92. 发明申请

US20080292764A1 Stevioside Polymorphic and Amorphous Forms, Methods for Their Formulation, and Uses 有权
标题翻译：甜菊糖苷多形态和非晶形式，其制剂方法和用途
公开(公告)号：US20080292764A1
公开(公告)日：2008-11-27
申请号：US11751625
申请日：2007-05-21
申请人： Indra Prakash , Mani Upreti
发明人： Indra Prakash , Mani Upreti
IPC分类号： A23L1/236
CPC分类号： C07H15/24 , A23L27/36 , A23V2002/00 , C07H1/06 , A23V2250/262
摘要： Exemplary embodiments of this invention encompass a method for purifying a substantially crude stevioside, methods for preparing polymorphic and amorphous forms of stevioside, and the polymorphic and amorphous forms prepared therefrom.
摘要翻译：本发明的示例性实施方案包括用于纯化基本上粗的甜菊苷的方法，用于制备甜菊糖苷的多晶型和无定形形式的方法，以及由其制备的多晶型和无定形形式。

93. 发明申请

US20070116839A1 High-Potency Sweetener Composition With C-Reactive Protein Reducing Substance and Compositions Sweetened Therewith 审中-公开
标题翻译：具有C反应蛋白质减少物质和组合物的高效甜味剂组合物
公开(公告)号：US20070116839A1
公开(公告)日：2007-05-24
申请号：US11556102
申请日：2006-11-02
申请人： Indra Prakash , Grant DuBois
发明人： Indra Prakash , Grant DuBois
IPC分类号： A23L1/236
CPC分类号： A23L2/60 , A23L27/34 , A23L27/36 , A23L27/84 , A23L33/10 , A23L33/11 , A23V2002/00 , A23V2200/326 , A23V2250/2136 , A23V2250/21366 , A23V2250/24 , A23V2250/60 , A23V2250/64
摘要： The present invention relates generally to functional sweetener compositions comprising non-caloric or low-caloric natural and/or synthetic, high-potency sweeteners and methods for making and using them. In particular, the present invention relates to different functional sweetener compositions comprising at least one non-caloric or low-caloric natural and/or synthetic, high-potency sweetener, at least one sweet taste improving composition, and at least one functional ingredient, such as C-reactive protein reducing substances. The present invention also relates to functional sweetener compositions and methods that can improve the tastes of non-caloric or low-caloric high-potency sweeteners by imparting a more sugar-like taste or characteristic. In particular, the functional sweetener compositions and methods provide a more sugar-like temporal profile, including sweetness onset and sweetness linger, and/or a more sugar-like flavor profile.
摘要翻译：本发明一般涉及包含非热量或低热量天然和/或合成的高效甜味剂的功能性甜味剂组合物及其制备和使用方法。特别地，本发明涉及不同的功能甜味剂组合物，其包含至少一种非热量或低热量天然和/或合成的高效甜味剂，至少一种甜味改善组合物和至少一种功能成分，例如作为C反应蛋白还原物质。本发明还涉及功能性甜味剂组合物和方法，其可以通过赋予更多的糖样味道或特征来改善非热量或低热量的高效甜味剂的口味。特别地，功能性甜味剂组合物和方法提供了更多的糖样时间分布，包括甜度起始和甜度徘徊，和/或更多的糖样香味。

94. 发明申请

US20070116834A1 Condiments with High-Potency Sweetener 有权
标题翻译：高效甜味剂调味品
公开(公告)号：US20070116834A1
公开(公告)日：2007-05-24
申请号：US11556062
申请日：2006-11-02
申请人： Indra Prakash , Grant DuBois
发明人： Indra Prakash , Grant DuBois
IPC分类号： A23L1/236
CPC分类号： A23L1/236 , A23D7/00 , A23D9/00 , A23L27/30 , A23L27/60 , A23L27/63
摘要： The present invention relates generally to condiment compositions comprising non-caloric or low-caloric high-potency sweeteners and methods for making and using them. In particular, the present invention relates to different condiment compositions comprising at least one non-caloric or low-caloric natural and/or synthetic high potency sweetener, at least one sweet taste improving composition, and a condiment base. The present invention also relates to condiment compositions and methods that can improve the tastes of non-caloric or low-caloric natural and/or synthetic, high-potency sweeteners by imparting a more sugar-like taste or characteristic. In particular, the condiment compositions and methods provide a more sugar-like temporal profile, including sweetness onset and sweetness linger, and/or a more sugar-like flavor profile.
摘要翻译：本发明一般涉及包含非热量或低热量的高效甜味剂的调味品组合物及其制备和使用方法。特别地，本发明涉及包含至少一种非热量或低热量天然和/或合成高效甜味剂，至少一种甜味改善组合物和调味品基质的不同调味品组合物。本发明还涉及通过赋予更多的糖样味道或特征，可以改善非热量或低热量天然和/或合成的高效甜味剂的口味的调味品组合物和方法。特别地，调味品组合物和方法提供了更多的糖状时间分布，包括甜度起始和甜度徘徊，和/或更多的糖样风味。

95. 发明申请

US20070116833A1 High-Potency Sweetener Composition with Calcium and Compositions Sweetened Therewith 审中-公开
标题翻译：具有钙和组合物的高效甜味剂组合物与其一起甜化
公开(公告)号：US20070116833A1
公开(公告)日：2007-05-24
申请号：US11556059
申请日：2006-11-02
申请人： Indra Prakash , Grant DuBois
发明人： Indra Prakash , Grant DuBois
IPC分类号： A23L1/236
CPC分类号： A61K33/06 , A23K20/147 , A23L2/60 , A23L27/33 , A23L27/34 , A23L27/36 , A23L33/165 , A23V2002/00 , A61K31/593 , A61K31/7008 , A61K31/726 , A61K33/42 , A61K45/06 , A23V2250/24 , A23V2250/262 , A23V2250/1578 , A23V2250/161
摘要： The present invention relates generally to functional sweetener compositions comprising non-caloric or low-caloric natural and/or synthetic high-potency sweeteners and methods for making and using them. In particular, the present invention relates to different functional sweetener compositions comprising at least one non-caloric or low-caloric natural and/or synthetic high potency sweetener, at least one sweet taste improving composition, and at least one functional ingredient, such as a calcium source. The present invention also relates to functional sweetener compositions and methods that can improve the tastes of non-caloric or low-caloric high-potency sweeteners by imparting a more sugar-like taste or characteristic. In particular, the functional sweetener compositions and methods provide a more sugar-like temporal profile, including sweetness onset and sweetness linger, and/or a more sugar-like flavor profile.
摘要翻译：本发明一般涉及包含非热量或低热量天然和/或合成高效甜味剂的功能甜味剂组合物及其制备和使用方法。特别地，本发明涉及包含至少一种非热量或低热量天然和/或合成高效甜味剂，至少一种甜味改善组合物和至少一种功能成分的不同功能甜味剂组合物，例如钙源。本发明还涉及功能性甜味剂组合物和方法，其可以通过赋予更多的糖样味道或特征来改善非热量或低热量的高效甜味剂的口味。特别地，功能性甜味剂组合物和方法提供了更多的糖样时间分布，包括甜度起始和甜度徘徊，和/或更多的糖样香味。

96. 发明申请

US20070116820A1 EDIBLE GEL COMPOSITIONS COMPRISING HIGH-POTENCY SWEETENERS 审中-公开
标题翻译：可食用凝胶组合物，包含高分子浸泡剂
公开(公告)号：US20070116820A1
公开(公告)日：2007-05-24
申请号：US11555774
申请日：2006-11-02
申请人： Indra Prakash , Grant DuBois
发明人： Indra Prakash , Grant DuBois
IPC分类号： A23L1/236
CPC分类号： A23G1/30 , A23L9/12 , A23L27/32 , A23L27/34 , A23L27/36 , A23L27/37 , A23L29/20 , A23L29/284
摘要： The present invention relates generally to edible gel compositions comprising non-caloric or low-caloric high-potency sweeteners and methods for making and using them. In particular, the present invention relates to different edible gel compositions comprising at least one non-caloric or low-caloric natural and/or synthetic high-potency sweetener and at least one sweet taste improving composition. The present invention also relates to edible gel compositions and methods that can improve the tastes of non-caloric or low-caloric natural and/or synthetic high-potency sweeteners by imparting a more sugar-like taste or characteristic. In particular, the edible gel compositions and methods provide a more sugar-like temporal profile, including sweetness onset and sweetness linger, and/or a more sugar-like flavor profile.
摘要翻译：本发明一般涉及包含非热量或低热量的高效甜味剂的可食用凝胶组合物及其制备和使用方法。特别地，本发明涉及不同的可食用凝胶组合物，其包含至少一种非热量或低热量天然和/或合成的高效甜味剂和至少一种甜味改善组合物。本发明还涉及可通过赋予更多的糖样味道或特征来改善非热量或低热量天然和/或合成高效甜味剂的口味的食用凝胶组合物和方法。特别地，可食用的凝胶组合物和方法提供了更多的糖样时间特征，包括甜度起始和甜度徘徊，和/或更多的糖样香味。

97. 发明申请

US20070116819A1 High-Potency Sweetener Composition with Fatty Acid and Compositions Sweetened Therewith 有权
标题翻译：具有脂肪酸和组合物的高效甜味剂组合物与其一起甜化
公开(公告)号：US20070116819A1
公开(公告)日：2007-05-24
申请号：US11555766
申请日：2006-11-02
申请人： Indra Prakash , Grant DuBois , Lihong D'Angelo , Youlung Chen
发明人： Indra Prakash , Grant DuBois , Lihong D'Angelo , Youlung Chen
IPC分类号： A23L1/236
CPC分类号： A23L1/2364 , A23L2/02 , A23L2/38 , A23L2/60 , A23L5/00 , A23L7/00 , A23L9/00 , A23L21/00 , A23L27/30 , A23L27/34 , A23L27/36 , A23L29/30 , A23L33/105 , A23L33/12 , A23L33/125 , A23L33/16 , A23L33/175 , A23V2002/00 , A23V2200/16 , A23V2250/06 , A23V2250/1882 , A23V2250/24 , A23V2250/64
摘要： The present invention relates generally to functional sweetener compositions comprising non-caloric or low-caloric natural and/or synthetic, high-potency sweeteners and methods for making and using them. In particular, the present invention relates to different functional sweetener compositions comprising at least one non-caloric or low-caloric natural and/or synthetic, high-potency sweetener, at least one sweet taste improving composition, and at least one functional ingredient, such as fatty acids. The present invention also relates to functional sweetener compositions and methods that can improve the tastes of non-caloric or low-caloric high-potency sweeteners by imparting a more sugar-like taste or characteristic. In particular, the functional sweetener compositions and methods provide a more sugar-like temporal profile, including sweetness onset and sweetness linger, and/or a more sugar-like flavor profile.
摘要翻译：本发明一般涉及包含非热量或低热量天然和/或合成的高效甜味剂的功能性甜味剂组合物及其制备和使用方法。特别地，本发明涉及不同的功能甜味剂组合物，其包含至少一种非热量或低热量天然和/或合成的高效甜味剂，至少一种甜味改善组合物和至少一种功能成分，例如作为脂肪酸。本发明还涉及功能性甜味剂组合物和方法，其可以通过赋予更多的糖样味道或特征来改善非热量或低热量的高效甜味剂的口味。特别地，功能性甜味剂组合物和方法提供了更多的糖样时间分布，包括甜度起始和甜度徘徊，和/或更多的糖样香味。

98. 发明申请

US20050014967A1 Synthesis of N-[N-(3,3-dimethylbutyl)-L-alpha-aspartyl]-L-phenylalanine 1-methyl ester using oxazolidinone derivatives 有权
标题翻译：使用恶唑烷酮衍生物合成N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸1-甲基酯
公开(公告)号：US20050014967A1
公开(公告)日：2005-01-20
申请号：US10902143
申请日：2004-07-30
申请人： Indra Prakash
发明人： Indra Prakash
IPC分类号： C07K5/072 , C07K5/075 , C07K5/04
CPC分类号： C07K5/06113
摘要： N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester is produced using novel oxazolidinone derivatives.
摘要翻译：使用新的恶唑烷酮衍生物制备N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸1-甲酯。

99. 发明授权

US06825384B1 Bromine free TEMPO based catalyst system for oxidation of primary and secondary alcohols using NaOCl as an oxidant 有权
标题翻译：使用无氧自由基TEMPO的催化剂体系，用NaOCl作为氧化剂氧化伯醇和仲醇
公开(公告)号：US06825384B1
公开(公告)日：2004-11-30
申请号：US10767805
申请日：2004-01-29
申请人： Indra Prakash , Setrak K. Tanielyan , Robert L. Augustine , Kenneth E. Furlong , Robert C. Scherm , Handley E. Jackson
发明人： Indra Prakash , Setrak K. Tanielyan , Robert L. Augustine , Kenneth E. Furlong , Robert C. Scherm , Handley E. Jackson
IPC分类号： C07C4529
CPC分类号： C07C45/30 , C07C2601/14 , C07C47/02 , C07C47/54 , C07C49/403 , C07C49/04
摘要： The present invention relates to a process of oxidation of alcohols selectively to aldehydes or ketones with NaOCl using a TEMPO—borate catalyst system. It is shown that the oxidation can be efficiently carried out without KBr additives under solvent free conditions. Aldehydes such as 3,3-dimethylbutyraldehyde can be produced efficiently using the present invention.
摘要翻译：本发明涉及使用TEMPO-硼酸盐催化剂体系，用NaOCl将醇选择性氧化成醛或酮的方法。表明在无溶剂条件下，无KBr添加剂可以有效地进行氧化。可以使用本发明有效地制备诸如3,3-二甲基丁醛的醛。

100. 发明授权

US06423864B1 Purification of N-[N-(3,3-dimethylbutyl)-L-&agr;-aspartyl]-L-phenylalanine 1-methyl ester via crystallization 有权
标题翻译：通过结晶纯化N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸1-甲酯
公开(公告)号：US06423864B1
公开(公告)日：2002-07-23
申请号：US09448671
申请日：1999-11-24
申请人： Indra Prakash , Christine M. V. Moore , Kurt Wachholder
发明人： Indra Prakash , Christine M. V. Moore , Kurt Wachholder
IPC分类号： C07C22900
CPC分类号： C07K5/06113
摘要： N-[N-(3,3-dimethylbutyl)-L-&agr;-aspartyl]-L-phenylalanine 1-methyl ester is crystallized in order to give highly pure product in high yield. In a preferred embodiment of the present invention, N-[N-(3,3-dimethylbutyl)-L-&agr;-aspartyl]-L-phenylalanine 1-methyl ester is crystallized directly from an aqueous methanol reaction mixture.
摘要翻译： N- [N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸1-甲酯结晶，以高产率得到高纯度产物。在本发明的优选实施方案中，N-甲基-N-（3,3-二甲基丁基）-L-α-天冬氨酰基] -L-苯丙氨酸1-甲酯直接从甲醇水溶液混合物中结晶。

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