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1. 发明授权

US5124073A Continuous preparation of aqueous non-self-emulsifying polymer dispersions 失效
标题翻译：连续制备水性非自发聚合物分散体
公开(公告)号：US5124073A
公开(公告)日：1992-06-23
申请号：US476736
申请日：1990-02-08
申请人： Friedrich Goffing , Joerg Kroker , Rainer Nachtrab , Heino Thiele
发明人： Friedrich Goffing , Joerg Kroker , Rainer Nachtrab , Heino Thiele
IPC分类号： C08J3/02 , C08J3/03
CPC分类号： C08J3/03
摘要： Aqueous non-self-emulsifying polymer dispersions having small particles and a long shelf life and based on highly viscous reaction resins are prepared without the addition of solvents, by means of an intensively dispersing screw apparatus, by a continuous process in which the preparation of the polymer dispersion is carried out in an intensive shear zone of the screw apparatus, the water/reaction resin ratio in this intensive shear zone corresponding to the phase inversion point or being close to it, and the specific energy supply is 0.01-0.15 kWh/kg, the residence time is 0.1-60 sec and the shear gradient is 2,000-20,000 sec.sup.-1.
摘要翻译：通过连续的方法，通过连续方法制备具有小颗粒和长保质期并且基于高粘度反应树脂的水性非自乳化聚合物分散体，而不通过浓缩分散螺杆装置添加溶剂，其中制备聚合物分散体在螺旋装置的强剪切区域中进行，该强化剪切区域中的水/反应树脂比率对应于相转化点或接近相转变点，比能量供应量为0.01-0.15kWh / kg ，停留时间为0.1-60秒，剪切梯度为2,000-20,000秒-1。

2. 发明授权

US06498232B1 Method for coagulating plastics dispersions using a device with shearing elements 失效
标题翻译：使用具有剪切元件的装置凝结塑料分散体的方法
公开(公告)号：US06498232B1
公开(公告)日：2002-12-24
申请号：US09857050
申请日：2001-05-31
申请人： Norbert Güntherberg , Jürgen Hofmann , Alexander Ludwig , Hartmut Heinen , Gerd Ehrmann , Peter Barghoorn , Andreas Kleinke , Sven Grabowski , Rainer Nachtrab , Bernhard Czauderna
发明人： Norbert Güntherberg , Jürgen Hofmann , Alexander Ludwig , Hartmut Heinen , Gerd Ehrmann , Peter Barghoorn , Andreas Kleinke , Sven Grabowski , Rainer Nachtrab , Bernhard Czauderna
IPC分类号： C08F600
CPC分类号： B29C47/8895 , B29B15/04 , B29C47/0009 , B29C47/0014 , B29C47/64
摘要： Shear forces are used for essentially salt-free coagulation of plastics dispersions or rubber dispersions. For this, method of use is made of an apparatus with at least one shearing module which has a stator and a rotor arranged within the stator, where the surfaces facing toward one another in the stator and in the rotor are in each case smooth, or at least the rotor exhibits a structure formed on its surface and facing from this in the direction of the stator, and between the stator and the rotor there is a gap of predetermined gap width. The process is carried out by passing the dispersion to be coagulated through the gap between stator and rotor and precipitating the dispersion by rotation of the rotor with predetermined shear rate and shear deformation.
摘要翻译：剪切力用于塑料分散体或橡胶分散体的基本无盐凝结。为此，使用的方法由具有至少一个剪切模块的装置制成，该剪切模块具有布置在定子内的定子和转子，其中在定子和转子中彼此面对的表面在每种情况下都是平滑的，或者至少转子表现出在其表面上形成并且在定子的方向上面对的结构，并且在定子和转子之间存在预定间隙宽度的间隙。该过程通过使待凝结的分散体通过定子和转子之间的间隙通过转子的转动而以预定的剪切速率和剪切变形使转子沉淀而使分散体沉淀。

3. 发明授权

US5081270A Preparation of hydroxyanthraquinones 失效
标题翻译：羟基四氢呋喃的制备
公开(公告)号：US5081270A
公开(公告)日：1992-01-14
申请号：US599975
申请日：1990-10-19
申请人： Juergen Pfister , Michael Schiessl , Rainer Nachtrab
发明人： Juergen Pfister , Michael Schiessl , Rainer Nachtrab
IPC分类号： B01J27/08 , B01J19/20 , C07B61/00 , C07C46/00 , C07C46/02 , C07C50/34 , C07C50/38
CPC分类号： C07C50/38 , B01J19/20 , C07C46/00 , C07C50/34
摘要： 1-Hydroxyanthraquinones are prepared in an improved process by reacting phthalic anhydride or derivatives thereof with phenol derivatives in the presence of a Lewis acid as catalyst and in the presence or absence of a diluent, wherein the improvement comprises conducting the reaction in a self-cleaning apparatus having a mixing effect, at a temperature of from 120.degree. C. to 300.degree. C. for from 5 to 1,000 seconds, the self-cleaning apparatus having a mixing effect subjecting the reactants to a shear gradient of from 50 to 20,000 sec.sup.-1 with an energy input of from 0.01 to 0.2 kwh/kg of reactants.
摘要翻译：通过邻苯二甲酸酐或其衍生物与苯酚衍生物在路易斯酸作为催化剂的存在下和在存在或不存在稀释剂的情况下反应制备1-羟基蒽醌，其中改进包括在自清洁中进行反应具有混合效果的装置，在120℃至300℃的温度下为5至1,000秒，所述自清洁装置具有将反应物的剪切梯度为50至20,000秒的混合效果， 1，能量输入为0.01至0.2千瓦时/ kg的反应物。

4. 发明授权

US5476628A GMT sheet material produced from GMT recyclate 失效
标题翻译： GMT格林尼治标准时间（GMT）材料从GMT回收生产
公开(公告)号：US5476628A
公开(公告)日：1995-12-19
申请号：US303465
申请日：1994-09-09
申请人： Horst Baumgartl , Karl-Ludwig Brentrup , Jurgen Hofmann , Peter Ittemann , Rainer Nachtrab , Hilmar Ohlig , Alois Schlarb
发明人： Horst Baumgartl , Karl-Ludwig Brentrup , Jurgen Hofmann , Peter Ittemann , Rainer Nachtrab , Hilmar Ohlig , Alois Schlarb
IPC分类号： B29B17/02 , C08J11/06 , B29C47/04
CPC分类号： B29B17/0042 , C08J11/06 , B29K2023/12 , B29K2101/12 , B29K2105/06 , B29K2105/08 , B29K2709/08 , Y02W30/62 , Y02W30/701 , Y10T428/249924
摘要： Semi-finished GMT sheet material of GMT recyclate in which more than 50% by weight of the glass fibers are more than 2 mm in length and which is produced by extruding GMT recyclate particles without significant comminution of the glass fibers.
摘要翻译：格林尼治标准时间回收的半成品GMT片材，其中超过50重量％的玻璃纤维的长度大于2mm，并且通过挤出GMT回收颗粒而不会显着粉碎玻璃纤维而产生。

5. 发明授权

US5006173A Transforming crude copper phthalocyanines into a pigmentary state 失效
标题翻译：将粗铜酞菁转变为颜料状态
公开(公告)号：US5006173A
公开(公告)日：1991-04-09
申请号：US370727
申请日：1989-06-23
申请人： Wolfgang Fath , Rainer Nachtrab , Rudolf Polster
发明人： Wolfgang Fath , Rainer Nachtrab , Rudolf Polster
IPC分类号： C09B67/12 , C09B67/20
CPC分类号： C09B67/0016
摘要： Crude copper phthalocyanines are transformed into a pigmentary state by treating finely divided but imperfectly crystallized and highly aggregated crude copper phthalocyanines having a primary particle size, produced by ball milling, or less than 0.1 .mu.m with an organic solvent by subjecting a suspension of the organic solvent and the milled crude copper phthalocyanine (hereinafter referred to as the solvent/pigment suspension), which has a pigment concentration of from 15 to 55% by weight and a solvent concentration of from 15 to 85% by weight and which may contain water in a concentration of from 0 to 30% by weight, to a shear gradient of from 1000 to 20000 s.sup.-1 for a period of from 2 to 1000 s with an energy uptake during shearing of from 0.01 to 0.02 kWh/kg of pigment throughput, then metering water into the solvent/pigment suspension in an amount of from 0.1 to 10 times the amount of the solvent, to effect a defined discontinuation of the conditioning process, and finally mixing the suspension until homogeneous.
摘要翻译：粗铜酞菁通过用有机溶剂处理细分但不完全结晶的高度聚集的粗铜酞菁，其具有初级粒度，通过球磨或小于0.1μm，通过使有机溶剂的悬浮液进行处理而转化为颜料状态溶剂和研磨的粗铜酞菁（以下称为溶剂/颜料悬浮液），其颜料浓度为15至55重量％，溶剂浓度为15至85重量％，并且可以含有水浓度为0至30重量％，剪切梯度为1000至20000秒-1，时间为2至1000秒，剪切时的能量摄取为0.01至0.02千瓦时/千克的颜料生产量，然后将溶剂/颜料悬浮液中的水量定量为溶剂量的0.1至10倍，以实现定义的中止调理过程，最后混合t 他暂停直到均匀。

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