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1. 发明专利

BR9707327A 未知
公开(公告)号：BR9707327A
公开(公告)日：1999-04-13
申请号：BR9707327
申请日：1997-12-02
申请人： ATSUSHI SUDO , AKIRA IWAMOTO , KAZUO SHIRAISHI , KOICHI WADA , YOSHIMASA SEO , HIROYOSHI NOWATARI , FUMIO SAKAI
发明人： SUDO ATSUSHI , IWAMOTO AKIRA , SHIRAISHI KAZUO , WADA KOICHI , SEO YOSHIMASA , NOWATARI HIROYOSHI , SAKAI FUMIO
IPC分类号： B01J23/88 , B01J8/06 , B01J23/31 , B01J23/887 , C07B61/00 , C07C27/14 , C07C45/35 , C07C47/22 , C07C51/25 , C07C57/05 , B01J27/192
摘要： The present invention concerns a method for producing acrolein and acrylic acid by carrying out vapor phase catalytic oxidation of propylene with molecular oxygen or a gas containing molecular oxygen using a oxidation catalysts comprising Mo, Bi and Fe as an essentially element and a fixed bed multitubular reactor, which comprises a) using a plurality of supported catalysts having different activities, which was obrtained, for example, by different calcination method in the production process of the supported catalysts, b) setting a catalyst layer in a reaction tube, which is formed by dividing it into plural portions in the tube axial direction, and c) arranging the aforementioned plural supported catalysts in such order that the activity becomes high toward the outlet from the inlet of the material gas in the reaction tube axial direction. According to the present invention, the generation of hot spot can be avoided and over oxidation reaction can be avoided and the acrolein and acrylic acid are produced constantly for a prolonged period of time.

2. 发明专利

JP2005221514A Thick slab lens, its manufacturing method, and optical wave coupling device using the thick slab lens 审中-公开
标题翻译：厚板镜片，其制造方法和光学耦合器件使用厚度均匀的镜片
公开(公告)号：JP2005221514A
公开(公告)日：2005-08-18
申请号：JP2002060849
申请日：2002-03-06
申请人： Hoya Corp , Hoya株式会社 , Kazuo Shiraishi , 和男白石
发明人： SHIRAISHI KAZUO
IPC分类号： G02B3/00 , G02B6/36 , G02B6/42 , H01S5/022
CPC分类号： G02B6/425
摘要： PROBLEM TO BE SOLVED: To provide a thick slab lens suitable for mass production, by being integrated in between a semiconductor laser array and an optical fiber array or the waveguide array of an optical integrated circuit, and to provide its manufacturing method.
SOLUTION: The thick slab lens 2 has the shape of a thick film, has a large specific refractive index difference which does not exceed several tens of percent, and has substantially a quarter of the cycle for meandering of a light beam by the length in the light propagating direction or odd multiples thereof. Thereby the light intensity distribution of a semiconductor laser or the like, having a small spot size in only one direction, can be directly converted into a substantially circular light intensity distribution which does not exceed the spot size of a standard optical fiber and a light source and a waveguide can be integrated. The structure is small in size and lightweight, and is simple to manufacture and can be mass-produced.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：通过集成在半导体激光器阵列和光纤阵列或光学集成电路的波导阵列之间来提供适合于批量生产的厚板坯透镜，并提供其制造方法。解决方案：厚板状透镜2具有厚膜的形状，具有不超过几十％的大的比折射率差，并且具有基本上四分之一的光束弯曲周期光传播方向的长度或其奇数倍。由此，可以将仅具有一个方向的小斑点尺寸的半导体激光器等的光强度分布直接转换为基本上不会超过标准光纤和光源的光斑尺寸的圆形光强度分布并且可以集成波导。结构尺寸小，重量轻，制造简单，可批量生产。版权所有（C）2005，JPO＆NCIPI

3. 发明申请

US20130310604A1 Process For Producing Unsaturated Aldehyde And/or Unsaturated Carboxylic Acid 有权
标题翻译：生产不饱和醛和/或不饱和羧酸的方法
公开(公告)号：US20130310604A1
公开(公告)日：2013-11-21
申请号：US13982808
申请日：2012-01-16
申请人： Tatsuhiko Kurakami , Susumu Matsumoto , Atsushi Sudo , Kazuo Shiraishi , Masashi Hashiba
发明人： Tatsuhiko Kurakami , Susumu Matsumoto , Atsushi Sudo , Kazuo Shiraishi , Masashi Hashiba
IPC分类号： C07C51/25 , C07C45/38 , C07C51/235 , C07C45/35
CPC分类号： C07C51/235 , C07C45/35 , C07C45/38 , C07C51/252 , C07C47/22 , C07C57/04
摘要： There is provided a process for producing aerolein, acrylic acid, methacrolein, methacrylic acid in a safe and steady manner and in high yields, which avoids a phenomenon of occurrence of an abnormal reaction attributable to the fact that the temperature at a raw material gas outlet side becomes considerably higher than the temperature at a raw material gas inlet side, with regard to the temperature of a catalyst packed in a reaction tube at vapor-phase catalytic oxidation of propylene, isobutylene, or the like.In the process of using a reaction tube on which a plurality of catalyst layers formed in a raw material gas flow direction, a catalyst and a catalyst packing schedule are designed so that a relation between the raw material conversion rate at which the yield of the objective product becomes maximum and the raw material conversion rate at which a high and low correlation between maximum temperature of the catalyst layer present closest to a reaction gas inlet side Zin and maximum temperature of the catalyst layer present closest to a reaction gas outlet side Zout is reversed satisfies a specific condition of 0.5≦Cmax−Ccrs≦5, in which Cmax: a raw material conversion rate at which yield of the objective products becomes maximum; and Ccrs: a raw material conversion rate at which, when maximum temperature of the catalyst layer Zin is regarded as Tin, maximum temperature of the catalyst layer Zout is regarded as Tout, and the raw material conversion rate is changed, a high and low correlation between Tin and Tout is reversed.
摘要翻译：提供了以安全稳定的方式和高产率生产气溶胶，丙烯酸，甲基丙烯醛，甲基丙烯酸的方法，避免了由于原料气体出口处的温度导致的异常反应的发生现象相对于在丙烯，异丁烯等的气相催化氧化反应管中填充的催化剂的温度，原料气体入口侧的温度显着高于原料气体入口侧的温度。在使用在原料气体流动方向上形成有多个催化剂层的反应管的过程中，设计催化剂和催化剂填充进度，使得目的物的产率的原料转化率之间的关系产物变得最大，并且最接近反应气体入口侧的催化剂层的最高温度和最接近反应气体出口侧的催化剂层的最高温度之间的高低相关性的原料转化率反转满足0.5 @ Cmax-Ccrs @ 5的特定条件，其中Cmax：目标产物的产率变为最大的原料转化率; Ccrs：将催化剂层Zin的最高温度设为Tin时的原料转化率，将催化剂层Zout的最高温度设为Tout，将原料转化率变更为高，低相关 Tin和Tout之间是相反的。

4. 发明授权

US5929275A Catalyst and process for producing unsaturated aldehyde and unsaturated acid 失效
标题翻译：用于生产不饱和醛和不饱和酸的催化剂和方法
公开(公告)号：US5929275A
公开(公告)日：1999-07-27
申请号：US853215
申请日：1997-05-09
申请人： Koichi Wada , Akira Iwamoto , Yoshimasa Seo , Atsusi Sudo , Fumio Sakai , Kazuo Shiraishi , Hideaki Miki
发明人： Koichi Wada , Akira Iwamoto , Yoshimasa Seo , Atsusi Sudo , Fumio Sakai , Kazuo Shiraishi , Hideaki Miki
IPC分类号： B01J23/88 , B01J23/887 , B01J35/08 , B01J37/00 , B01J37/02 , C07B61/00 , C07C27/14 , C07C45/35 , C07C45/37 , C07C45/38 , C07C47/22 , C07C51/25 , C07C51/275 , C07C57/05 , C07C51/16 , B01J23/16 , C07C45/32
CPC分类号： C07C45/37 , B01J23/002 , B01J23/8876 , B01J37/0223 , C07C45/35 , C07C51/252 , B01J2523/00
摘要： A catalyst for the production of unsaturated aldehyde and unsaturated acid, obtained by loading a catalytically active component on a carrier and calcining the loaded catalyst, characterized by an average particle diameter of the catalyst of 4 to 16 mm, an average particle diameter of the carrier of 3 to 12 mm, a calcining temperature of 520 to 600.degree. C. and an amount of the catalytically active component loaded on the carrier of 5 to 80% by weight �weight of the catalytically active component)/(weight of the catalytically active component+weight of the carrier+weight of a strength improver)!, and a process for producing unsaturated aldehyde and unsaturated acid with the catalyst.
摘要翻译：用于生产不饱和醛和不饱和酸的催化剂，其通过将催化活性组分负载在载体上并煅烧负载的催化剂而获得，其特征在于催化剂的平均粒径为4至16mm，载体的平均粒径 3至12mm，煅烧温度为520-600℃，负载在载体上的催化活性组分的量为5-80重量％[催化活性组分的重量] /（催化活性组分的重量）组分+载体重量+强度改进剂的重量）]以及用催化剂生产不饱和醛和不饱和酸的方法。

5. 发明授权

US4892832A Filter bag for microbiological examination 失效
标题翻译：滤袋用于微生物检测
公开(公告)号：US4892832A
公开(公告)日：1990-01-09
申请号：US127651
申请日：1987-12-02
申请人： Kiyotaka Omote , Yuichi Matsushima , Masami Taki , Harutomo Oshio , Kazuo Shiraishi
发明人： Kiyotaka Omote , Yuichi Matsushima , Masami Taki , Harutomo Oshio , Kazuo Shiraishi
IPC分类号： B01D35/00 , C12M1/26 , G01N33/02 , C12M1/12
CPC分类号： G01N33/02 , B01D35/00
摘要： There is here provided a convenient bag used at the time when microorganisms which adhere to a specimen containing a solid material are extracted with a saline solution and are then examined. In this bag, a filter sheet is stuck to plastic film sidewalls so as to extend from the opening inlet to the bottom portion of the sidewalls, so that the bag is divided into two chambers. A specimen and a saline solution are poured into one of the two chambers, and the resulting extract is taken out by a pipet from another chamber.
摘要翻译：这里提供了当用含有固体物质的样品附着的微生物用盐水溶液萃取时使用的方便的袋子，然后进行检查。在该袋中，将过滤片粘贴到塑料膜侧壁上，以从侧壁的开口入口延伸到底部，使得袋被分成两个室。将样品和盐水溶液倒入两个室中的一个，并且通过移液管从所述另一个室取出所得到的提取物。

6. 发明授权

US06852203B1 Three-dimensional periodical structure, its manufacturing method, and method of manufacturing film 有权
标题翻译：三维周期结构，其制造方法和制作方法
公开(公告)号：US06852203B1
公开(公告)日：2005-02-08
申请号：US09402112
申请日：1998-03-24
申请人： Shojiro Kawakami , Hiroyuki Sakaki , Kazuo Shiraishi
发明人： Shojiro Kawakami , Hiroyuki Sakaki , Kazuo Shiraishi
IPC分类号： G02B5/18 , G02B6/12 , G02B6/122 , G02B6/13 , H01S5/00 , H01S5/10 , H01S5/20 , C23C14/34 , B32B3/12
CPC分类号： B82Y20/00 , G02B6/12002 , G02B6/1225 , Y10T428/24165
摘要： A three-dimensional periodical structure whose period is about 1 μm or smaller is provided. At least two kinds of films which have two-dimensionally substantially periodical projections are successively formed in layers substantially periodical to construct structure which is substantially three-dimensionally periodical. For instance, the films are made of materials different in refractive index. The three-dimensional periodical structure whose period is about 1 μm or smaller can be obtained by a simple fabricating method. By this structure, the propagation of a wave with a specific wavelength in many solid angular directions including several axial directions parallel to the plane and the thickness direction of the layers can be cut off.
摘要翻译：提供了周期为1m或更小的三维周期结构。至少两种具有二维基本上周期性的突起的膜基本周期地依次形成，以构造基本上三维周期的结构。例如，膜由折射率不同的材料制成。周期约为1um或更小的三维周期结构可以通过简单的制造方法获得。通过这种结构，可以切断具有特定波长的波在许多固体角方向上的传播，包括平行于平面的几个轴向和层的厚度方向。

7. 发明授权

US5774607A Lensed-fiber with cascaded graded-index fiber chip configuration 失效
标题翻译：具有级联渐变折射率光纤芯片配置的光纤
公开(公告)号：US5774607A
公开(公告)日：1998-06-30
申请号：US718375
申请日：1996-09-27
申请人： Kazuo Shiraishi , Kazuhito Matsumura , Isamu Ohishi
发明人： Kazuo Shiraishi , Kazuhito Matsumura , Isamu Ohishi
IPC分类号： G02B6/32 , G02B6/02 , G02B6/028 , G02B6/42
CPC分类号： G02B6/4203 , G02B6/4206
摘要： A lensed-fiber including a single-mode fiber having a core and a cladding, a coreless fiber having a coreless isotropic refractive index and a convex surface at a first end thereof, and a square-law index fiber having a square-law index profile. The square-law index fiber is positioned between the single-mode fiber and the coreless fiber so as to connect an end of the single-mode fiber to a second end of the coreless fiber. The lensed-fiber may be arranged in a optical module facing an optical semiconductor element which emits a light beam to be propagated through the single-mode fiber.
摘要翻译： PCT No.PCT / JP96 / 00398 Sec。 371日期1996年9月27日第 102（e）1996年9月27日PCT PCT 1996年2月22日PCT公布。公开号WO96 / 26459 日期1996年8月29日包括具有芯和包层的单模光纤的透镜光纤，具有无芯各向同性折射率的无芯光纤和其第一端的凸面，以及具有平方律索引。平方律索引光纤位于单模光纤和无芯光纤之间，以将单模光纤的一端连接到无芯光纤的第二端。透镜光纤可以布置在面向发射要通过单模光纤传播的光束的光学半导体元件的光学模块中。

8. 发明授权

US5446816A Optical fiber having a lens formed at an end thereof 失效
标题翻译：具有在其端部形成的透镜的光纤
公开(公告)号：US5446816A
公开(公告)日：1995-08-29
申请号：US283959
申请日：1994-08-01
申请人： Kazuo Shiraishi , Kazuhito Matsumura , Isamu Oishi , Katsuo Ebine
发明人： Kazuo Shiraishi , Kazuhito Matsumura , Isamu Oishi , Katsuo Ebine
IPC分类号： G02B6/02 , G02B6/255 , G02B6/32 , G02B6/42
CPC分类号： G02B6/322 , G02B6/2552 , G02B6/4203
摘要： An optical fiber having a lens formed at an end thereof comprises a fiber body including a core and a cladding, and an incident light guide portion having a uniform refractive index and integrally formed at an end portion of the fiber body, wherein the incident light guide portion has a convex surface, and the core has a distal end located within the incident light guide portion at a position close to a focal point of the incident light guide portion. When the incident light guide portion is arranged in alignment with a light source such that an extremity of the convex surface of the incident light guide portion faces a light-emitting surface of the light source, assuming that an X-Y coordinate system is established wherein the X axis coincides with the optical axis of the fiber body and the Y axis coincides with a radius direction of the fiber body, the relationship expressed by the following equation is fulfilled: ##EQU1## where coordinates of the extremity of the convex surface of the incident light guide portion are (0, 0), coordinates of the light-emitting surface of the light source are (-k, 0), coordinates of the distal end of the core are (L, 0), coordinates of an incident point at which light from the light-emitting surface of the light source falls upon the convex surface of the incident light guide portion are (z, r), and the refractive index of the incident light guide portion is n. Accordingly, no phase difference of laser beams occurs when the optical fiber is connected to a semiconductor laser, making it possible to provide a high coupling efficiency optical fiber.
摘要翻译：具有在其端部形成的透镜的光纤包括具有芯和包层的纤维体和具有均匀折射率并且一体地形成在纤维体的端部的入射光导部，其中入射光导所述芯具有位于所述入射光导部内的远端，所述远端位于所述入射光导部的焦点附近的位置。当入射光导部分与光源对准地布置，使得入射光导部分的凸表面的末端面向光源的发光表面时，假设建立XY坐标系，其中X 轴与光纤体的光轴重合，Y轴与纤维体的半径方向一致，满足下式所表示的关系：入射光的凸面的末端的坐标引导部分为（0,0），光源的发光面的坐标为（-k，0），芯的前端的坐标为（L，0），入射点的坐标为来自入射光导部的凸面的光源的发光面的光为（z，r），入射导光部的折射率为n。因此，当光纤连接到半导体激光器时，不会发生激光束的相位差，使得可以提供高耦合效率的光纤。

9. 发明授权

US08586785B2 Process for producing catalyst for methacrylic acid production and process for producing methacrylic acid 有权
标题翻译：生产甲基丙烯酸催化剂的方法和生产甲基丙烯酸的方法
公开(公告)号：US08586785B2
公开(公告)日：2013-11-19
申请号：US13298645
申请日：2011-11-17
申请人： Atsushi Sudo , Kazuo Shiraishi , Hideki Sugi , Hiroyoshi Nowatari , Fumio Sakai , Tomoaki Kobayashi , Tatsuhiko Kurakami
发明人： Atsushi Sudo , Kazuo Shiraishi , Hideki Sugi , Hiroyoshi Nowatari , Fumio Sakai , Tomoaki Kobayashi , Tatsuhiko Kurakami
IPC分类号： C07C51/16 , B01J27/199 , B01J27/19
CPC分类号： B01J37/0219 , B01J23/002 , B01J27/199 , B01J37/0045 , B01J37/0221 , B01J2523/00 , C07C51/252 , B01J2523/17 , B01J2523/51 , B01J2523/52 , B01J2523/55 , B01J2523/68 , C07C57/04
摘要： An object of the present invention is to provide a process for stably producing a catalyst for methacrylic acid production exhibiting high activity and high performance. The process for producing a catalyst for methacrylic acid production of the invention is characterized in that the water content of the catalyst ingredient powder for use in molding, temperature and humidity of a molding step, humidity and temperature of a baking step are individually controlled in the case where molding is performed by a coating method using an Mo—V—P—Cu-based hetero polyacid as an active ingredient and water or an alcohol and/or an aqueous solution of an alcohol as a binder.
摘要翻译：本发明的目的是提供稳定地生产表现出高活性和高性能的甲基丙烯酸生产催化剂的方法。本发明的甲基丙烯酸制造用催化剂的制造方法的特征在于，在成型步骤中使用的成型用的催化剂成分粉末，成型步骤的温度和湿度，烘烤步骤的湿度和温度的含水量分别控制在通过使用Mo-VP-Cu系杂多酸作为活性成分的涂布方法和水或醇和/或醇的水溶液作为粘合剂进行成型的情况。

10. 发明申请

US20120065427A1 Process For Producing Catalyst For Methacrylic Acid Production And Process For Producing Methacrylic Acid 有权
标题翻译：用于生产甲基丙烯酸生产催化剂的方法和生产甲基丙烯酸的方法
公开(公告)号：US20120065427A1
公开(公告)日：2012-03-15
申请号：US13298645
申请日：2011-11-17
申请人： Atsushi Sudo , Kazuo Shiraishi , Hideki Sugi , Hiroyoshi Nowatari , Fumio Sakai , Tomoaki Kobayashi , Tatsuhiko Kurakami
发明人： Atsushi Sudo , Kazuo Shiraishi , Hideki Sugi , Hiroyoshi Nowatari , Fumio Sakai , Tomoaki Kobayashi , Tatsuhiko Kurakami
IPC分类号： C07C51/16 , B01J27/199
CPC分类号： B01J37/0219 , B01J23/002 , B01J27/199 , B01J37/0045 , B01J37/0221 , B01J2523/00 , C07C51/252 , B01J2523/17 , B01J2523/51 , B01J2523/52 , B01J2523/55 , B01J2523/68 , C07C57/04
摘要： An object of the present invention is to provide a process for stably producing a catalyst for methacrylic acid production exhibiting high activity and high performance. The process for producing a catalyst for methacrylic acid production of the invention is characterized in that the water content of the catalyst ingredient powder for use in molding, temperature and humidity of a molding step, humidity and temperature of a baking step are individually controlled in the case where molding is performed by a coating method using an Mo—V—P—Cu-based hetero polyacid as an active ingredient and water or an alcohol and/or an aqueous solution of an alcohol as a binder.
摘要翻译：本发明的目的是提供稳定地生产表现出高活性和高性能的甲基丙烯酸生产催化剂的方法。本发明的甲基丙烯酸制造用催化剂的制造方法的特征在于，在成型步骤中使用的成型用的催化剂成分粉末，成型步骤的温度和湿度，烘烤步骤的湿度和温度的含水量分别控制在通过使用Mo-V-P-Cu系杂多酸作为活性成分的涂布法和水或醇和/或醇的水溶液作为粘合剂进行成型的情况。

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