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1. 发明授权

US5194914A Furnace for the electrothermal atomization of samples in atomic absorption spectroscopy 失效
标题翻译：原子吸收光谱样品的电热原子荧光
公开(公告)号：US5194914A
公开(公告)日：1993-03-16
申请号：US475585
申请日：1990-02-06
申请人： Rolf Tamm , Gunther Rodel
发明人： Rolf Tamm , Gunther Rodel
IPC分类号： F27B17/02 , F27D11/02 , G01N21/31 , G01N21/74
CPC分类号： F27D11/02 , G01N21/74
摘要： A tubular furnace having an inner body connecting by an integral radially extending web. The web is positioned on the side of the tubular furnace so that a sample placed in the inner body and resting in the bottom thereof will not be heated by the web. Other embodiments illustrate the web positioned at different axial locations.
摘要翻译：一种管式炉，其具有通过一体的径向延伸的纤维网连接的内部主体。纸幅位于管状炉的侧面，使得放置在内部主体中并搁置在其底部的样品将不被纸幅加热。其它实施方案说明了位于不同轴向位置的纤维网。

2. 发明授权

US5594547A Multielement atomic absorption spectrometer and measurement method using such an atomic absorption spectrometer 失效
标题翻译：多元原子吸收光谱仪和使用这种原子吸收光谱仪的测量方法
公开(公告)号：US5594547A
公开(公告)日：1997-01-14
申请号：US404017
申请日：1995-03-14
申请人： Gunther Rodel , Bernhard Radziuk , Michael Zeiher , Herbert Stenz
发明人： Gunther Rodel , Bernhard Radziuk , Michael Zeiher , Herbert Stenz
IPC分类号： G01J3/42 , G01N21/31 , G01J3/30 , G01N21/74
CPC分类号： G01J3/42
摘要： The invention relates to a multielement atomic absorption spectrometer for simultaneously performing measurements for determining both one element and a plurality of elements under optimum conditions. The atomic absorption spectrometer comprises at least two lamps respectively emitting lines of at least one analyte element, a furnace heating the analyte sample into its atomized state, at least one optical dispersion element having an entrance slit arranged upstream thereof, detector elements, as well as means for passing radiation emanating from the lamps through the furnace, through the entrance slit and the dispersion element to the detector elements, and measuring means. The spectrometer is characterized in that there are provided replaceable optical reflection means which can selectively be moved into the optical path of the lamps in such a manner that the radiation emanating from one, two or a plurality of lamps can be passed through the furnace at the same time, that the dispersion element for producing a two-dimensional dispersion spectrum comprises an echelle grating and a dispersion prism, and that the detector elements are formed by semiconductor photodiodes arranged in one plane. The invention includes a measurement method for further increasing the accuracy of measurements regarding the measurement of one element and the simultaneous measurement of a plurality of elements.
摘要翻译：本发明涉及一种多元素原子吸收光谱仪，用于在最佳条件下同时进行测量以确定一个元件和多个元件。原子吸收光谱仪包括分别发射至少一种分析物元素的管道的至少两个灯，将分析物样品加热至其雾化状态的炉子，至少一个具有设置在其上游的入口狭缝的光学色散元件，检测器元件，以及用于将从灯发出的辐射通过炉，通过入口狭缝和分散元件传递到检测器元件的测量装置。光谱仪的特征在于，提供了可更换的光学反射装置，其可以选择性地移动到灯的光路中，使得从一个，两个或多个灯发出的辐射可以在同时，用于产生二维色散谱的色散元件包括梯形光栅和分散棱镜，并且检测器元件由布置在一个平面中的半导体光电二极管形成。本发明包括用于进一步增加关于一个元件的测量和多个元件的同时测量的测量精度的测量方法。

3. 发明授权

US5118187A Furnace for the electro-thermal atomization of samples for spectroscopical purposes 失效
标题翻译：用于光谱目的的用于电热雾化样品的炉
公开(公告)号：US5118187A
公开(公告)日：1992-06-02
申请号：US556050
申请日：1990-07-20
申请人： Rolf Tamm , Gunther Rodel
发明人： Rolf Tamm , Gunther Rodel
IPC分类号： G01N21/74
CPC分类号： G01N21/74
摘要： The manufacturing of a furnace for electro-thermal atomization of samples for spectroscopical purposes having a cavity for the accommodation of sample is simplified and improved. To this end, the furnace consists of two halves which are joined along a separating plane intersecting the cavity. The furnace is made of graphite and provided with a layer of pyrolytic graphite. A platform for the accommodation of the sample is integral with one of the halves. A method for the production of such a furnace comprises the method steps: (a) producing two blank parts which engage each other with planar surfaces; (b) machining the two blank parts in common so that a cavity intersected by the plane of the planar surfaces is generated and each of the blank parts forms one half of the furnace; (c) separating the two halves of the furnace which were produced in this way; (d) coating the halves of the furnace separately, the inner surfaces of the cavity forming outer surfaces of each of the two halves of the furnace; and (e) joining the halves of the furnace, generated in this way, to a furnace. There is also a method described for decreasing the refuse in the manufacturing of the furnaces.
摘要翻译：用于光谱目的的用于电热雾化用于具有用于容纳样品的空腔的用于光学目的的炉的制造被简化和改进。为此，炉子由沿着与腔体相交的分离平面连接的两个半部组成。该炉由石墨制成，并具有一层热解石墨。一个适合样品的平台是其中一个的一部分。制造这种炉子的方法包括以下方法步骤：（a）制备两个彼此相互接合的坯料部分，（b）共同加工两个坯件，使得产生与平面的平面相交的空腔，并且每个坯件形成炉的一半; （c）分离以这种方式生产的炉子的两半; （d）分别涂覆炉子的一半，空腔的内表面形成炉的两半的每一个的外表面; 和（e）将以这种方式产生的炉子的一半连接到炉子。还有一种描述用于减少炉子制造中的垃圾的方法。

4. 发明授权

US5087123A Atomic emission spectrometer with background compensation 失效
标题翻译：具有背景补偿的原子发射光谱仪
公开(公告)号：US5087123A
公开(公告)日：1992-02-11
申请号：US526779
申请日：1990-05-17
申请人： Edgar Gerlacher , Carl G. Dencks , Uwe Gunther , Gunther Rodel
发明人： Edgar Gerlacher , Carl G. Dencks , Uwe Gunther , Gunther Rodel
IPC分类号： G01J3/12 , G01J3/18 , G01J3/28 , G01J3/36 , G01J3/443 , G01N21/73 , G01N21/74
CPC分类号： G01J3/1809 , G01J3/443 , G01J2003/1208 , G01J2003/2869 , G01J3/36 , G01N21/73 , G01N21/74
摘要： A method of and a device for multi-element measurement of elements in a sample with correction for background emission. The method starts with atomizing a sample and then exciting the transformed atoms to emit light containing characteristic spectral lines for each element, followed by generating a spectrum of spectral lines characteristic of the elements, followed by measuring the intensity of selected spectral lines falling within a predetermined measuring range without changing their intensity. The next steps are sensing the background emission adjacent the selected spectral lines simultaneously with measuring the intensity of selected spectral lines and determining the concentration of each element from the measured intensity of the corresponding spectral line and sensed background emission.
摘要翻译：用于多元素测量样本中的元素的方法和装置，其具有用于背景发射的校正。该方法开始于对样品进行雾化，然后激发转化的原子以发射含有每个元素的特征谱线的光，随后产生元素特征谱带的频谱，随后测量落在预定的范围内的所选谱线的强度测量范围而不改变它们的强度。接下来的步骤是通过测量所选谱线的强度同时测量与所选谱线相邻的背景发射，并从相应光谱线的测量强度和感测到的背景辐射确定每个元素的浓度。

5. 发明授权

US5002390A Atomic emission spectrometer for simultaneous multi-element measurement of elements in a sample 失效
标题翻译：用于同时多元素测量样品中元素的原子发射光谱仪
公开(公告)号：US5002390A
公开(公告)日：1991-03-26
申请号：US335077
申请日：1989-04-07
申请人： Edgar Gerlacher , Carl G. Dencks , Uwe Gunther , Gunther Rodel
发明人： Edgar Gerlacher , Carl G. Dencks , Uwe Gunther , Gunther Rodel
IPC分类号： G01J3/443 , G01J3/36 , G01N21/73
CPC分类号： G01J3/36 , G01J3/443
摘要： An atomic emission spectrometer for multi-element measurement of elements in a sample comprises an apparatus to atomize the sample and to excite the atoms for emitting characteristic spectral lines, a dispersion device which generates a spectrum of the light emitted by the atoms in a focal plane, and a plurality of semiconductor photodetectors, each of which is exposed to one of said characteristic spectral lines. A plurality of semiconductor photodetectors which are exposed to different spectral lines of different intensities of the line spectrum emitted by the atoms of the respective element are utilized so as to achieve a sufficiently large dynamic range for each element to be measured. For measuring each element, an evaluating circuit is arranged to select one semiconductor photodetector for which the intensity of the associated spectral line lies within a part of the measuring range of the semiconductor photodetector which is as favorable as possible.
摘要翻译：用于样品中元素多元素测量的原子发射光谱仪包括：雾化样品并激发用于发射特征谱线的原子的装置;产生由焦平面中的原子发射的光的光谱的分散装置以及多个半导体光电检测器，其中的每一个都暴露于所述特征谱线之一。利用多个半导体光电检测器，其暴露于由各个元件的原子发射的线谱的不同强度的不同谱线，以便为每个要测量的元件获得足够大的动态范围。为了测量每个元件，评估电路被布置为选择一个半导体光电检测器，其中相关联的谱线的强度位于尽可能有利的半导体光电探测器的测量范围的一部分内。

6. 发明授权

US5066123A Device for electrothermal atomizing of samples for spectroscopic purposes 失效
标题翻译：用于电光源用于光谱目的的样品的设备
公开(公告)号：US5066123A
公开(公告)日：1991-11-19
申请号：US481834
申请日：1990-02-16
申请人： Rolf Tamm , Gunther Rodel , Erich Stengele
发明人： Rolf Tamm , Gunther Rodel , Erich Stengele
IPC分类号： G01N1/00 , G01N21/31 , G01N21/74
CPC分类号： G01N21/74 , G01N1/10
摘要： A device for electrothermal atomization of samples for spectroscopic purposes with a furnace body made of graphite, designed such that electrical current can be passed through, and a pot-shaped sample receptacle which is separated from the furnace body and projects into a lateral aperture of the furnace body comprises a driving device by which the sample receptacle is movable into and out of thermal contact with the furnace body. The driving device together with the heating current of the furnace body is controlled by a controlling device such that the sample receptacle engages the furnace body during a drying and decomposing step and thereafter, is raised from the furnace body by the driving device. Thereafter, with raised sample receptacle, the furnace body is heated to atomization temperature until a temperature stabilization is achieved and, finally, the sample receptacle is again moved into contact with the furnace body.
摘要翻译：用于光谱雾化用于光谱目的的装置，用石墨制成的炉体，设计成能够通过电流，以及从炉体分离并突出到炉体的侧向孔中的罐形样品容器炉体包括驱动装置，通过该驱动装置，样品容器可移动进入和离开与炉体的热接触。驱动装置与炉体的加热电流一起由控制装置控制，使得样品容器在干燥和分解步骤期间与炉体接合，然后通过驱动装置从炉体升起。此后，用升高的样品容器将炉体加热至雾化温度，直到达到温度稳定，最后，样品容器再次与炉体接触。

7. 发明授权

US5005976A Electrothermal atomization of a sample for spectroscopic purposes 失效
标题翻译：用于光谱目的的样品的电热雾化
公开(公告)号：US5005976A
公开(公告)日：1991-04-09
申请号：US377992
申请日：1989-07-11
申请人： Rolf Tamm , Bernhard Huber , Gunther Rodel , Erich Stengele
发明人： Rolf Tamm , Bernhard Huber , Gunther Rodel , Erich Stengele
IPC分类号： G01N21/31 , G01N21/74
CPC分类号： G01N21/74
摘要： A device for electrothermal atomization of a sample for spectroscopic purposes comprises a furnace (10) which is held between two contacts (54, 56). The contacts (54, 56) surround the furnace (10 ) and form a cavity (58) with an insulating gap (88) being formed between the contacts (54, 56). This gap (88) is closed by a seal (142) made of ceramic felt so that inert gas passed into the cavity (58) emerges only through a bore (14) of the furnace (10) and sample inlet ports (116, 120). Thereby, the inert gas consumption is reduced well-defined flow conditions also result for the inert gas in the cavity (58) which expands when the furnace (10) is heated.
摘要翻译：用于光谱目的的用于电热雾化样品的装置包括保持在两个触点（54,56）之间的炉（10）。触点（54,56）围绕炉子（10）并形成空腔（58），在触头（54,56）之间形成绝缘间隙（88）。这个间隙（88）被由陶瓷毡制成的密封件（142）封闭，使得进入空腔（58）的惰性气体仅通过炉（10）的孔（14）和样品入口（116,120））。因此，减少了惰性气体消耗，明确的流动条件也导致当炉子（10）被加热时膨胀的空腔（58）中的惰性气体。

8. 发明授权

US4968141A Electrothermal atomization furnace 失效
标题翻译：电热雾化炉
公开(公告)号：US4968141A
公开(公告)日：1990-11-06
申请号：US304993
申请日：1989-02-01
申请人： Rolf Tamm , Gunther Rodel
发明人： Rolf Tamm , Gunther Rodel
IPC分类号： G01N21/31 , G01N21/74 , H05B3/02 , H05B3/06
CPC分类号： H05B3/06 , G01N21/74
摘要： An electrothermal atomization furnace for atomizing samples for analysis by atomic absorption spectoscopy comprising a tubular furnace body (36) which is provided on both sides with longitudinal contact ribs (38, 40) and cylindrical contact pieces (18, 20) integral with these contact ribs. In one embodiment, bores (49, 50, 52, 54) are provided in the contact ribs (38, 40) parallel to the furnace body (36) in order to reduce the cross-section for the current supply along the center area of the furnace body (36). These bores are intersected by transverse bores (56, 58, 60 and 62, 64, 66, respectively) and communicate with inert gas passages (68, 70) so that the bores contribute to reduce the cross-section as well as to distribute the inert gas. In another embodiment, grooves are provided in the planar surfaces instead of the bores. An equal temperature distribution along the furnace body (36) is achieved. A hollow, generally semicylindrical inner body (76) with half of an internally threaded portion (78) is arranged in the furnace body (36).
摘要翻译：一种用于通过原子吸收分光镜分析的用于雾化样品的电热雾化炉，包括：管状炉体（36），其在两侧设置有纵向接触肋（38,40）和与这些接触肋成一体的圆柱形接触片（18,20）。在一个实施例中，孔（49,50,52,54）设置在与炉体（36）平行的接触肋（38,40）中，以便沿着炉体（36）的中心区域减小电流供应的横截面炉体（36）。这些孔与横向孔（分别为56,58,60,62,64,66）相交并与惰性气体通道（68,70）连通，使得孔有助于减小横截面以及分布惰性气体。在另一个实施例中，凹槽设置在平面表面而不是孔中。实现了沿着炉体（36）的相等的温度分布。具有一半内螺纹部分（78）的中空的大致半圆柱形内体（76）设置在炉体（36）中。

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