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1. 发明授权

US5294667A Preparation of thermoplastic molding materials based on pulverulent polyphenylene ethers and aromatic vinyl polymers 失效
标题翻译：基于粉状聚亚苯基醚和芳族乙烯基聚合物制备热塑性成型材料
公开(公告)号：US5294667A
公开(公告)日：1994-03-15
申请号：US994635
申请日：1992-12-21
申请人： Robert Weiss , Axel Gottschalk , Klaus Muehlbach , Carola Hedtmann-Rein , Robert Heinz
发明人： Robert Weiss , Axel Gottschalk , Klaus Muehlbach , Carola Hedtmann-Rein , Robert Heinz
IPC分类号： C08G65/46 , C08J3/00 , C08L25/02 , C08L71/12 , C08L25/04
CPC分类号： C08L25/02 , C08G65/46 , C08J3/005 , C08L71/123 , C08L71/12
摘要： In order to prepare thermoplastic molding materials from pulverulent polyphenylene ethers and aromatic vinyl polymers by melt extrusion, the pulverulent polyphenylene ether is first of all compacted and/or sintered under pressure and if necessary with the addition of heat, preferably under a pressure corresponding to a nip pressure of from 1 to 100 kN/cm, to form a porous compact. The compact is then fed in the form of agglomerates having a particle size of from about 0.5 mm to about 20 mm into an extruder or the like, mixed with the aromatic vinyl polymer and if desired further components, and melted. In this way the proportion of the fines in the polyphenylene ether is considerably reduced, with the result that there is virtually no further danger of dust explosions. Further advantages include improved ease of metering and reduced electrostatic charge of the agglomerates. The extruded molding materials have good mechanical properties and also high thermal stability.
摘要翻译：为了通过熔融挤出从粉状聚亚苯基醚和芳族乙烯基聚合物制备热塑性成型材料，粉状聚苯醚首先在压力下压实和/或烧结，如果需要加热，优选在相当于压区压力为1至100kN / cm，以形成多孔压块。然后将压块以粒度为约0.5mm至约20mm的附聚物的形式进料到挤出机等中，与芳族乙烯基聚合物混合并且如果需要，进一步熔融。以这种方式，聚苯醚中的细粉比例大大降低，实际上没有进一步的灰尘爆炸危险。另外的优点包括提高计量的容易性和降低凝聚体的静电电荷。挤出成型材料具有良好的机械性能和高的热稳定性。

2. 发明授权

US5130356A Molding for optical purposes 失效
标题翻译：模具用于光学目的
公开(公告)号：US5130356A
公开(公告)日：1992-07-14
申请号：US473453
申请日：1990-02-01
申请人： Karl-Heinz Feuerherd , Carola Hedtmann-Rein , Ludger Leber
发明人： Karl-Heinz Feuerherd , Carola Hedtmann-Rein , Ludger Leber
IPC分类号： B41M5/26 , B29D11/00 , C07C39/15 , C07C50/08 , C07C50/24 , C07C50/30 , C07C211/03 , C07C215/78 , C07C215/80 , C07C225/20 , C07C225/28 , C07C305/24 , C07D295/02 , C07D295/027 , C07D295/096 , C07D295/112 , C07D295/116 , C08K5/08 , C08K5/13 , C08K5/42 , C08L25/04 , C08L25/06 , C08L25/16 , C08L71/00 , C08L71/08 , C08L71/12 , G02B1/04 , G11B7/24 , G11B7/253 , G11B11/10 , G11B11/105
CPC分类号： C07D295/027 , C07C211/03 , C07C215/78 , C07C215/80 , C07C225/28 , C07C305/24 , C07C39/15 , C07C50/08 , C07C50/24 , C07C50/30 , C07D295/096 , C07D295/112 , C07D295/116 , C08K5/08 , C08K5/13 , C08K5/42 , C08L25/06 , C08L71/123 , G11B11/10582 , G11B11/10584 , G11B11/10586 , G11B7/24 , G11B7/253 , C07C2101/14 , C08L25/16 , C08L71/12 , G11B7/24038 , Y10S525/905
摘要： A novel, optically transparent, isotropic molding for optical purposes which is free of orientation birefringence consists of a mixture of polyphenylene ethers, vinylaromatic polymers and additives. The novel molding contains traces of novel diphenoquinone and/or diphenohydroquinone derivatives as additives and may also contain novel ammonium salts of sulfuric acid half esters of diphenohydroquinones as further additives. The novel molding has a yellowness index (YI) of from 40 to 90. It can be produced in a simple manner by injection molding processes. The novel molding in the form of a circular disk having a central hole is very useful as a dimensionally stable substrate of audio compact disks (CD), audiovisual compact disks (CDV), laser-optical computer disks and magneto-optical computer disks, and data media of this type which contain these novel dimensionally stable substrates have particularly advantageous performance characteristics.
摘要翻译：用于光学目的的新型光学透明的各向同性模制物，其不含取向双折射，由聚苯醚，乙烯基芳族聚合物和添加剂的混合物组成。该新型成型物含有痕量的新颖的联苯醌和/或二苯氢醌衍生物作为添加剂，并且还可以含有二苯氢醌的硫酸半酯的新型铵盐作为其它添加剂。新型成型品的黄色指数（YI）为40〜90。可以通过注塑成型工艺简单地生产。具有中心孔的圆盘形式的新颖模制作为音频光盘（CD），视听光盘（CDV），激光光学计算机盘和磁光计算机盘的尺寸稳定的基板是非常有用的，以及包含这些新颖的尺寸稳定的基板的这种数据介质具有特别有利的性能特性。

3. 发明授权

US5237039A Preparation of polyphenylene ethers in the presence of defoamer 失效
标题翻译：在存在缺陷的情况下制备聚苯乙烯
公开(公告)号：US5237039A
公开(公告)日：1993-08-17
申请号：US876163
申请日：1992-04-30
申请人： Doris Zeltner , Peter Steieri , Heike Feldman , Klaus Muehlbach , Carola Hedtmann-Rein , Bernhard Czauderna , Karl Hennig
发明人： Doris Zeltner , Peter Steieri , Heike Feldman , Klaus Muehlbach , Carola Hedtmann-Rein , Bernhard Czauderna , Karl Hennig
IPC分类号： C08G65/40 , C08G65/44
CPC分类号： C08G65/44
摘要： Polyphenylene ethers are prepared from monohydric phenols by oxidative coupling with oxygen-containing gases in the presence of an oxidation catalyst in an organic solvent by carrying out the polycondensation in the presence of a defoamer.
摘要翻译：通过在有机溶剂中的氧化催化剂存在下，通过在消泡剂的存在下进行缩聚，通过与含氧气体的氧化偶联，由一元酚制备聚苯醚。

4. 发明授权

US5171825A Preparation of polyphenylene ethers 失效
标题翻译：聚苯乙烯的制备
公开(公告)号：US5171825A
公开(公告)日：1992-12-15
申请号：US695385
申请日：1991-05-03
申请人： Carola Hedtmann-Rein , Bernhard Czauderna , Martina von Deessen , Karl Hennig
发明人： Carola Hedtmann-Rein , Bernhard Czauderna , Martina von Deessen , Karl Hennig
IPC分类号： C08G65/38 , C08G65/44
CPC分类号： C08G65/44
摘要： A process for preparing polyphenylene ethers from monohydric phenols which have alkyl substituents in both ortho positions and possibly also in one meta position but not in the para position, by oxidative coupling with oxygen-containing gases in the presence of an oxidation catalyst and of an electrically conducting compound which counteracts the electrostatic charge in the reaction mixture, in organic solution, comprises using as electrically conducting compound a salt of a carboxamide derivative of the formula I ##STR1## or mixtures of such salts, where R.sup.1 is a saturated or singly or multiply unsaturated aliphatic group which can have a terminal phenyl group and which contains a total of 8-30 carbon atoms, it also being possible for these carbon atoms to be interrupted by isolated oxygen atoms,R.sup.2 is hydrogen or C.sub.1 -C.sub.4 -alkyl,A is an aliphatic, araliphatic or cycloaliphatic or aromatic bridge of up to 10 carbon atoms,n and m are each 1 to 3,Q.sup..sym. is ammonium, an alkali metal cation or the equivalent of an alkaline earth metal cation or a cation of a metal of groups IVb to VIIb of the periodic table.
摘要翻译：在氧化催化剂存在下，通过与含氧气体的氧化偶联和电化学反应，由一元酚制备聚苯醚的方法，它们在邻位和可能还在一个间位而不是在对位具有烷基取代基在有机溶液中抵抗反应混合物中的静电荷的导电化合物包括使用式I的羧酰胺衍生物或其混合物作为导电化合物的盐或其混合物，其中R1是饱和或单独或可以具有末端苯基并且含有总共8-30个碳原子的多重不饱和脂族基团，这些碳原子也可以被分离的氧原子中断，R2是氢或C1-C4-烷基，A 是至多10个碳原子的脂族，芳脂或脂环族或芳族桥，n和m各自为1至3，Q（+）为铵，碱金属阳离子或当量的碱金属阳离子或元素周期表IVb至VIIb族金属的阳离子。

5. 发明授权

US5296563A Preparation of polyphenylene ether/polyamide molding materials 失效
标题翻译：聚苯醚/聚酰胺成型材料的制备
公开(公告)号：US5296563A
公开(公告)日：1994-03-22
申请号：US994255
申请日：1992-12-21
申请人： Axel Gottschalk , Robert Weiss , Klaus Muehlbach , Carola Hedtmann-Rein , Robert Heinz
发明人： Axel Gottschalk , Robert Weiss , Klaus Muehlbach , Carola Hedtmann-Rein , Robert Heinz
IPC分类号： C08L71/12 , C08L77/00 , C08G65/48 , C08G71/04 , C08G77/10
CPC分类号： C08L77/00 , C08L71/12 , C08L71/126
摘要： In order to prepare thermoplastic molding materials ofA) 5-95% by weight of a modified polyphenylene ether,B) 5 to 95% by weight of a thermoplastic polyamide,C) 0 to 25% by weight of an impact-modifying rubber, andD) 0 to 50% by weight of auxiliaries and/or additives,the components A and B and if necessary the components C and D are fed individually at one or more points into an extruder, mixed with one another, and melted. The component A present in a pulverulent consistency is compacted and/or sintered under pressure and if necessary with the addition of heat, preferably at a pressure corresponding to a nip pressure of 1 to 100 kn/cm to form a porous compact before it is fed into the extruder. The compact is then modified and added as granules to the feed zone of the extruder. In this way the proportion of the fines in the polyphenylene ether is considerably reduced, so that there is virtually no further danger of dust explosions. Further advantages include an improved ease of metering and reduced electrostatic charge.
摘要翻译：为了制备A）5-95重量％的改性聚苯醚的热塑性成型材料，B）5-95重量％的热塑性聚酰胺，C）0-25重量％的抗冲击改性橡胶，和D）0至50重量％的助剂和/或添加剂，组分A和B以及组分C和D如果需要，在一个或多个点分别进料到彼此混合并熔化的挤出机中。存在粉碎稠度的组分A在压力下压实和/或烧结，如果需要加热，优选在相当于1至100kn / cm的压区压力的压力下形成多孔压块，然后再进料进入挤出机。然后将压块改性并作为颗粒加入挤出机的进料区。以这种方式，聚苯醚中细粉的比例大大降低，实际上没有进一步的粉尘爆炸危险。另外的优点包括改进的计量方便性和减少的静电电荷。

6. 发明授权

US5036146A High temperature resistant polysulfone-polyimide block copolycondensates and preparation thereof by melt condensation 失效
标题翻译：耐高温聚砜 - 聚酰亚胺嵌段共缩聚并通过熔融缩合制备
公开(公告)号：US5036146A
公开(公告)日：1991-07-30
申请号：US451233
申请日：1989-12-15
申请人： Carola Hedtmann-Rein , Gerhard Heinz
发明人： Carola Hedtmann-Rein , Gerhard Heinz
IPC分类号： C08G73/10 , C08G75/20 , C08G81/00
CPC分类号： C08G73/1082 , C08G73/10 , C08G73/1046 , C08G73/1064 , C08G75/20 , C08G81/00 , Y10S525/906
摘要： High temperature resistant polysulfone-polyimide block copolycondensates suitable for example for producing shaped articles are composed of at least one polyarylene ether sulfone block comprising units of the structure ##STR1## and at least one polyimide block comprising units of the structure ##STR2## where R.sup.1 and R.sup.2 are identical or different and each is hydrogen or methyl and X is methylene or 1,2-ethylene, and are prepared by condensing conventionally obtained amine-terminated polyarylene ether sulfone blocks with polyimide blocks in the melt.
摘要翻译：适合于例如用于生产成形制品的耐高温聚砜 - 聚酰亚胺嵌段共聚缩合物由至少一种包含结构单元（I）和/或图像（II）的聚亚芳基醚砜嵌段和至少一种聚酰亚胺其包含结构单元（III）和/或其中R 1和R 2相同或不同并且各自为氢或甲基且X为亚甲基或1,2-亚乙基，并且由将常规获得的胺封端的聚亚芳基醚砜嵌段与熔融体中的聚酰亚胺嵌段缩合。

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