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1. 发明申请

WO2008053421A3 REMOVAL OF HYDROGEN CYANIDE FROM SYNTHESIS GAS 审中-公开
标题翻译：从合成气中除去氢氰化物
公开(公告)号：WO2008053421A3
公开(公告)日：2008-06-26
申请号：PCT/IB2007054378
申请日：2007-10-29
申请人： SASOL TECH PTY LTD , VAN DYK BRAAM , MARRIOTT JOHN , PILLAY BAVANETHAN , VAN DER WESTHUIZEN HENDRIK JOH , COMBRINK RONEL , PHILLIPS TREVOR DAVID , VENTER DENISE LOUISETTE , STEYNBERG ANDRE PETER
发明人： VAN DYK BRAAM , MARRIOTT JOHN , PILLAY BAVANETHAN , VAN DER WESTHUIZEN HENDRIK JOH , COMBRINK RONEL , PHILLIPS TREVOR DAVID , VENTER DENISE LOUISETTE , STEYNBERG ANDRE PETER
IPC分类号： B01D53/79 , C10K1/10
CPC分类号： B01D53/78 , B01D53/54 , B01D2251/60 , B01D2257/408 , C10K1/105 , C10K1/106 , C10K1/108
摘要： A process (10) for at least partially removing hydrogen cyanide from synthesis gas includes feeding a synthesis gas (30) containing hydrogen cyanide to a gas-liquid contacting stage (18) and, in the gas-liquid contacting stage (18), contacting the synthesis gas with an aqueous washing solution (36) comprising at least one dissolved metal salt, with metal cations of the metal salt being capable of forming metal cyanide complexes and/or metal cyanide precipitates, and weak acid anions of the metal salt serving to buffer the pH of the washing solution in a range between 6 and 10. Hydrogen cyanide is washed from the synthesis gas by the washing solution to form a treated synthesis gas (38) and a spent washing solution (40). From time to time or continuously, at least a portion of the spent washing solution is withdrawn from the gas- liquid contacting stage. The treated synthesis gas (38) is also withdrawn from the gas- liquid contacting stage.
摘要翻译：用于从合成气中至少部分去除氰化氢的方法（10）包括将含有氰化氢的合成气（30）进料到气 - 液接触级（18）中，并且在气 - 液接触级（18）中，所述合成气与包含至少一种溶解的金属盐的金属盐的金属阳离子和能够形成金属氰化物络合物和/或金属氰化物沉淀物的含水洗涤溶液（36）以及金属盐的弱酸性阴离子用作将洗涤溶液的pH缓冲在6至10之间的范围内。通过洗涤溶液从合成气中洗涤氰化物以形成处理过的合成气（38）和废洗涤溶液（40）。不时或连续地，至少一部分废洗涤溶液从气 - 液接触阶段中排出。经处理的合成气（38）也从气 - 液接触阶段排出。

2. 发明申请

WO2013030448A3 A TWO-STAGE GAS WASHING METHOD APPLYING SULFIDE PRECIPITATION AND ALKALINE ABSORPTION 审中-公开
标题翻译：应用硫化物降解和碱吸收的两阶段气体洗涤方法
公开(公告)号：WO2013030448A3
公开(公告)日：2013-07-18
申请号：PCT/FI2012050816
申请日：2012-08-28
申请人： NESTE OIL OYJ , WAHLSTROEM JAN , AITTAMAA JUHANI , EILOS ISTO , KESKINEN KARI I , KOSKINEN JUKKA , TIITTA MARJA , VUORI HELI
发明人： WAHLSTROEM JAN , AITTAMAA JUHANI , EILOS ISTO , KESKINEN KARI I , KOSKINEN JUKKA , TIITTA MARJA , VUORI HELI
IPC分类号： B01D53/52 , C10G2/00 , C10K1/00 , C10K1/10 , C10K1/12 , C10K3/00 , C10K3/04
CPC分类号： B01D53/526 , B01D2251/404 , B01D2257/304 , B01D2257/504 , C10G2/30 , C10G2300/1011 , C10G2300/1022 , C10G2300/207 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/08 , C10K1/105 , C10K1/106 , C10K1/108 , C10K1/12 , C10K1/122 , C10K3/006 , C10K3/04 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： The present description is related to the field of hydrocarbon production by gasification of carbonaceous material. It provides a two-stage gas washing method as a part of gas refining. More specifically it discloses a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. It introduces a use of a novel combination of two chemical wash approaches for this application. As a specific application, this process is utilized as a part of biomass to liquid (BTL) process.
摘要翻译：本说明书涉及通过碳质材料的气化生产烃类的领域。它作为气体精炼的一部分提供了两阶段的气体清洗方法。更具体地，其公开了从气化产生的合成气中除去硫化氢和二氧化碳的方法。它引入了两种化学洗涤方法的新颖组合在本申请中的应用。作为具体应用，该方法被用作生物质与液体（BTL）过程的一部分。

3. 发明申请

WO2013030448A2 A TWO-STAGE GAS WASHING METHOD APPLYING SULFIDE PRECIPITATION AND ALKALINE ABSORPTION 审中-公开
标题翻译：应用硫化物沉淀和碱吸收的两段式气体洗涤方法
公开(公告)号：WO2013030448A2
公开(公告)日：2013-03-07
申请号：PCT/FI2012/050816
申请日：2012-08-28
申请人： NESTE OIL OYJ , WAHLSTRÖM, Jan , AITTAMAA, Juhani , EILOS, Isto , KESKINEN, Kari I. , KOSKINEN, Jukka , TIITTA, Marja , VUORI, Heli
发明人： WAHLSTRÖM, Jan , AITTAMAA, Juhani , EILOS, Isto , KESKINEN, Kari I. , KOSKINEN, Jukka , TIITTA, Marja , VUORI, Heli
IPC分类号： C10K1/10
CPC分类号： B01D53/526 , B01D2251/404 , B01D2257/304 , B01D2257/504 , C10G2/30 , C10G2300/1011 , C10G2300/1022 , C10G2300/207 , C10J2300/0916 , C10K1/004 , C10K1/005 , C10K1/08 , C10K1/105 , C10K1/106 , C10K1/108 , C10K1/12 , C10K1/122 , C10K3/006 , C10K3/04 , Y02E50/32 , Y02P20/145 , Y02P20/152 , Y02P30/20
摘要： The present description is related to the field of hydrocarbon production by gasification of carbonaceous material. It provides a two-stage gas washing method as a part of gas refining. More specifically it discloses a method for hydrogen sulfide and carbon dioxide removal from synthesis gas produced by gasification. It introduces a use of a novel combination of two chemical wash approaches for this application. As a specific application, this process is utilized as a part of biomass to liquid (BTL) process.
摘要翻译：本说明书涉及通过碳质材料的气化生产碳氢化合物的领域。它提供了一种两段式气体清洗方法作为气体精炼的一部分。更具体地说，它公开了一种从气化产生的合成气中除去硫化氢和二氧化碳的方法。它介绍了这种应用中两种化学清洗方式的新型组合的用法。作为具体应用，这个过程被用作生物质液化（BTL）过程的一部分。

4. 发明申请

WO2008053421A2 REMOVAL OF HYDROGEN CYANIDE FROM SYNTHESIS GAS 审中-公开
标题翻译：合成气脱除氰化氢
公开(公告)号：WO2008053421A2
公开(公告)日：2008-05-08
申请号：PCT/IB2007/054378
申请日：2007-10-29
申请人： SASOL TECHNOLOGY (PROPRIETARY) LIMITED , VAN DYK, Braam , MARRIOTT, John , PILLAY, Bavanethan , VAN DER WESTHUIZEN, Hendrik, Johannes , COMBRINK, Ronél , PHILLIPS, Trevor, David , VENTER, Denise, Louisette , STEYNBERG, André, Peter
发明人： VAN DYK, Braam , MARRIOTT, John , PILLAY, Bavanethan , VAN DER WESTHUIZEN, Hendrik, Johannes , COMBRINK, Ronél , PHILLIPS, Trevor, David , VENTER, Denise, Louisette , STEYNBERG, André, Peter
IPC分类号： B01D53/79 , C10K1/10
CPC分类号： B01D53/78 , B01D53/54 , B01D2251/60 , B01D2257/408 , C10K1/105 , C10K1/106 , C10K1/108
摘要： A process (10) for at least partially removing hydrogen cyanide from synthesis gas includes feeding a synthesis gas (30) containing hydrogen cyanide to a gas-liquid contacting stage (18) and, in the gas-liquid contacting stage (18), contacting the synthesis gas with an aqueous washing solution (36) comprising at least one dissolved metal salt, with metal cations of the metal salt being capable of forming metal cyanide complexes and/or metal cyanide precipitates, and weak acid anions of the metal salt serving to buffer the pH of the washing solution in a range between 6 and 10. Hydrogen cyanide is washed from the synthesis gas by the washing solution to form a treated synthesis gas (38) and a spent washing solution (40). From time to time or continuously, at least a portion of the spent washing solution is withdrawn from the gas- liquid contacting stage. The treated synthesis gas (38) is also withdrawn from the gas- liquid contacting stage.
摘要翻译：用于从合成气中至少部分地除去氰化氢的方法（10）包括将含有氰化氢的合成气（30）供给到气液接触阶段（18），并且在气 - 液接触阶段（18），使合成气与包含至少一种溶解的金属盐的水性洗涤溶液（36）接触，金属盐的金属阳离子能够形成金属氰化物络合物和/或金属氰化物沉淀物，并且弱金属盐的酸阴离子用来缓冲洗涤溶液的pH在6和10之间的范围内。用洗涤溶液从合成气中洗涤氰化氢，形成处理过的合成气（38）和用过的洗涤液（ 40）。不时或连续地，至少一部分用过的洗涤溶液从气液接触段中排出。处理过的合成气（38）也从气液接触段中排出。

5. 发明申请

WO99055804A1 GASIFICATION METHOD 审中-公开
标题翻译：气化方法
公开(公告)号：WO99055804A1
公开(公告)日：1999-11-04
申请号：PCT/JP1999/002099
申请日：1999-04-20
IPC分类号： C02F1/20 , C02F1/58 , C10K1/10 , C10K1/26 , C10K1/32 , C10K3/00 , B01D19/00 , C02F1/62 , C10K1/02
CPC分类号： C02F1/58 , C02F1/20 , C10K1/105 , C10K1/26 , C10K1/32
摘要： A method for removing a cyanide component by or in application of steam stripping while suppressing the formation of a nickel-cyanide complex. A mixture of a raw material and sulfur is fed to a gasification step (101) in a way such that the mixture has a sulfur content of 0.5 to 2.0 wt. % and is gasificated. The resultant crude gas is washed in a cooling/carbon washing step (102), wherein nickel sulfide or the like is preferentially formed in a drain water and the formation of a nickel-cyanide complex is suppressed. A cyanide component is emitted as HCN. Alternatively, to stripper (201), drain water is introduced from line (210), a strong acid from line (211) and steam from line (212). A nickel-cyanide complex contained in a drain water having a controlled pH of 2.0 to 6.0 is decomposed to a cyanide ion and a nickel ion. The cyanide ion is finally emitted as HCN from line (216), and a nickel ion is discharged from line (217) and treated as nickel hydroxide.
摘要翻译：一种在抑制氰化镍络合物的形成的同时通过蒸汽汽提除去氰化物成分或者应用蒸汽汽提的方法。将原料和硫的混合物以使得混合物的硫含量为0.5〜2.0重量％的方式进料至气化工序（101）。％并被气化。所得粗气体在冷却/碳清洗步骤（102）中洗涤，其中优选在排水中形成硫化镍等，并且抑制形成氰化镍络合物。氰化物成分以HCN的形式排放。或者，对于汽提器（201），从管线（210）引入排水，来自管线（211）的强酸和来自管线（212）的蒸汽。受控pH为2.0〜6.0的排水中含有的氰化镍络合物分解为氰离子和镍离子。氰化物离子最终作为HCN从管线（216）中排出，镍离子从管线（217）排出并作为氢氧化镍处理。

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