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1. 发明申请

WO2014003907A1 METALLOPHOSPHATE MOLECULAR SIEVES, METHOD OF PREPARATION AND USE 审中-公开
标题翻译：金属磷酸酯分子筛，制备和使用方法
公开(公告)号：WO2014003907A1
公开(公告)日：2014-01-03
申请号：PCT/US2013/041049
申请日：2013-05-15
申请人： UOP LLC
发明人： LEWIS, Gregory J. , KNIGHT, Lisa M. , JAKUBCZAK, Paulina , STANCZYK, Justin E.
IPC分类号： C01B39/54 , B01J29/85 , C01B37/08
CPC分类号： B01J29/85 , B01J29/83 , B01J29/84 , B01J2229/183 , C01B37/06 , C01B37/065 , C01B37/08 , C01B39/54
摘要： A new family of crystalline microporous metallophosphates designated AlPO-57 has been synthesized. These metallophosphates are represented by the empirical formula R + r M m n+ EP x Si y O z where R is an organoammonium cation such as the DEDMA + , M is a divalent framework metal such as an alkaline earth or transition metal, and E is a framework element such as aluminum or gallium. The microporous AlPO-57 compositions are characterized by a new unique ABC-6 net structure and have catalytic properties for carrying out various hydrocarbon conversion processes and separation properties for separating at least one component.
摘要翻译：已经合成了一系列名为AlPO-57的结晶微孔金属磷酸盐系列。这些金属磷酸盐由经验式R + rMm n + EPxSiyOz表示，其中R是有机铵阳离子，例如DEDMA +，M是二价骨架金属如碱土金属或过渡金属，E是骨架元素如铝或镓。微孔AlPO-57组合物的特征在于新的独特的ABC-6网状结构，并且具有用于进行各种烃转化方法和用于分离至少一种组分的分离性能的催化性质。

2. 发明申请

WO2008035374A3 MICROPOROUS CRYSTALLINE SILICOALUMINO/(METALLO) ALUMINOPHOSPHATE MOLECULAR SIEVE AND METHOD OF SYNTHESIS THEREOF 审中-公开
标题翻译：微孔结晶硅铝酸盐/（金属）铝磷酸盐分子筛及其合成方法
公开(公告)号：WO2008035374A3
公开(公告)日：2008-07-17
申请号：PCT/IN2007000302
申请日：2007-07-20
申请人： BHARAT PETROLEUM CORP LTD , PAI SHIVANAND , NEWALKAR BHARAT LAKSHMAN , CHOUDARY NETTEM VENKATESWARLU
发明人： PAI SHIVANAND , NEWALKAR BHARAT LAKSHMAN , CHOUDARY NETTEM VENKATESWARLU
IPC分类号： C01B39/54 , C01B37/04 , C01B37/06 , C01B37/08
CPC分类号： C01B39/54 , C01B37/04 , C01B37/06 , C01B37/065 , C01B37/08
摘要： The present invention discloses a novel microporous crystalline silicoalumino/(metallo)aluminophosphate molecular sieve framework (designated as BPC-1), having in its as-synthesized form, an X-ray diffraction pattern including the lines listed in Table 1, and method of its synthesis using 4-dimethylaminopyridine as organic templating agent in fluoride medium under microwave-hydrothermal conditions.
摘要翻译：本发明公开了一种新颖的微孔结晶硅铝酸盐/（金属）铝磷酸盐分子筛骨架（称为BPC-1），其具有其合成后的形式，包括表1中列出的线的X射线衍射图，以及其在微波 - 水热条件下使用4-二甲基氨基吡啶作为有机模板剂在氟化物介质中的合成。

3. 发明申请

WO01036328A1 METHOD FOR THE SYNTHESIS OF MOLECULAR SIEVES 审中-公开
标题翻译：合成分子筛的方法
公开(公告)号：WO01036328A1
公开(公告)日：2001-05-25
申请号：PCT/US2000/030319
申请日：2000-11-03
IPC分类号： B01J29/84 , B01J29/85 , C01B37/06 , C01B37/08
CPC分类号： B01J29/85 , B01J29/84 , C01B37/06 , C01B37/065 , C01B37/08 , Y10S423/30
摘要： The present invention provides a method for the synthesis of MeAPO molecular sieves which includes the following steps: providing a source of alumina, a source of phosphorus, water, and a template suitable for forming a MeAPO molecular sieve; providing a source of metal (Me)including metal particles, the metal particles measuring, in their largest dimension, equal to or less than five nanometers; providing a water soluble organic solvent capable of solubilizing the source of metal; forming a synthesis mixture from the source of alumina, the source of phosphorus, the water, the template, the source of metal, and the solvent; and forming a MeAPO molecular sieve from the synthesis mixture.
摘要翻译：本发明提供了一种合成MeAPO分子筛的方法，其包括以下步骤：提供氧化铝源，磷源，水和适于形成MeAPO分子筛的模板; 提供包括金属颗粒的金属（Me）源，金属颗粒在其最大尺寸上测量等于或小于5纳米; 提供能溶解金属源的水溶性有机溶剂; 从氧化铝源，磷源，水，模板，金属源和溶剂形成合成混合物; 并从合成混合物中形成MeAPO分子筛。

4. 发明申请

WO2008110528A1 METHOD FOR PREPARING METALLOALUMINOPHOSPHATE (MEAPO) MOLECULAR SIEVE 审中-公开
标题翻译：制备金属磷酸盐（MEAPO）分子筛的方法
公开(公告)号：WO2008110528A1
公开(公告)日：2008-09-18
申请号：PCT/EP2008/052813
申请日：2008-03-10
申请人： TOTAL PETROCHEMICALS RESEARCH FELUY , CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (CNRS) , VERMEIREN, Walter , NESTERENKO, Nikolai , PETITTO, Carolina , DI RENZO, Francesco , FAJULA, François
发明人： VERMEIREN, Walter , NESTERENKO, Nikolai , PETITTO, Carolina , DI RENZO, Francesco , FAJULA, François
IPC分类号： C01B37/08 , B01J29/85 , C07C1/20 , C07C1/26 , C07C1/32
CPC分类号： B01J29/84 , B01J29/85 , C01B37/06 , C01B37/08 , C07C1/20 , C07C1/26 , C07C1/322 , C07C2529/84 , C07C2529/85 , Y02P30/42 , C07C11/02
摘要： The present invention also relates to a method for preparing metalloaluminophosphate (MeAPO) molecular sieve said method comprising: a) forming a reaction mixture containing a texture influencing agent (TIA), an organic templating agent (TEMP), at least a reactive inorganic source of MeO 2 insoluble in the TIA, reactive sources of Al 2 O 3 and P 2 O 5 , b) crystallizing the above reaction mixture thus formed until crystals of the metalloaluminophosphate are formed, c) recovering a solid reaction product, d) washing it with water to remove the TIA and e) calcinating it to remove the organic template. In a usual embodiment said reaction mixture has a composition expressed in terms of molar oxide ratios of :TEMP/Al 2 O 3 = 0.3-5, more desirable 0.5-2 MeO 2 /Al 2 O 3 = 0.005-2.0, more desirable 0.022-0.8 P 2 O 5 /Al 2 O 3 = 0.5-2, more desirable 0.8-1.2 TIA/Al 2 O 3 = 3-30, more desirable 6-20. In a usual embodiment the metalloaluminophosphate (MeAPO) molecular sieves made with the above method have a lamellar crystal morphology having an empirical chemical composition on an anhydrous basis, after synthesis and calcination, expressed by the formula H x Me y Al z P k O 2 wherein, y+z+k=1, x
摘要翻译：本发明还涉及一种制备金属铝磷酸盐（MeAPO）分子筛的方法，所述方法包括：a）形成含有纹理影响剂（TIA），有机模板剂（TEMP），至少反应性无机源不溶于TIA的Al 2 O 3和P 2 O 5的反应性源的MeO 2 b）使如此形成的上述反应混合物结晶直到形成金属磷酸铝的晶体，c）回收固体反应产物，d）用水洗涤以除去TIA，和e）煅烧以除去有机模板。在通常的实施方案中，所述反应混合物具有以摩尔氧化物比例表示的组成：TEMP / Al 2 O 3 N 3 = 0.3-5，更优选0.5-2 MeO 更优选的是0.022-0.8 P 2 O 2 O 3， 5/3/3/3/3>更优选0.8-1.2 TIA / Al 2 O 3 3〜30，更优选6〜20。在通常的实施方案中，用上述方法制备的金属铝磷酸盐（MeAPO）分子筛具有层状晶体形态，其在合成和煅烧之后具有无水基础上的经验化学组成，由式H 其中，y + z + k = 1，x <= y;其中，y + z + k = 1，x <= y; y的值为0.0008〜0.4，更优选为0.005〜0.18; z的值为0.25至0.67，更优选为0.38至0.5525; k具有0.2至0.67范围内的值，更优选0.36至0.54，所述分子筛主要具有平板晶体形态。在有利的实施方案中，通过本发明的方法制备的MeAPO基本上具有结构CHA或AEI或其混合物。优选地，它们基本上具有结构SAPO 18或SAPO 34或其混合物。本发明还涉及由通过本发明的方法制备的上述MeAPO分子筛或包含通过本发明的方法制备的上述MeAPO分子筛组成的催化剂。本发明还涉及一种由含氧卤化物或含硫有机原料制备烯烃产物的方法，其中所述含氧卤化物或含硫有机原料与上述催化剂接触有效地将含氧卤化物或含硫有机原料转化为烯烃产物的条件。

5. 发明申请

WO2003101892A1 METHOD FOR IN-SITU SYNTHESIS OF CRYSTALLINE MICROPOROUS METALLOALUMINOPHOSPHATE IN A FORMED BODY 审中-公开
标题翻译：在形成体内的晶体微孔金属磷酸盐酸盐的合成方法
公开(公告)号：WO2003101892A1
公开(公告)日：2003-12-11
申请号：PCT/NO2003/000170
申请日：2003-05-23
申请人： NORSK HYDRO ASA , FUGLERUD, Terje , GRØNVOLD, Arne, Gidløv , WENDELBO, Rune , SLAGTERN, Åse , DAHL, Ivar, Martin
发明人： FUGLERUD, Terje , GRØNVOLD, Arne, Gidløv , WENDELBO, Rune , SLAGTERN, Åse , DAHL, Ivar, Martin
IPC分类号： C01B37/06
CPC分类号： B01J20/02 , B01J20/0248 , B01J20/0292 , B01J20/10 , B01J29/84 , B01J29/85 , B01J2229/64 , C01B37/06 , C01B37/08 , C01B39/54
摘要： The invention concerns a method for production of microporous crystalline metalloaluminium phosphates (ELAPO) based adsorbents or catalysts by in-situ crystallisation of ELAPO inside a formed body. First the formed body containing aluminium phosphate (AIPO) and binder is prepared, thereafter the organic structure directing agent, EL source and water are added and finally ELAPO is crystallised in-situ at elevated temperature and pressure, while keeping the shape and size of the formed body.
摘要翻译：本发明涉及通过在成形体内ELAPO的原位结晶来生产微孔结晶金属磷酸铝（ELAPO）基吸附剂或催化剂的方法。首先制备含有磷酸铝（AIPO）和粘合剂的成型体，然后加入有机结构导向剂，EL源和水，最后将ELAPO在升高的温度和压力下原位结晶，同时保持其形状和尺寸成型体。

6. 发明申请

WO2003035549A1 SYNTHESIS OF SILICOALUMINOPHOSPHATES 审中-公开
标题翻译：硅烷基磷酸酯的合成
公开(公告)号：WO2003035549A1
公开(公告)日：2003-05-01
申请号：PCT/US2002/023525
申请日：2002-07-24
申请人： EXXONMOBIL CHEMICAL PATENTS INC.
发明人： MERTENS, Machteld, M. , ENGELS, Brita
IPC分类号： C01B37/04
CPC分类号： C07C1/20 , B01J29/85 , C01B37/04 , C01B37/06 , C01B37/08 , C10G3/49 , C10G2300/703 , C10G2400/20 , Y02P30/20
摘要： Disclosed is a method for the manufacture of silicoaluminophosphate (SAPO) and/or aluminophosphate (ALPO) molecular sieves. The method includes maintaining the slurry of the as crystallized molecular sieve under substantially static conditions when stored after substantially complete crystallization and prior to recovery of the product.
摘要翻译：公开了一种制造硅铝磷酸盐（SAPO）和/或磷酸铝（ALPO）分子筛的方法。该方法包括当基本上完全结晶并且在产物回收之前储存时，使结晶分子筛的浆液保持在基本上静态的条件下。

7. 发明申请

WO2002060835A1 多孔質体及びその製造方法审中-公开
标题翻译：多孔材料及其制备方法
公开(公告)号：WO2002060835A1
公开(公告)日：2002-08-08
申请号：PCT/JP2002/000166
申请日：2002-01-11
申请人：科学技術振興事業団 , 山中昭司 , 佐々木俊之
发明人：山中昭司 , 佐々木俊之
IPC分类号： C04B38/04
CPC分类号： C01B37/06 , C01B25/36 , C01B37/04 , C03C3/19 , C03C11/00 , C03C11/005
摘要： A glass of AlPO4-B2O3-Na2O system maintaining an amorphous state was placed in an autoclave together with distilled water and treated at 150 DEG C for 2 hr. The glass which had an extremely little specific surface area before the above autoclave treatment was converted to a mesopore material having a specific surface area of 236 m /g and a pore diameter distribution ranging from 5 to 10 nm, through the dissolution of most part of the borate component and sodium component in the glass into the water by the autoclave treatment. The mesopore material exhibits a weak acidity, a low polarity and hydrophobicity.
摘要翻译：将保持无定形状态的一杯AlPO 4 -B 2 O 3·Na 2 O体系与蒸馏水一起放入高压釜中，并在150℃下处理2小时。将上述高压釜处理前的比表面积非常小的玻璃，通过溶解，将其转化成比表面积为236m 2 / g，孔径分布为5〜10nm的中孔材料大部分硼酸盐组分和钠组分在玻璃中通过高压釜处理进入水中。中孔材料表现出弱酸性，低极性和疏水性。

8. 发明申请

WO2012161985A1 FIBROUS SUBSTRATE-BASED HYDROPROCESSING CATALYSTS AND ASSOCIATED METHODS 审中-公开
标题翻译：基于底物的水解催化剂及相关方法
公开(公告)号：WO2012161985A1
公开(公告)日：2012-11-29
申请号：PCT/US2012/037427
申请日：2012-05-11
申请人： UOP LLC , NEGIZ, Antoine , WANG, Hui
发明人： NEGIZ, Antoine , WANG, Hui
IPC分类号： B01J37/025 , B01J35/06 , B01J29/06 , B01J21/08
CPC分类号： B01J29/7007 , B01J29/06 , B01J29/084 , B01J29/18 , B01J29/40 , B01J35/06 , B01J2229/64 , C01B37/02 , C01B37/06 , C01B37/08 , C01B39/04 , C01B39/40 , C01B39/54 , C10G47/16
摘要： Catalysts are disclosed comprising fibrous substrates having silica-containing fibers with diameters generally from 1 to 50 microns, which act effectively as "micro cylinders." Such catalysts can dramatically improve physical surface area, for example per unit length of a reactor or reaction zone. At least a portion of the silica, originally present in the silica- containing fibers of a fibrous material used to form the fibrous substrate, is converted to a zeolite ( e.g. , having a SiO 2 /AI 2 O 3 ratio of at least 150) that remains deposited on these fibers. The fibrous substrates possess important properties, for example in terms of acidity, which are useful in hydroprocessing ( e.g. , hydrotreating or hydrocracking) applications.
摘要翻译：公开了包含具有通常为1至50微米的直径的含二氧化硅的纤维的纤维基材的催化剂，其有效地作为“微型气瓶”起作用。这样的催化剂可以显着改善物理表面积，例如每单位长度的反应器或反应区。原来存在于用于形成纤维基质的纤维材料的含二氧化硅的纤维中的二氧化硅的至少一部分转化成保持沉积在其上的沸石（例如，具有至少150的SiO 2 / Al 2 O 3比例）这些纤维。纤维基质具有重要的性质，例如在酸性方面，其可用于加氢处理（例如加氢处理或加氢裂化）应用。

9. 发明申请

WO01036329A1 MOLECULAR SIEVES 审中-公开
标题翻译：分子筛
公开(公告)号：WO01036329A1
公开(公告)日：2001-05-25
申请号：PCT/US2000/030346
申请日：2000-11-03
IPC分类号： B01J29/84 , B01J29/85 , C01B37/06 , C01B37/08
CPC分类号： B01J29/85 , B01J29/84 , C01B37/06 , C01B37/065 , C01B37/08 , Y10S423/30
摘要： The present invention provides a method for the synthesis of MeAPO molecular sieves which includes the following steps: providing a source of alumina, a source of phosphorus, water, and a template suitable for forming a MeAPO molecular sieves; providing a source of metal (Me) including metal particles, the metal particles measuring, in their largest dimension, equal to or less than five nanometers; providing a water soluble organic solvent capable of solubilizing the source of metal; forming a synthesis mixture from the source of alumina, the source of phosphorus, the water, the template, the source of metal, and the solvent; and forming a MeAPO molecular sieve from the synthesis mixture.
摘要翻译：本发明提供了一种合成MeAPO分子筛的方法，其包括以下步骤：提供氧化铝源，磷源，水和适于形成MeAPO分子筛的模板; 提供包括金属颗粒的金属（Me）源，金属颗粒在其最大尺寸上测量等于或小于5纳米; 提供能溶解金属源的水溶性有机溶剂; 从氧化铝源，磷源，水，模板，金属源和溶剂形成合成混合物; 并从合成混合物中形成MeAPO分子筛。

10. 发明申请

WO00006494A1 CRYSTALLINE MOLECULAR SIEVES 审中-公开
标题翻译：晶体分子筛
公开(公告)号：WO00006494A1
公开(公告)日：2000-02-10
申请号：PCT/GB1999/002468
申请日：1999-07-28
IPC分类号： B01D53/02 , B01J20/18 , B01J29/18 , B01J29/65 , B01J29/70 , B01J29/85 , B01J35/00 , C01B37/00 , C01B37/04 , C01B37/06 , C01B37/08 , C01B39/02 , C01B39/26 , C01B39/44 , C01B39/46 , C01B39/48 , C01B39/54 , C01G3/00 , C07B61/00 , C07C1/24 , C07C11/04 , C07C11/06 , C07C11/08 , C10G3/00 , B01J29/04 , C01B39/30
CPC分类号： B01J29/7026 , B01J20/0292 , B01J20/18 , B01J29/18 , B01J29/50 , B01J29/65 , B01J29/7011 , B01J29/7023 , B01J29/85 , B01J35/0013 , B01J2229/62 , C01B37/00 , C01B37/04 , C01B37/06 , C01B37/08 , C01B39/02 , C01B39/265 , C01B39/44 , C01B39/445 , C01B39/48 , C01G3/00 , C10G3/49 , C10G25/03 , C10G2400/20 , C10G2400/22 , Y02P30/20
摘要： A colloidal suspension of LEV structure type crystalline molecular sieve, making the suspension by washing smaller crystallites from a previously found solid LEV product, and using the suspension as seeds in further crystalline molecular sieve syntheses.
摘要翻译： LEV结构型结晶分子筛的胶体悬浮液，通过从先前发现的固体LEV产物洗涤较小的微晶，并将悬浮液用作进一步的结晶分子筛合成中的种子制备悬浮液。

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