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1. 发明申请

WO2007019205A3 A PROCESS FOR PREPARING MOLECULAR SIEVES VIA CONTINUOUS ADDITION OF NUTRIENTS 审中-公开
标题翻译：通过连续添加营养来制备分子筛的方法
公开(公告)号：WO2007019205A3
公开(公告)日：2007-04-12
申请号：PCT/US2006030189
申请日：2006-08-03
申请人： UOP LLC , KONRAD BRIAN S , MARTE JULIO C , MEZZA BECKAY J , WILSON STEPHEN T , JACOBSEN LANCE L , LESCH DAVID A
发明人： KONRAD BRIAN S , MARTE JULIO C , MEZZA BECKAY J , WILSON STEPHEN T , JACOBSEN LANCE L , LESCH DAVID A
IPC分类号： C01B37/08 , C01B39/02
CPC分类号： C01B39/48 , C01B39/04 , C01B39/54 , Y10S423/30
摘要： A process for synthesizing a variety of molecular sieves has been developed. The process involves forming a reaction mixture comprising reactive sources of the framework elements plus at least one templating agent, reacting the mixture to at least partially crystallize the molecular sieve and provide a slurry of seed crystals and adding to it nutrients (sources) of the framework elements, e.g. aluminum and silicon in order to grow the seed crystals. The rate of addition of the nutrients is controlled such that it is substantially the same as the crystal growth rate and such that there is substantially no nucleation of new crystals. The seed crystals may be the same or different than the nutrients being added, thus allowing for a layered molecular sieve. When the crystals have reached a desired size, they are isolated by conventional techniques.
摘要翻译：已经开发了合成各种分子筛的方法。该方法包括形成包含框架元件的反应性源加上至少一种模板剂的反应混合物，使混合物反应至少部分地使分子筛结晶并提供晶种的浆料并向其中添加骨架的营养物（来源）元素，例如铝和硅，以生长晶种。控制营养素的添加速度，使其与晶体生长速度基本相同，并且基本上不存在新晶体的成核。晶种可以与添加的营养物相同或不同，从而允许层状分子筛。当晶体达到所需尺寸时，它们通过常规技术分离。

2. 发明申请

WO2009058548A3 MICROPOROUS ALUMINOPHOSPHATE MOLECULAR SIEVE MEMBRANES FOR HIGHLY SELECTIVE SEPARATIONS 审中-公开
标题翻译：用于高选择性分离的微孔磷酸铝分子筛膜
公开(公告)号：WO2009058548A3
公开(公告)日：2009-07-09
申请号：PCT/US2008079766
申请日：2008-10-14
申请人： UOP LLC , LIU CHUNQING , WILSON STEPHEN T , LESCH DAVID A
发明人： LIU CHUNQING , WILSON STEPHEN T , LESCH DAVID A
IPC分类号： C01B25/36 , B01J27/18 , B01J29/04 , C01B37/04
CPC分类号： B01D53/228 , B01D67/0046 , B01D67/0051 , B01D67/0088 , B01D67/0095 , B01D69/10 , B01D71/028 , B01D2256/24 , B01D2257/504 , B01D2323/14 , B01D2323/24 , B01D2323/40 , B01J20/0292 , B01J20/08 , C01B37/04 , C01B39/54 , Y02C10/10 , Y02P20/152
摘要： The present invention discloses microporous aluminophosphate (AlPO4) molecular sieve membranes and methods for making and using the same. The microporous AlPO4 molecular sieve membranes, particularly small pore microporous AlPO-14 and AlPO-18 molecular sieve membranes, are prepared by three different methods, including in-situ crystallization of a layer of AlPO4 molecular sieve crystals on a porous membrane support, coating a layer of polymer-bound AlPO4 molecular sieve crystals on a porous membrane support, and a seeding method by in-situ crystallization of a continuous second layer of AlPO4 molecular sieve crystals on a seed layer of AlPO4 molecular sieve crystals supported on a porous membrane support. The microporous AlPO4 molecular sieve membranes have superior thermal and chemical stability, good erosion resistance, high CO2 plasticization resistance, and significantly improved selectivity over polymer membranes for gas and liquid separations, including carbon dioxide/methane, carbon dioxide/nitrogen and hydrogen/methane separations.
摘要翻译：本发明公开了微孔铝磷酸盐（AlPO 4）分子筛膜及其制备和使用方法。通过三种不同的方法制备微孔AlPO 4分子筛膜，特别是小孔微孔AlPO-14和AlPO-18分子筛膜，包括在多孔膜载体上原位结晶一层AlPO 4分子筛晶体，在多孔膜载体上的聚合物结合的AlPO 4分子筛晶体层以及通过在由多孔膜载体支撑的AlPO 4分子筛晶体的晶种层上连续的第二层AlPO 4分子筛晶体原位结晶的晶种法。微孔AlPO4分子筛膜具有优异的热稳定性和化学稳定性，良好的抗侵蚀性，高二氧化碳增塑性，以及对气体和液体分离（包括二氧化碳/甲烷，二氧化碳/氮气和氢气/甲烷分离）的聚合物膜的选择性显着提高。

3. 发明申请

WO2006099078A2 HIGH FLUX, MICROPOROUS, SIEVING MEMBRANES AND SEPARATORS CONTAINING SUCH MEMBRANES AND PROCESSES USING SUCH MEMBRANES 审中-公开
标题翻译：高通量，微孔，切割膜和分离器，这些膜和使用这种膜的方法
公开(公告)号：WO2006099078A2
公开(公告)日：2006-09-21
申请号：PCT/US2006008478
申请日：2006-03-10
申请人： UOP LLC , KULPRATHIPANJA SANTI , LIU CHUNQING , WILSON STEPHEN T , LESCH DAVID A , RICE LYNN H , SHECTERLE DAVID J , SHIELDS DALE J , FREY STANLEY J
发明人： KULPRATHIPANJA SANTI , LIU CHUNQING , WILSON STEPHEN T , LESCH DAVID A , RICE LYNN H , SHECTERLE DAVID J , SHIELDS DALE J , FREY STANLEY J
IPC分类号： B01D61/00
CPC分类号： B01D71/028 , B01D67/0002 , B01D67/0006 , B01D67/0039 , B01D67/0041 , B01D67/0044 , B01D67/0046 , B01D67/0051 , B01D67/0072 , B01D69/10 , B01D69/141 , B01D71/021 , B01D71/027 , B01D71/64 , B01D2323/40 , B01D2325/02 , B01D2325/28 , C07C7/144 , C10G31/11 , Y02P20/582 , C07C15/08 , C07C9/14
摘要： A sieving membrane comprises a thin, microporous barrier to provide a high flux. The membrane structure can tolerate defects yet still obtain commercially-attractive separations.
摘要翻译：筛分膜包括薄的微孔屏障以提供高通量。膜结构可以容忍缺陷，但仍然获得商业上有吸引力的分离。

4. 发明申请

WO2009158157A3 MIXED MATRIX MEMBRANES CONTAINING ION-EXCHANGED MOLECULAR SIEVES 审中-公开
标题翻译：含有离子交换分子筛的混合基质膜
公开(公告)号：WO2009158157A3
公开(公告)日：2010-04-29
申请号：PCT/US2009046071
申请日：2009-06-03
申请人： UOP LLC , LIU CHUNQING , MOSCOSO JAIME G , SERBAYEVA RAISA , WILSON STEPHEN T , LESCH DAVID A
发明人： LIU CHUNQING , MOSCOSO JAIME G , SERBAYEVA RAISA , WILSON STEPHEN T , LESCH DAVID A
IPC分类号： B01D71/00 , B01D69/00
CPC分类号： B01D71/028 , B01D67/0079 , B01D69/148 , B01D2323/21 , B01D2323/36 , B01D2325/16
摘要： The present invention discloses mixed matrix membranes (MMMs) comprising ion-exchanged molecular sieves such as UZM-5 zeolite ion-exchanged with Li+ cation (Li-UZM 5) and a continuous polymer matrix and methods for making and using these membranes. These MMMs, comprising ion-exchanged molecular sieves, in the form of symmetric dense films, asymmetric flat sheets, asymmetric hollow fibers, or thin-film composites, have exhibited simultaneously increased selectivity and permeability (or permeance) over polymer-only membranes and the mixed matrix membranes made from molecular sieves that have not been ion exchanged for gas separations. These MMMs are suitable for a variety of liquid, gas, and vapor separations such as desalination of water by reverse osmosis, deep desulfurization of gasoline and diesel fuels, ethanol/water separations, pervaporation dehydration of aqueous/organic mixtures, CO2/CH4, CO2/N2, H2/CH4, O2/N2, olefin/paraffin, iso/normal paraffins separations, and other light gas mixture separations.
摘要翻译：本发明公开了包含离子交换分子筛（例如与Li +阳离子（Li-UZM 5）离子交换的UZM-5沸石）和连续聚合物基质的混合基质膜（MMM）以及制备和使用这些膜的方法。这些包含离子交换分子筛，以对称致密膜，不对称平板，不对称中空纤维或薄膜复合材料形式的MMM已经显示出与聚合物膜相比增加的选择性和渗透性（或渗透性），并且由分子筛制成的未经离子交换进行气体分离的混合基质膜。这些MMM适用于各种液体，气体和蒸汽分离，如通过反渗透脱水，汽油和柴油燃料的深度脱硫，乙醇/水分离，水/有机混合物的渗透蒸发脱水，CO 2 / CH 4，CO 2 / N2，H2 / CH4，O2 / N2，烯烃/石蜡，异/正链烷烃分离和其他轻质气体混合物分离。

5. 发明申请

WO2007106677A2 HIGH FLUX MIXED MATRIX MEMBRANES FOR SEPARATIONS 审中-公开
标题翻译：用于分离的高通量混合MATRIX膜
公开(公告)号：WO2007106677A2
公开(公告)日：2007-09-20
申请号：PCT/US2007063305
申请日：2007-03-05
申请人： UOP LLC , LIU CHUNQING , KULPRATHIPANJA SANTI , WILSON STEPHEN T
发明人： LIU CHUNQING , KULPRATHIPANJA SANTI , WILSON STEPHEN T
IPC分类号： B01D53/22
CPC分类号： B01D53/228 , B01D61/362 , B01D67/0079 , B01D69/141 , B01D69/147 , B01D71/028 , B01D71/72
摘要： The present invention discloses a new class of high flux mixed matrix membranes that are made by incorporating porous inorganic fillers (e.g. microporous and mesoporous molecular sieves, carbon molecular sieves, porous metal-organic frameworks) into a high flux high surface area microporous organic polymer matrix. These microporous organic polymers are referred to as "polymers of intrinsic microporosity" or PIMs. The high flux membranes are promising for a wide range of separations including liquid separations such as pervaporation of phenol/water and also gas separations in the petrochemical, refinery, and natural gas industries such as methane/carbon dioxide, olefin/paraffin and iso/normal paraffins separations.
摘要翻译：本发明公开了一种新型高通量混合基质膜，其通过将多孔无机填料（例如微孔和介孔分子筛，碳分子筛，多孔金属 - 有机骨架）并入高通量高表面积微孔有机聚合物基体。这些微孔有机聚合物被称为“内在微孔聚合物”或PIM。高通量膜对于广泛的分离是有希望的，包括液体分离，例如苯酚/水的渗透蒸发，以及在石化，炼油和天然气工业中的气体分离，例如甲烷/二氧化碳，烯烃/石蜡和异/正常石蜡分离。

6. 发明申请

WO2004039725A3 "CRYSTALLINE ALUMINOSILICATE ZEOLITIC COMPOSITION: UZM-4M" 审中-公开
标题翻译： “水晶铝酸酯组合物：UZM-4M”
公开(公告)号：WO2004039725A3
公开(公告)日：2005-05-12
申请号：PCT/US0314564
申请日：2003-05-08
申请人： UOP LLC , WILSON BEN A , LEWIS GREGORY J , JAN DENG-YANG , WILSON STEPHEN T , PATTON R LYLE
发明人： WILSON BEN A , LEWIS GREGORY J , JAN DENG-YANG , WILSON STEPHEN T , PATTON R LYLE
IPC分类号： C01B39/00 , B01J29/70 , C01B39/02 , C01B39/48 , C10G29/20 , C10G45/64 , C10G47/16 , B01J20/18 , C01B39/06 , C07C2/66 , C07C5/27 , C07C6/12
CPC分类号： C10G47/16 , B01J29/70 , B01J2229/36 , C01B39/026 , C01B39/48 , C10G2400/30
摘要： A crystalline aluminosilicate zeolite identified as UZM-4M has been synthesized. This zeolite is obtained by treating a UZM-4 zeolite with a fluorosilicate salt to obtain a zeolite having the empirical formula:M1an+Al1-xExSiyOzwhere M1 is an alkali metal, alkaline earth metal, rare earth metal, hydronium ion or ammonium ion, E can be gallium, iron, boron, indium and mixtures thereof and has a Si/Al ratio of 1.5 to 10.
摘要翻译：鉴定为UZM-4M的结晶硅铝酸盐沸石已被合成。该沸石是通过用氟硅酸盐处理UZM-4沸石得到具有以下经验式的沸石得到的：M1an + Al1-xExSiyOz其中M1是碱金属，碱土金属，稀土金属，水合氢离子或铵离子，E 可以是镓，铁，硼，铟及其混合物，Si / Al比为1.5〜10。

7. 发明申请

WO2012128857A3 MICROPOROUS UZM-5 INORGANIC ZEOLITE MEMBRANES FOR GAS, VAPOR, AND LIQUID SEPARATIONS 审中-公开
标题翻译：用于气体，蒸气和液体分离的微波UZM-5无机沸石膜
公开(公告)号：WO2012128857A3
公开(公告)日：2012-10-26
申请号：PCT/US2012024401
申请日：2012-02-09
申请人： UOP LLC , LIU CHUNQING , MOSCOSO JAIME G , WILSON STEPHEN T
发明人： LIU CHUNQING , MOSCOSO JAIME G , WILSON STEPHEN T
IPC分类号： B01D71/02 , B01D69/02 , B01D69/12 , B01J20/16 , B01J20/18
CPC分类号： B01D71/028 , B01D53/228 , B01D67/0048 , B01D67/0051 , B01D67/0088 , B01D69/10 , B01D2323/14 , B01J20/186 , B01J20/28007 , B01J20/28035 , B01J20/3057 , B01J20/3078 , B01J20/3085 , B01J20/3238 , B01J20/3272 , B82Y30/00
摘要： The present invention discloses microporous UZM-5 zeolite membranes, methods for making the same, and methods of separating gases, vapors, and liquids using the same. The small-pore microporous UZM-5 zeolite membrane is prepared by two different methods, including in-situ crystallization of one or more layers of UZM-5 zeolite crystals on a porous membrane support, and a seeding method by in-situ crystallization of a continuous second layer of UZM-5 zeolite crystals on a seed layer of UZM-5 zeolite crystals supported on a porous membrane support. The membranes in the form of disks, tubes, or hollow fibers have superior thermal and chemical stability, good erosion resistance, high CO2 plasticization resistance, and significantly improved selectivity over polymer membranes for gas, vapor, and liquid separations.
摘要翻译：本发明公开了微孔UZM-5沸石膜，其制造方法，以及使用其分离气体，蒸汽和液体的方法。小孔微孔UZM-5沸石膜通过两种不同的方法制备，包括在多孔膜载体上的一层或多层UZM-5沸石晶体的原位结晶，以及通过原位结晶的接种方法在支撑在多孔膜载体上的UZM-5沸石晶种的种子层上连续的第二层UZM-5沸石晶体。圆盘，管或中空纤维形式的膜具有优异的热稳定性和化学稳定性，良好的抗侵蚀性，高的二氧化碳抗塑化性，并且对于气体，蒸汽和液体分离，在聚合物膜上显着提高了选择性。

8. 发明申请

WO2009148733A3 CROSSLINKED ORGANIC-INORGANIC HYBRID MEMBRANES AND THEIR USE IN GAS SEPARATION 审中-公开
标题翻译：交联有机无机混合膜及其在气体分离中的应用
公开(公告)号：WO2009148733A3
公开(公告)日：2010-02-18
申请号：PCT/US2009042458
申请日：2009-05-01
申请人： UOP LLC , LIU CHUNQING , WILSON STEPHEN T , KULPRATHIPANJA SANTI
发明人： LIU CHUNQING , WILSON STEPHEN T , KULPRATHIPANJA SANTI
IPC分类号： C08J3/24 , C08J5/22 , C08K3/20 , C08K5/00 , C08K5/541 , C08L71/02
CPC分类号： C08L1/20 , B01D53/228 , B01D67/0079 , B01D71/00 , B01D71/16 , B01D71/52 , B01D71/70 , B01D2257/102 , B01D2257/504 , C08B7/00 , C08G65/33306 , C08G65/33351 , C08G65/336 , C08G2650/58 , C08L71/02 , Y02C10/10 , Y02P20/152
摘要： The present invention is for crosslinked membranes and in particular for crosslinked poly(ethylene oxide)-cellulose acetate-silsesquioxane (PEO-CA-Si) organic-inorganic hybrid membranes and their use in gas separation. These crosslinked PEO-CA-Si membranes were prepared by in-situ sol-gel co-condensation of crosslinkable PEO-organotrialkoxysilane and CA-organotrialkoxysilane polymers in the presence of acetic acid catalyst during the formation of membranes. The crosslinkable PEO- and CA-organotrialkoxysilane polymers were synthesized via the reaction between the hydroxyl groups on PEO (or on CA) and the isocyanate on organotrialkoxysilane to form urethane linkages under mild conditions. The crosslinked PEO-CA-Si membranes exhibited both increased selectivity of CO2/N2 and CO2 permeability as compared to a CA membrane, suggesting that these membranes are very promising for gas separations such as CO2/N2 separation.
摘要翻译：本发明涉及交联膜，特别是交联聚（环氧乙烷） - 醋酸纤维素 - 倍半硅氧烷（PEO-CA-Si）有机 - 无机混合膜及其在气体分离中的应用。这些交联的PEO-CA-Si膜通过在形成膜期间在乙酸催化剂存在下通过可交联的PEO-有机三烷氧基硅烷和CA-有机三烷氧基硅烷聚合物的原位溶胶 - 凝胶共缩合制备。通过PEO（或CA）上的羟基与有机三烷氧基硅烷上的异氰酸酯之间的反应合成可交联PEO-和CA-有机三烷氧基硅烷聚合物，以在温和条件下形成氨基甲酸酯键。与CA膜相比，交联的PEO-CA-Si膜显示出增加的CO 2 / N 2和CO 2渗透性的选择性，表明这些膜对于气体分离如CO 2 / N 2分离是非常有希望的。

9. 发明申请

WO2007032899A3 SAPO-34 MOLECULAR SIEVES WITH HIGH SELECTIVITY TOWARDS LIGHT OLEFINS IN METHANOL TO OLEFIN CONVERSION 审中-公开
标题翻译：具有高选择性的SAPO-34分子筛将甲醇中的烯烃转化为烯烃转化
公开(公告)号：WO2007032899A3
公开(公告)日：2007-05-03
申请号：PCT/US2006033525
申请日：2006-08-29
申请人： UOP LLC , BROACH ROBERT W , VANEK MARY A , RINGWELSKI ANDRZEJ Z , WILSON STEPHEN T , MILLER RAELYNN M , CHEN JOHN Q
发明人： BROACH ROBERT W , VANEK MARY A , RINGWELSKI ANDRZEJ Z , WILSON STEPHEN T , MILLER RAELYNN M , CHEN JOHN Q
IPC分类号： B01J29/85 , C07C1/20
CPC分类号： C10G3/49 , B01J29/85 , C07C1/20 , C07C2529/85 , C10G2400/20 , Y02P30/42 , C07C11/02
摘要： A sapo-34 based catalyst for the use in methanol to olefin conversion is identified, and a process for identifying the structure of the catalyst is presented, which is used to determine the quality of the catalyst for its selectivity for producing high light olefins yield. The ratio of peak heights, from the x-ray diffraction pattern, for the peaks at 30.7° 2? and 31.0° 2? shall be greater than 0.75 .
摘要翻译：鉴定了用于甲醇至烯烃转化的基于sapo-34的催化剂，并且提出了用于鉴定催化剂结构的方法，其用于确定催化剂的质量，以获得其产生高轻质烯烃产率的选择性。峰的高度与X射线衍射图的比值为30.7°2？和31.0°2？应大于0.75。

10. 发明申请

WO2006065591A3 A PROCESS FOR PREPARING A DIELECTRIC INTERLAYER FILM CONTAINING SILICON BETA ZEOLITE 审中-公开
标题翻译：一种制备含有硅酮沸石的介电层间膜的方法
公开(公告)号：WO2006065591A3
公开(公告)日：2006-08-10
申请号：PCT/US2005044210
申请日：2005-12-06
申请人： UOP LLC , ABREVAYA HAYIM , WILLIS RICHARD R , WILSON STEPHEN T
发明人： ABREVAYA HAYIM , WILLIS RICHARD R , WILSON STEPHEN T
IPC分类号： C01B39/48
CPC分类号： C01B39/026
摘要： A process for forming a zeolite beta dielectric layer onto a substrate such as a silicon wafer has been developed. The zeolite beta is characterized in that it has a Si/Al of at least 25 and has crystallites from 5 to 40 nanometers. The process involves first dealuminating a starting zeolite beta, then preparing a slurry of the dealuminated zeolite beta followed by coating a substrate, e.g. silicon wafer with the slurry, heating to form a zeolite beta film and treating the zeolite beta with a silylating agent.
摘要翻译：已经开发了在诸如硅晶片的基底上形成沸石β电介质层的方法。沸石β的特征在于其具有至少25的Si / Al并且具有5至40纳米的微晶。该方法首先对起始沸石β进行脱铝，然后制备脱铝沸石β的浆料，然后涂布底物，例如硅晶片，加热形成沸石β膜并用甲硅烷基化剂处理沸石β。

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