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1. 发明申请

WO2006029344A2 GREEN ELECTROCHROMIC (EC) MATERIAL AND DEVICE 审中-公开
标题翻译：绿色电子（EC）材料和器件
公开(公告)号：WO2006029344A2
公开(公告)日：2006-03-16
申请号：PCT/US2005/032211
申请日：2005-09-09
申请人： UNIVERSITY OF WASHINGTON , LIU, Lu , XU, Chunye , TAYA, Minoru , NING, Dai , KANEKO, Calen
发明人： LIU, Lu , XU, Chunye , TAYA, Minoru , NING, Dai , KANEKO, Calen
IPC分类号： G03C1/00
CPC分类号： C09K9/02 , C07D495/04 , C09K2211/1051 , C09K2211/1092 , G03C1/73
摘要： Three green EC materials based on thiophene, and a green EC material based on pyrazine are disclosed. A first thiophene derivative (2,3-Di-thiophen-2-yl-thieno[3,4-b]pyrazine), which was previously investigated as a nonlinear optical material, is here disclosed for its use as an EC material, and for its incorporation into an EC device. Synthesis of two new thiophene derivatives (2,5-di(thien-2-yl)-3,4-di(2,2,2-trifluoro-ethoxy)-thiophene and 2,5-(2,3-dihydro-thieno[3,4-b][1,4]dioxin-5-yl)-3,4-di(2,2,2-trifluoro-ethoxy)-thiophene), and a new pyrazine derivative (2,3-dibenzyl-5,7-di(thien-2-yl) thieno[3,4-b]pyrazine) are also disclosed, since these materials are all able to selectively change to a green color state, and can be polymerized to achieve a green EC polymer.
摘要翻译：公开了基于噻吩的三种绿色EC材料和基于吡嗪的绿色EC材料。作为非线性光学材料，先前研究的第一个噻吩衍生物（2,3-二噻吩-2-基 - 噻吩并[3,4-b]吡嗪）在此被公开用作EC材料，并且将其并入EC设备。合成两种新的噻吩衍生物（2,5-二（噻吩-2-基）-3,4-二（2,2,2-三氟 - 乙氧基） - 噻吩和2,5-（2,3-二氢 - 噻吩并[3,4-b] [1,4]二恶英-5-基）-3,4-二（2,2,2-三氟 - 乙氧基） - 噻吩）和新的吡嗪衍生物还公开了二苄基-5,7-二（噻吩-2-基）噻吩并[3,4-b]吡嗪），因为这些材料都能够选择性地变为绿色状态，并且可以聚合以实现绿色EC聚合物。

2. 发明申请

WO2005050294A2 ELECTROPOLYMERIZATION OF ENHANCED ELECTROCHROMIC (EC) POLYMER FILM 审中-公开
标题翻译：增强电化学（EC）聚合物膜的电化学
公开(公告)号：WO2005050294A2
公开(公告)日：2005-06-02
申请号：PCT/US2004/038888
申请日：2004-11-18
申请人： UNIVERSITY OF WASHINGTON , XU, Chunye , LIU, Lu , TAYA, Minoru
发明人： XU, Chunye , LIU, Lu , TAYA, Minoru
IPC分类号： G02F
CPC分类号： C09K9/02 , C08G61/123 , C08G61/124 , C08G61/126 , C09K2211/1029 , C09K2211/1096 , C09K2211/1458 , C09K2211/1466 , C09K2211/1491 , G01N21/553 , G02F1/155 , G02F2001/1515 , G02F2001/1555
摘要： Electropolymerization of EC monomers is employed to obtain an EC polymer film deposited on a substrate. A first embodiment of a method to produce the film employs cyclic voltammetry alone, while a second embodiment deposits a very thin homogeneous layer using chronoamperometry, and then cyclic voltammetry is employed to increase the density of the film. Another aspect of the present invention is directed to specific web like configurations for a grid of conductive material deposited onto a transparent substrate. The web like configuration is based either on concentric circles, or on concentric ellipses. Yet another aspect of the present invention is directed to an imaging system including a digital window that is disposed between a prism and a patterned analytic layer.
摘要翻译：使用EC单体的电聚合来获得沉积在基材上的EC聚合物膜。制造薄膜的方法的第一实施例单独使用循环伏安法，而第二实施方案使用计时电流法沉积非常薄的均匀层，然后循环伏安法用于增加膜的密度。本发明的另一方面涉及沉积在透明基底上的导电材料格栅的特定网状结构。网状配置基于同心圆或同心椭圆。本发明的另一方面涉及一种成像系统，其包括设置在棱镜和图案化分析层之间的数字窗口。

3. 发明申请

WO2010039141A1 FLEXIBLE PANEL BASED ON ELECTROCHROMIC POLYMERS 审中-公开
标题翻译：基于电致发光聚合物的柔性面板
公开(公告)号：WO2010039141A1
公开(公告)日：2010-04-08
申请号：PCT/US2008/078599
申请日：2008-10-02
申请人： UNIVERSITY OF WASHINGTON , XU, Chunye , MA, Chao , TAYA, Minoru
发明人： XU, Chunye , MA, Chao , TAYA, Minoru
IPC分类号： G01F1/115
CPC分类号： G02F1/161 , G02F1/133305 , G02F2001/1515
摘要： A flexible electrochromic (EC) panel that is usable for a display device or for other applications in which at least a region of the panel is selectively caused to change opacity. An exemplary panel includes an EC working layer or electrode formed of a PProDOT-Me 2 polymer film that is deposited on an indium tin oxide (ITO)-coated polyethylene terephthalate (PET) flexible substrate. Similarly, a counter electrode is formed by depositing a vanadium oxide-titanium oxide (V 2 O 5 -TiO 2 ) composite film on another ITO PET coated flexible substrate. An ultraviolet light-cured film sealant is employed to seal the flexible panel and also serves as a spacer between the electrodes. The film sealant is patterned to define a volume for injecting an electrolyte solution through an inlet port provided in the film sealant. The inlet port is then closed. The EC panel can readily be flexed without damage.
摘要翻译：一种柔性电致变色（EC）面板，可用于显示设备或其他应用中，其中面板的至少一个区域被选择性地引起改变不透明度。示例性面板包括EC工作层或由沉积在氧化铟锡（ITO）涂覆的聚对苯二甲酸乙二醇酯（PET）柔性基底上）的PProDOT-Me2聚合物膜形成的电极。类似地，通过在另一个ITO PET涂覆的柔性衬底上沉积氧化钒 - 氧化钛（V2O5-TiO2）复合膜来形成对电极。使用紫外光固化膜密封剂来密封柔性板，并且还用作电极之间的间隔物。图案化膜密封剂以限定用于通过设置在膜密封剂中的入口注入电解质溶液的体积。然后关闭入口。 EC面板可以轻松地弯曲而不受损坏。

4. 发明申请

WO2005084350A2 SWITCHABLE WINDOW BASED ON ELECTROCHROMIC POLYMERS 审中-公开
标题翻译：基于电致发光聚合物的可切换窗口
公开(公告)号：WO2005084350A2
公开(公告)日：2005-09-15
申请号：PCT/US2005/006806
申请日：2005-03-01
申请人： UNIVERSITY OF WASHINGTON , LU, Liu , XU, Chunye , LEGENSKI, Susan , TAYA, Minoru
发明人： LU, Liu , XU, Chunye , LEGENSKI, Susan , TAYA, Minoru
CPC分类号： G02F1/15 , C08G61/124 , C08G61/126 , C09K9/02 , C09K2211/1458 , G02F1/155 , G02F2001/133374 , G02F2001/1515
摘要： Syntheses of a new blue EC monomer (ProDOT-MePro), and a new red EC monomer (ProDOP-Et2) are described. Two additional new types of EC monomers based on 3, 4-alkylenedioxythiophene include fluorinated EC monomers and an EC monomer including silicon. EC polymer devices having more than one different color EC polymer to enable additional colors to be provided using subtractive color mixing are also described, as well as EC polymer devices incorporating a logo, image, or text, are generally obscured when the device is colored, but become visible when the device is not colored. Also described are EC polymer devices that include a cathodic EC polymer layer, a gel electrolyte, a counter electrode, and a reference electrode. Working prototypes of such devices exhibit significant increases in the speed of transition of the EC device from a colored state to a transparent state.
摘要翻译：描述了新的蓝色EC单体（ProDOT-MePro）和新的红色EC单体（ProDOP-Et2）的合成。基于3,4-亚烷基二氧噻吩的另外两种新型EC单体包括氟化EC单体和包含硅的EC单体。还描述了具有多于一种不同颜色的EC聚合物的EC聚合物装置，以使得能够使用减色混合来提供附加的颜色，以及包含标志，图像或文本的EC聚合物装置在装置着色时通常是模糊的，但当设备未着色时变得可见。还描述了包括阴极EC聚合物层，凝胶电解质，对电极和参比电极的EC聚合物装置。这种装置的工作原型表现出EC装置从有色状态转变为透明状态的速度的显着增加。

5. 发明申请

WO2008118967A1 SMART SUNGLASSES, HELMET FACESHIELDS AND GOGGLES BASED ON ELECTROCHROMIC POLYMERS 审中-公开
标题翻译：基于电致发光聚合物的SMART SUNGLASSES，HELMET FACESHIELDS和GOGGLES
公开(公告)号：WO2008118967A1
公开(公告)日：2008-10-02
申请号：PCT/US2008/058277
申请日：2008-03-26
申请人： UNIVERSITY OF WASHINGTON , XU, Chunye , MA, Chao , TAYA, Minoru
发明人： XU, Chunye , MA, Chao , TAYA, Minoru
IPC分类号： G02C5/00
CPC分类号： G02C7/101
摘要： Eyewear exhibiting a variable light transmittance functionality is achieved by including a smart lens incorporating an electrochromic (EC) polymer, switchable between a first state and a second state in response to a voltage selectively applied thereto. The smart eyewear includes the smart lens, a voltage source, and a support. The EC polymer transmits more light in the first state than in the second state, because changing the state of the EC polymer varies the light transmittance of the smart lens. The voltage source is configured to provide the voltage required to switch the EC polymer between the first state and the second state, while the support member is configured to support the smart lens and enable a user to wear the smart eyewear. Embodiments can include sensors and controllers to automate the switching, as well as energy harvesting elements to increase battery life.
摘要翻译：通过包括结合电致变色（EC）聚合物的智能镜头，响应于选择性施加到其上的电压，可以在第一状态和第二状态之间切换，实现具有可变光透射功能的眼镜。智能眼镜包括智能镜头，电压源和支架。 EC聚合物在第一状态下透射比第二状态更多的光，因为改变EC聚合物的状态会改变智能透镜的透光率。电压源被配置为提供在第一状态和第二状态之间切换EC聚合物所需的电压，而支撑构件被配置为支撑智能镜头并且使得使用者佩戴智能眼镜。实施例可以包括用于自动切换的传感器和控制器以及能量收集元件以增加电池寿命。

6. 发明申请

WO2007035576A2 SURFACE PLASMON RESONANCE BIOSENSOR SYSTEM FOR DETECTION OF ANTIGENS AND METHOD FOR DETERMINING THE PRESENCE OF ANTIGENS 审中-公开
标题翻译：用于检测抗原的表面等离子体共振生物传感器系统和用于确定抗原存在的方法
公开(公告)号：WO2007035576A2
公开(公告)日：2007-03-29
申请号：PCT/US2006/036193
申请日：2006-09-15
申请人： NORTHERN ADVANCEMENT CENTER FOR SCIENCE & TECHNOLGY , HAKOMORI, Senitiroh , TAYA, Minoru , SU, Fengyu , XU, Chunye , HANDA, Kazuko , MURAYAMA, Kimie , FUJIMURA, Tsutomu
发明人： HAKOMORI, Senitiroh , TAYA, Minoru , SU, Fengyu , XU, Chunye , HANDA, Kazuko , MURAYAMA, Kimie , FUJIMURA, Tsutomu
IPC分类号： G01N33/551
CPC分类号： G01N33/57423 , B82Y15/00 , B82Y30/00 , B82Y40/00 , G01N33/54373 , G01N33/57415 , G01N33/57434 , G01N33/57446 , G01N33/57492
摘要： The present invention provides an SPR system and corresponding methods of use, for determining the presence or concentration of tumor-associated antigens in cancer patient samples. The SPR system may have multiple channels, with each channel having operably affixed thereto an antibody specific for a tumor-associated antigen, so as to allow detection of multiple tumor-associated antigens simultaneously. When a biological sample from a patient is applied to the SPR system, the presence of two or more tumor-associated antigens can be determined by measuring an SPR signal shift from each channel. The SPR system may detect the presence or concentration of a tumor-associated carbohydrate antigen, where the sensor surface contains affixed thereto an antibody specific for the glycosyl epitope, as well as an antibody specific for the polypeptide to which the carbohydrate antigen is naturally associated in cancer patients.
摘要翻译：本发明提供一种SPR系统和相应的使用方法，用于确定癌症患者样品中肿瘤相关抗原的存在或浓度。 SPR系统可以具有多个通道，每个通道具有可操作地附着于其上的针对肿瘤相关抗原特异的抗体，以便同时检测多个肿瘤相关抗原。当将来自患者的生物样品应用于SPR系统时，可以通过测量每个通道的SPR信号移位来确定两个或多个肿瘤相关抗原的存在。 SPR系统可以检测肿瘤相关碳水化合物抗原的存在或浓度，其中传感器表面含有固定于其上的糖基表位特异的抗体，以及对于碳水化合物抗原天然相关的多肽具有特异性的抗体癌症患者。

7. 发明申请

WO2003001290A1 ELECTROCHROMIC ORGANIC POLYMER SYNTHESIS AND DEVICES UTILIZING ELECTROCHROMIC ORGANIC POLYMERS 审中-公开
标题翻译：电化学有机聚合物合成及利用电化学有机聚合物的器件
公开(公告)号：WO2003001290A1
公开(公告)日：2003-01-03
申请号：PCT/US2002/020218
申请日：2002-06-25
申请人： UNIVERSITY OF WASHINGTON
发明人： XU, Chunye , TAYA, Minoru
IPC分类号： G02F1/153
CPC分类号： G02F1/15 , C09K9/02 , G02F2001/1502 , H01L51/0037
摘要： Large contrast ratio and rapid switching laminated electrochromic (EC) polymer device includes transparent electrode, cathodic EC polymer, gel electrolyte, and counter electrode. Preferably the cathodic EC polymer is a poly(3,4 propylenedioxythiophene) derivative, PProDOT Me2. Counter electrode is a conductive coating deposited on transparent substrate, with preferred coatings including gold and highly conductive carbon. Lithography and sputtering can be employed to pattern a gold layer, while screen printing can be employed to similarly pattern graphite. Empirical studies of preferred device indicate a color change of high contrast ratio of transmittance (> 50 %?) is rapidly (0.5 1s) obtained upon applied 2.5V, repeatable to at least 10,000 times, as estimated by electrochemistry. Dual layer EC devices including PProDOT Me2 are also disclosed, as are methods for synthesizing preferred EC polymers. Preferred synthesis method for obtaining PProDOT Me2 involves refluxing reagents in toluene in the presence of catalyst, while continually removing methanol byproduct from refluxing solution.
摘要翻译：大对比度和快速切换叠层电致变色（EC）聚合物装置（50b）包括透明电极（42），阴极EC聚合物（44b），凝胶电解质（46）和对电极（52）。阴极EC聚合物优选为聚（3,4-亚丙基二氧噻吩）衍生物PProDOT Me2。反电极（52）是沉积在透明基底上的导电涂层，优选的涂层包括金和高导电性碳。可以使用平版印刷和溅射来图案化金层，而丝网印刷可以用于类似地图案化石墨。对于优选装置的实证研究表明，如通过电化学估算的，施加2.5V时获得的透射率（> 50％λ）的高对比度的颜色变化快速（0.51s），可重复至少10,000次。还公开了包括PProDOT Me2的双层EC装置，以及用于合成优选的EC聚合物的方法。

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