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2. 发明申请

WO2002100802A2 FLUOROUS TRIPHASE AND OTHER MULTIPHASE SYSTEMS 审中-公开
标题翻译：荧光三肽和其他多相体系
公开(公告)号：WO2002100802A2
公开(公告)日：2002-12-19
申请号：PCT/US2002/017829
申请日：2002-06-05
申请人： UNIVERSITY OF PITTSBURGH
发明人： CURRAN, Dennis, P. , WEBER, Stephen, G. , NAKAMURA, Hiroyuki , LINCLAU, Bruno , SUN, Lifang , RYU, Ilhyong , MATSUBARA, Hiroshi
IPC分类号： C07B
CPC分类号： C07D207/333 , C07B37/04 , C07B61/00 , C07B63/00 , C07C1/325 , C07C17/02 , C07C45/46 , C07D307/46 , C07D333/22 , C07C15/52 , C07C23/10 , C07C22/04 , C07C49/84
摘要： A method of reacting a first compound to produce a second compound includes the step of contacting a first non-fluorous phase including the first compound with a first fluorous phase at a first phase interface. The first compound distributes between the first fluorous phase and the first non-fluorous phase. The method further includes the steps of contacting the first fluorous phase with a second non-fluorous phase at a second phase interface and including at least a third compound in the second non-fluorous phase that reacts with the first compound to produce the second compound. The second compound has a distribution coefficient less than the first compound. This method can, for example be used to separate the second compound from unreacted first compound wherein, for example, the first compound is of a fluorous nature and distributes more readily into (or transports more quickly through) the fluorous phase than does the second compound. In general, the fluorous phase serves as a barrier to prevent the two non-fluorous phases from mixing, but molecules that can migrate through the fluorous phase can pass from one side to the other.
摘要翻译：使第一化合物反应以产生第二化合物的方法包括使第一化合物的第一非氟相与第一相界面处的第一氟相接触的步骤。第一化合物在第一氟相和第一非氟相之间分配。该方法还包括以下步骤：在第二相界面处使第一氟相与第二非氟相接触，并且在第二非氟相中包含至少第三化合物，其与第一化合物反应以产生第二化合物。第二化合物的分配系数小于第一化合物。该方法可以例如用于将第二化合物与未反应的第一化合物分离，其中例如第一化合物具有氟性质，并且比第二化合物更容易地分配（或更快地通过）氟相。通常，氟相用作防止两个非氟相混合的屏障，但是可以迁移穿过氟相的分子可以从一侧传递到另一侧。

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