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1. 发明申请

WO2012022624A1 ALUMINUM DRY-COATED AND HEAT TREATED CATHODE MATERIAL PRECURSORS 审中-公开
标题翻译：铝干涂层和热处理阴极材料前驱体
公开(公告)号：WO2012022624A1
公开(公告)日：2012-02-23
申请号：PCT/EP2011/063456
申请日：2011-08-04
申请人： UMICORE , PAULSEN, Jens , KIM, JiHye , HONG, HeonPyo
发明人： PAULSEN, Jens , KIM, JiHye , HONG, HeonPyo
IPC分类号： H01M4/505 , H01M4/525 , C01G53/00
CPC分类号： H01M4/525 , C01G45/1221 , C01G51/42 , C01G51/44 , C01G53/42 , C01G53/44 , C01P2002/50 , C01P2002/52 , C01P2002/72 , C01P2002/77 , C01P2004/03 , C01P2004/51 , C01P2004/61 , C01P2004/84 , C01P2006/12 , C01P2006/40 , C01P2006/60 , C01P2006/80 , C04B35/01 , C04B35/62675 , C04B35/62813 , C04B2235/3203 , C04B2235/3262 , C04B2235/3275 , C04B2235/3279 , C04B2235/44 , C04B2235/5409 , C04B2235/5436 , C04B2235/5472 , C04B2235/721 , C04B2235/726 , H01M4/366 , H01M4/505 , H01M10/052 , H01M10/0525
摘要： Aluminum dry-coated and heat treated cathode material precursors. A particulate precursor compound for manufacturing an aluminum coatedlithium transition metal (M)-oxide powder usable as an active positive electrode material in lithium-ion batteries includes a transition metal (M)-oxide core and a non-amorphous aluminum oxide coating layercovering the core. By providing a heat treatment process for mixed metal precursors that may be combined with an aluminum dry-coating process, novel aluminum containing precursors that may be used to form high quality nickel based cathode materials are obtained. The aluminum dry-coated and heat treated precursors include particles have, compared to prior art precursors, relatively low impurity levels of carbonate and/or sulfide, and can be produced at lower cost.
摘要翻译：铝干涂和热处理阴极材料前体。用作锂离子电池中可用作活性正极材料的铝包覆的锂过渡金属（M） - 氧化物粉末的颗粒前体化合物包括过渡金属（M） - 氧化物核和覆盖芯的非无定形氧化铝涂层。通过提供可以与铝干涂法组合的混合金属前体的热处理工艺，可以获得可用于形成高质量镍基阴极材料的新型含铝前体。铝干涂和热处理的前体包括与现有技术的前体相比具有相对较低的碳酸盐和/或硫化物杂质水平的颗粒，并且可以以较低的成本生产。

2. 发明申请

WO2012022618A1 ALUMINA DRY -COATED CATHODE MATERIAL PRECURSORS 审中-公开
标题翻译：氧化铝干燥阴极材料前体
公开(公告)号：WO2012022618A1
公开(公告)日：2012-02-23
申请号：PCT/EP2011/063412
申请日：2011-08-04
申请人： UMICORE , PAULSEN, Jens , KIM, JiHye , HONG, HeonPyo
发明人： PAULSEN, Jens , KIM, JiHye , HONG, HeonPyo
IPC分类号： C04B35/628 , C01G53/04 , H01M4/525 , C04B35/01
CPC分类号： H01M4/525 , B82Y30/00 , C01G51/04 , C01G53/04 , C01P2002/52 , C01P2002/72 , C01P2004/03 , C01P2004/84 , C04B35/01 , C04B35/62813 , C04B35/62892 , C04B2235/3262 , C04B2235/3275 , C04B2235/3279 , C04B2235/44 , C04B2235/5454 , H01M4/485 , H01M4/505 , Y02E60/122 , Y02P70/54
摘要： A particulate precursor compound for manufacturing an aluminum doped lithium transition metal (M)-oxide powder usable as an active positive electrode material in lithium- ion batteries includes a transition metal (M)-hydroxide or (M)-oxyhydroxide core and a non-amorphous aluminum oxide coating layer covering the core. By providing an aluminum dry-coating process where the particulate precursor core compound is mixed with alumina powder in one or more procedures, higher doping levels of aluminum compared to the known prior art may be achieved. The crystal structure of the alumina is maintained during the coating procedures and the core of each mixed transition metal precursor particle is surrounded by a coating layer containing crystalline alumina nano particles. The aluminum concentration in the particulate precursor decreases as the size of the core increases.
摘要翻译：可用作锂离子电池中的活性正极材料的铝掺杂锂过渡金属（M） - 氧化物粉末的颗粒前体化合物包括过渡金属（M） - 羟基氧化物或（M） - 羟基氧化物核心和非 - 无定形氧化铝覆层覆盖核心。通过提供铝干法涂覆方法，其中颗粒前体核心化合物与氧化铝粉末以一种或多种方法混合，可以实现与已知现有技术相比较较高掺杂水平的铝。在涂布过程中保持氧化铝的晶体结构，并且每个混合的过渡金属前体颗粒的芯被包含结晶氧化铝纳米颗粒的涂层包围。颗粒前体中的铝浓度随着核心尺寸的增加而减小。

3. 发明申请

WO2011054440A1 DOUBLE-SHELL CORE LITHIUM NICKEL MANGANESE COBALT OXIDES 审中-公开
标题翻译：双壳镍铁镍锰锰氧化物
公开(公告)号：WO2011054440A1
公开(公告)日：2011-05-12
申请号：PCT/EP2010/006351
申请日：2010-10-19
申请人： UMICORE , PAULSEN, Jens , DE PALMA, Randy , HONG, HeonPyo , KIM, KyuBo
发明人： PAULSEN, Jens , DE PALMA, Randy , HONG, HeonPyo , KIM, KyuBo
IPC分类号： H01M4/62 , H01M4/525 , H01M4/131 , H01M4/1391
CPC分类号： H01M4/62 , H01M4/131 , H01M4/1315 , H01M4/1391 , H01M4/13915 , H01M4/366 , H01M4/525 , H01M4/623 , H01M10/052 , Y02E60/122
摘要： A lithium transition metal oxide powder for use in a rechargeable battery is disclosed, where the surface of the primary particles of said powder is coated with a first inner and a second outer layer, the second outer layer comprising a fluorine-containing polymer, and the first inner layer consisting of a reaction product of the fluorine-containing polymer and the primary particle surface. An example of this reaction product is LiF, where the lithium originates from the primary particles surface. Also as an example, the fluorine-containing polymer is either one of PVDF, PVDF-HFP or PTFE. Examples of the lithium transition metal oxide are either one of - LiCO d M e O 2 , wherein M is either one or both of Mg and Ti, with e 1+a M' i-a O 2±b M 1 k S m with -0.03 1 consisting of either one or more elements of the group Ca, Sr, Y, La, Ce and Zr, with 0 k 0.1 in wt%; and 0 m 0.6, m being expressed in mol%; and - Li a Ni x CO y M" z O 2±e A f , with 0.9 x 0.9, 0 0.4, 0 0.35, e f 0.05 and 0.9
摘要翻译：公开了一种用于可充电电池的锂过渡金属氧化物粉末，其中所述粉末的初级颗粒的表面涂覆有第一内层和第二外层，第二外层包含含氟聚合物，第一内层由含氟聚合物和一次粒子表面的反应产物组成。该反应产物的一个实例是LiF，其中锂源自初级颗粒表面。另外作为实例，含氟聚合物是PVDF，PVDF-HFP或PTFE中的任一种。锂过渡金属氧化物的实例是LiCOdMeO2中的一种，其中M是Mg和Ti中的一种或两种，e1 + aM'i-aO2±b M1 k Sm与-0.03

4. 发明申请

WO2011054441A1 CORE-SHELL LITHIUM TRANSITION METAL OXIDES 审中-公开
标题翻译：核心锂离子转移金属氧化物
公开(公告)号：WO2011054441A1
公开(公告)日：2011-05-12
申请号：PCT/EP2010/006352
申请日：2010-10-19
申请人： UMICORE , PAULSEN, Jens , DE PALMA, Randy , HONG, HeonPyo , KIM, KyuBo
发明人： PAULSEN, Jens , DE PALMA, Randy , HONG, HeonPyo , KIM, KyuBo
IPC分类号： H01M4/62 , H01M4/525 , H01M4/131 , H01M4/1391 , H01M4/505
CPC分类号： H01M4/62 , H01M4/131 , H01M4/1391 , H01M4/366 , H01M4/505 , H01M4/525 , H01M4/623 , H01M10/052 , Y02E60/122 , Y10T29/49115 , Y10T428/3154
摘要： A lithium transition metal oxide powder for use in a rechargeable battery is disclosed, where the surface of the primary particles of said powder is coated with a LiF layer, where this layer consists of a reaction product of a fluorine-containing polymer and the primary particle surface. The lithium of the LiF originates from the primary particles surface. Examples of the fluorine-containing polymer are either one of PVDF, PVDF-HFP or PTFE. Examples of the lithium transition metal oxide are either one of - LiCo d MeO 2 , wherein M is either one of both of Mg and Ti, with e 1 + a M' 1 -a O 2±b M 1 k S m with -0.03 1 consisting of either one or more elements of the group Ca, Sr, Y, La, Ce and Zr, with 0≤k≤0.1 in wt%; and 0 a Ni x CO y M" z O 2±e A f , with 0.9
摘要翻译：公开了一种用于可充电电池的锂过渡金属氧化物粉末，其中所述粉末的初级颗粒的表面涂覆有LiF层，其中该层由含氟聚合物和主要颗粒的反应产物表面。 LiF的锂源自初级颗粒表面。含氟聚合物的实例是PVDF，PVDF-HFP或PTFE之一。锂过渡金属氧化物的实例是LiCodMeO2之一，其中M是Mg和Ti中的一种，e1 + aM'1-aO2±b M1 k Sm与-0.03

5. 发明申请

WO2015036882A2 WATER-BASED CATHODE SLURRY FOR A LITHIUM ION BATTERY 审中-公开
标题翻译：锂离子电池用水基阴极泥浆
公开(公告)号：WO2015036882A2
公开(公告)日：2015-03-19
申请号：PCT/IB2014/064018
申请日：2014-08-22
申请人： UMICORE , UMICORE KOREA LTD.
发明人： PAULSEN, Jens , HONG, HeonPyo , AHN, Hyo Sun
CPC分类号： H01M4/366 , B60L11/1861 , B60L11/1879 , B60L11/1887 , B60L2240/36 , B60L2240/545 , C01G53/50 , C01P2004/03 , C01P2004/50 , C01P2004/62 , C01P2004/80 , C01P2006/40 , H01M4/131 , H01M4/1315 , H01M4/1391 , H01M4/505 , H01M4/525 , H01M4/623 , H01M10/0525 , H01M2004/021 , H01M2004/028 , H01M2220/20 , Y02T10/7011 , Y02T10/7044 , Y02T10/705 , Y02T90/34
摘要： A water-based lithium ion battery cathode slurry comprising a cathode active material comprising a lithium transition metal oxide powder wherein the lithium transition metal oxide powder consists of agglomerates of primary particles, the primary particles comprising a coating layer comprising a polymer is proposed. The polymer is preferably a fluorine-containing polymer comprising at least 50 wt% of fluorine. The coating layer preferably comprises a first inner and a second outer coating layer, the second outer layer comprising the fluorine-containing polymer, and the first inner layer consisting of a reaction product of the fluorine-containing polymer and the surface of the primary particles. The reaction product preferably comprises LiF.
摘要翻译：包含含有锂过渡金属氧化物粉末的正极活性材料的水基锂离子电池正极浆料，其中所述锂过渡金属氧化物粉末由初级粒子的聚集体组成，所述初级粒子包含涂层包含聚合物。聚合物优选为包含至少50重量％的氟的含氟聚合物。涂层优选包括第一内层和第二外层，第二外层包含含氟聚合物，第一内层由含氟聚合物与初级颗粒表面的反应产物组成。反应产物优选包含LiF。

6. 发明申请

WO2015132647A1 DOPED AND COATED LITHIUM TRANSITION METAL OXIDE CATHODE MATERIALS FOR BATTERIES IN AUTOMOTIVE APPLICATIONS 审中-公开
标题翻译：用于电动汽车应用的电镀和涂覆的锂离子转换金属氧化物阴极材料
公开(公告)号：WO2015132647A1
公开(公告)日：2015-09-11
申请号：PCT/IB2015/000260
申请日：2015-03-03
申请人： UMICORE , UMICORE KOREA LTD.
发明人： ZHU, Liang , PAULSEN, Jens , AHN, Hyo, Sun , HONG, HeonPyo
IPC分类号： H01M4/525 , H01M4/505 , H01M4/46 , H01M4/131 , H01M10/05
CPC分类号： H01M4/131 , C01G53/50 , C01P2004/03 , C01P2004/61 , C01P2004/80 , C01P2006/12 , C01P2006/40 , H01M4/0404 , H01M4/0435 , H01M4/1391 , H01M4/366 , H01M4/483 , H01M4/505 , H01M4/525 , H01M4/623 , H01M4/625 , H01M10/052 , H01M10/0525 , H01M10/0587 , H01M2004/028 , H01M2220/20 , Y02E60/122
摘要： A lithium metal oxide powder for use as a cathode material in a rechargeable battery, consisting of Li metal oxide core particles having a general formula Li 1+d (Ni x Mn y Co z Zr k M' m ) i-d 0 2±e Ar; wherein Al 2 0 3 is attached to the surface of the core particles; wherein 0≤d≤0.08, 0.2≤x≤0.9, 0 2 0 3 content in the powder is between 0.05 and 1 wt%.
摘要翻译：用作可再充电电池中的阴极材料的锂金属氧化物粉末，由具有通式Li 1 + d（Nix Mny Coz Zrk M'm）i-d 02±e Ar的Li金属氧化物核心颗粒组成; 其中Al 2 O 3附着在芯颗粒的表面上; 其中0≤d≤0.08,0.2≤x≤0.9,0

7. 发明申请

WO2014135923A1 OLIVINE COMPOSITION WITH IMPROVED CELL PERFORMANCE 审中-公开
标题翻译：具有改进的细胞性能的OLIVINE组合物
公开(公告)号：WO2014135923A1
公开(公告)日：2014-09-12
申请号：PCT/IB2013/051846
申请日：2013-03-08
申请人： UMICORE , UMICORE KOREA LTD.
发明人： KIM, DaeHyun , PAULSEN, Jens , HONG, HeonPyo
IPC分类号： H01M4/525 , H01M4/505
CPC分类号： H01M4/5825 , C01B25/45 , H01M10/052 , H01M10/0525 , H01M2004/021 , H01M2004/028
摘要： The invention discloses an olivine cathode material comprising Li, M and PO 4, having a non-stoichiometric composition wherein: -the phosphor stoichiometry PO 4 :[(Li+M)/2] is between 0.940and 1.020, -the lithium to metal ratio Li:M is between 1.040 and 1.150, and wherein M=Fe -x-z' Mn x D z', with 0.10 0, D being a dopant comprising either one or both of Cr and Mg.In one embodiment PO 4 :[(Li+M)/2] is between 0.960 and 1.000, resulting in an even better performing material. Performance is improved even more in another embodiment wherein PO 4 :[(Li+M)/2] is less than 1.000. Improvements in performance are also obtained for either an embodiment wherein the lithium to metal ratio Li:M is between 1.070 and 1.120; or an embodiment wherein the manganese to iron ratio Mn/(Mn+Fe) is between 0.25 and 0.75; or for another embodiment wherein z'
摘要翻译：本发明公开了一种包含Li，M和PO 4的橄榄石阴极材料，具有非化学计量组成，其中： - 荧光体化学计量PO 4：[（Li + M）/ 2]在0.940和1.020之间，锂与金属比例Li：M在1.040和1.150之间，其中M = Fe-xz'Mn x D z'，其中0.10 0，D是包含Cr和Mg中的一种或两种的掺杂剂。在一个实施方案中，PO 4：[（Li + M）/ 2]在0.960和1.000之间，导致更好的材料。在PO 4：[（Li + M）/ 2]小于1.000的另一个实施方案中，性能得到改善。对于其中锂与金属之比Li：M在1.070和1.120之间的实施例，也可获得性能的改进; 或其中锰与铁之比Mn /（Mn + Fe）为0.25至0.75的实施方案; 或另一个实施方案，其中z'<0.05。

8. 发明申请

WO2016055911A1 IMPURITY CONTAINING CATHODE MATERIAL WITH PREFERRED MORPHOLOGY AND METHOD TO PREPARE FROM IMPURITY CONTAINING METAL CARBONATE 审中-公开
标题翻译：具有优选形态的阴极材料的含量和从含有金属碳酸盐的含量制备的方法
公开(公告)号：WO2016055911A1
公开(公告)日：2016-04-14
申请号：PCT/IB2015/057492
申请日：2015-09-30
申请人： UMICORE , UMICORE KOREA LTD
发明人： PAULSEN, Jens , HONG, HeonPyo , OH, JinDoo
IPC分类号： H01M4/525 , H01M4/505 , H01M10/052
CPC分类号： H01M4/505 , C01G53/006 , C01G53/06 , C01G53/50 , C01P2002/50 , C01P2002/72 , C01P2004/03 , C01P2004/51 , C01P2006/11 , C01P2006/12 , C01P2006/40 , C01P2006/80 , H01M4/525 , H01M10/0525 , H01M2004/028
摘要： A carbonate precursor compound for manufacturing a lithium metal (M)-oxide powder usable as an active positive electrode material in lithium-ion batteries, M comprising 20 to 90 mol% Ni, 10 to 70 mol% Mn and 10 to 40 mol% Co, the precursor further comprising a sodium and sulfur impurity, wherein the sodium to sulfur molar ratio (Na/S) is 0.4
摘要翻译：用于制造锂离子电池用作活性正极材料的锂金属（M） - 氧化物粉末的碳酸酯前体化合物，M为20〜90摩尔％的Ni，10〜70摩尔％的Mn和10〜40摩尔％的Co 该前体还包含钠和硫杂质，其中钠与硫的摩尔比（Na / S）为0.4

9. 发明申请

WO2016055910A1 CARBONATE PRECURSORS FOR LITHIUM NICKEL MANGANESE COBALT OXIDE CATHODE MATERIAL AND THE METHOD OF MAKING SAME 审中-公开
标题翻译：用于镍铬锰氧化物阴极材料的碳酸盐前体及其制备方法
公开(公告)号：WO2016055910A1
公开(公告)日：2016-04-14
申请号：PCT/IB2015/057491
申请日：2015-09-30
申请人： UMICORE , UMICORE KOREA LTD
发明人： HU, Jin , HONG, HeonPyo , PAULSEN, Jens , OH, JinDoo , NELIS, Daniël , ROBERT, Eric
IPC分类号： H01M4/525 , H01M4/505 , H01M4/485
CPC分类号： H01M4/1391 , C01G53/006 , C01G53/44 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2004/32 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/0471 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/052 , Y02T10/7011
摘要： A method for producing a M-carbonate precursor of a Li-M oxide cathode material in a continuous reactor, wherein M=NixMnyCozAn, A being a dopant, with x>0, y>0,0≤z≤0.35, 0≤n≤0.02 and x+y+z+n=1, the method comprising the steps of: -providing a feed solution comprising Ni-, Mn-, Co-and A-ions, and having a molar metal content M" feed, -providing an ionic solution comprising either one or both of a carbonate and a bicarbonate solution, the ionic solution further comprising either one or both of Na-and K-ions, -providing a slurry comprising seeds comprising M'-ions and having a molar metal content M' seeds, wherein M'=Nix'Mny'Coz'A'n', A' being a dopant, with 0≤x'≤1, 0≤y'≤1, 0≤z'≤1, 0≤n'≤1 and x'+y'+z'+n'=1, and wherein the molar ratio M' seeds/M" feed is between 0.001 and 0.1, -mixing the feed solution, the ionic solution and the slurry in the reactor, thereby obtaining a reactive liquid mixture, -precipitating a carbonate onto the seeds in the reactive liquid mixture, thereby obtaining a reacted liquid mixture and the M-carbonate precursor, and -separating the M-carbonate precursor from the reacted liquid mixture.
摘要翻译：一种在连续反应器中制备Li-M氧化物阴极材料的M-碳酸酯前体的方法，其中M = NixMnyCozAn，A为掺杂剂，x> 0，y>0,0≤z≤0.35,0≤n ≤0.02，x + y + z + n = 1，该方法包括以下步骤：提供包含Ni-，Mn-，Co-和A-离子并且具有摩尔金属含量M“进料的进料溶液，提供包含碳酸盐和碳酸氢盐溶液中的一种或两种的离子溶液，所述离子溶液还包含Na-和K-离子中的一种或两种， - 提供包含包含M'离子并具有摩尔金属的种子的浆料含量M'种子，其中M'= Nix'Mny'Coz'A'n'，A'为掺杂剂，0≤x'≤1,0≤y'≤1,0≤z'≤1,0≤ n'≤1且x'+ y'+ z'+ n'= 1，其中M'种子/ M“进料的摩尔比为0.001至0.1，将进料溶液，离子溶液和浆料混合反应器，从而获得反应性液体混合物，将碳酸盐沉淀在反应性液体混合物中的种子上从而获得反应的液体混合物和M-碳酸酯前体，并将M-碳酸酯前体与反应的液体混合物分离。

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