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1. 发明申请

WO2005123272A2 LIQUID FEED FLAME SPRAY MODIFICATION OF NANOPARTICLES 审中-公开
标题翻译：液体进料火焰喷雾修饰纳米颗粒
公开(公告)号：WO2005123272A2
公开(公告)日：2005-12-29
申请号：PCT/US2005/006481
申请日：2005-02-28
申请人： THE REGENTS OF THE UNIVERSITY OF MICHIGAN , LAINE, Richard, M. , MARCHEL, Julien , AZURDIA, Jose , RENNENSUND, Roy
发明人： LAINE, Richard, M. , MARCHEL, Julien , AZURDIA, Jose , RENNENSUND, Roy
IPC分类号： B05D1/08
CPC分类号： C01B13/34 , B82Y30/00 , C01B13/145 , C01F7/021 , C01F7/027 , C01G1/02 , C01P2004/32 , C01P2004/34 , C01P2004/51 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2004/86 , C01P2006/10 , C01P2006/12 , C04B33/04 , C04B35/111 , C04B35/6263 , C04B35/6264 , C04B35/62665 , C04B35/628 , C04B35/62813 , C04B35/62818 , C04B35/62821 , C04B35/62826 , C04B41/009 , C04B41/4584 , C04B41/87 , C04B2235/3217 , C04B2235/322 , C04B2235/3222 , C04B2235/3224 , C04B2235/3225 , C04B2235/3232 , C04B2235/3241 , C04B2235/3279 , C04B2235/441 , C04B2235/5409 , C04B2235/5454 , C04B2235/77 , C09C1/407 , C09C1/42 , C23C4/123 , C23C4/134 , C23C24/00 , Y02T50/67 , C04B41/4537 , C04B41/5041 , C04B41/5027 , C04B41/5032 , C04B35/10
摘要： Nano- and micron sized metal oxide and mixed metal oxide particles are injected into a high temperature region wherein the temperature is between about 400 ° C and less than 2000 ° C, and collected as particles or as coatings wherein a particulate nature is substantially maintained. The particles are altered in at least one of phase, morphology, composition, and particle size distribution, and may achieve further changes in these characteristics by coinjection of metal oxide precursor in liquid form.
摘要翻译：将纳米和微米尺寸的金属氧化物和混合金属氧化物颗粒注入到温度在约400℃至小于2000℃之间的高温区域中，并作为颗粒或作为其颗粒性质的涂层基本保持。颗粒以相，形态，组成和粒度分布中的至少一种改变，并且可以通过液体形式的金属氧化物前体的共注入来实现这些特征的进一步变化。

2. 发明申请

WO2002100867A1 WELL-DEFINED NANOSIZED BUILDING BLOCKS FOR ORGANIC/INORGANIC NANOCOMPOSITES 审中-公开
标题翻译：用于有机/无机纳米复合材料的定义明确的纳米结构块
公开(公告)号：WO2002100867A1
公开(公告)日：2002-12-19
申请号：PCT/US2001/048451
申请日：2001-10-29
申请人： THE REGENTS OF THE UNIVERSITY OF MICHIGAN , LAINE, Richard, M. , TAMAKI, Ryo , CHOI, Jiwon
发明人： LAINE, Richard, M. , TAMAKI, Ryo , CHOI, Jiwon
IPC分类号： C07F7/21
CPC分类号： C07F7/21
摘要： Functionalized silsesquioxanes containing from 6 to 24 silicon atoms and minimally about 67 mol percent RSiO 3/2 moieties where R is a phenyl group bearing a chemically reactive functional group are highly suitable for use as nanoparticles in producing highly ordered nanocomposites of many types, containing a high proportion of interphase. The nanocomposites have unusual physicochemical properties due to the use of uniform, highly functionalized nanoparticles.
摘要翻译：含有6至24个硅原子的官能化倍半硅氧烷和最低约67mol％的RSiO 3/2部分，其中R是具有化学反应性官能团的苯基，其高度适用于制备许多类型的高度有序纳米复合材料的纳米粒子，其含有高相间比例。由于使用均匀的高官能化纳米粒子，纳米复合材料具有不寻常的物理化学性质。

3. 发明申请

WO2006062219A1 ULTRAVIOLET TRANSMISSIVE POLYHEDRAL SILSESQUIOXANE POLYMERS 审中-公开
标题翻译：超紫外线透射聚苯乙烯聚合物
公开(公告)号：WO2006062219A1
公开(公告)日：2006-06-15
申请号：PCT/JP2005/022719
申请日：2005-12-05
申请人： MATSUSHITA ELECTRIC WORKS, LTD. , THE REGENTS OF THE UNIVERSITY OF MICHIGAN , TAKAMURA, Norihiro , SHINOTANI, Ken-ichi , LAINE, Richard, M. , VICULIS, Lisa
发明人： TAKAMURA, Norihiro , SHINOTANI, Ken-ichi , LAINE, Richard, M. , VICULIS, Lisa
IPC分类号： C08G77/06 , C08G77/14 , C09D183/04
CPC分类号： C09D183/04 , C08G77/045 , C08G77/06 , C08G77/14 , H01L23/296 , H01L27/14623 , H01L27/14625 , H01L31/0216 , H01L31/02164 , H01L2924/0002 , H01L2924/00
摘要： Inorganic/organic hybrid polymers containing silsesquioxane cages are robust and exhibit desirable physical properties such as strength, hardness, and optical transparency at infrared and ultraviolet wavelengths. The polymers are prepared by polymerizing functionalized polyhedral silsesquioxane monomers such as polyhedral silsesquioxanes bearing two complementarily reactive functional groups bonded to cage silicon atoms by means of spacer moieties. The spacer moieties allow for steric mobility and more complete cure than polyhedral silsesquioxanes bearing reactive functional groups bound directly to cage silicon atoms.
摘要翻译：含有倍半硅氧烷笼的无机/有机杂化聚合物是牢固的并且表现出期望的物理性质，例如红外和紫外线波长下的强度，硬度和光学透明度。聚合物是通过聚合功能化的多面体倍半硅氧烷单体制备的，例如通过间隔基部分带有两个与笼状硅原子键合的互补反应性官能团的多面体倍半硅氧烷。间隔基部分允许空间移动和更完全的固化比承载反应性官能团直接结合到笼状硅原子的多面体倍半硅氧烷。

4. 发明申请

WO2010062695A2 PROPERTIES TAILORING IN SILSESQUIOXANES 审中-公开
标题翻译：在SILESESQUIOXANES的物业定制
公开(公告)号：WO2010062695A2
公开(公告)日：2010-06-03
申请号：PCT/US2009/062815
申请日：2009-10-30
申请人： THE REGENTS OF THE UNIVERSITY OF MICHIGAN , LAINE, Richard, M. , SULAIMAN, Santy
发明人： LAINE, Richard, M. , SULAIMAN, Santy
IPC分类号： C08G77/38 , C08G77/08
CPC分类号： C08G77/045
摘要： Fluoride catalyzed rearrangement reactions of polymeric silsesquioxanes [RSiO 1.5 ] n involve reacting at least one silsesquioxane material with a catalytic amount of an organic fluoride at a temperature ranging from about -50C to about 120C thereby forming a reaction mixture for a period ranging from 60 minutes to 48 hours. To the reaction mixture, a quenching agent is added to remove fluoride from the reaction mixture. A silsesquioxane cage compound can be isolated from the reaction mixture using a precipitation or other extraction process.
摘要翻译：聚合倍半硅氧烷[RSiO1.5] n的氟化物催化重排反应包括在约-50℃至约120℃的温度范围内使至少一种倍半硅氧烷材料与催化量的有机氟化物反应，从而形成反应混合物，时间范围为60 分钟至48小时。向反应混合物中加入淬灭剂以从反应混合物中除去氟化物。可以使用沉淀或其它提取方法从反应混合物中分离倍半硅氧烷笼形化合物。

5. 发明申请

WO2010011891A2 METHOD OF PRESSURELESS SINTERING PRODUCTION OF DENSIFIED CERAMIC COMPOSITES 审中-公开
标题翻译：无压烧结生产密度陶瓷复合材料的方法
公开(公告)号：WO2010011891A2
公开(公告)日：2010-01-28
申请号：PCT/US2009/051644
申请日：2009-07-24
申请人： THE REGENTS OF THE UNIVERSITY OF MICHIGAN , LAINE, Richard, M. , KIM, Min
发明人： LAINE, Richard, M. , KIM, Min
IPC分类号： C04B35/624 , C04B35/119 , C04B35/64 , C04B35/48 , C04B35/10
CPC分类号： C04B35/119 , B82Y30/00 , C04B35/48 , C04B35/4885 , C04B35/624 , C04B35/62665 , C04B35/62813 , C04B35/62886 , C04B35/6325 , C04B35/64 , C04B2235/3206 , C04B2235/3217 , C04B2235/322 , C04B2235/3222 , C04B2235/3225 , C04B2235/3229 , C04B2235/3244 , C04B2235/3272 , C04B2235/3275 , C04B2235/3279 , C04B2235/3284 , C04B2235/441 , C04B2235/449 , C04B2235/5409 , C04B2235/5445 , C04B2235/5454 , C04B2235/604 , C04B2235/608 , C04B2235/6562 , C04B2235/765 , C04B2235/77 , C04B2235/785 , C04B2235/786
摘要： Methods of making and compositions of dense sintered ceramic nano- and micro-composite materials that are highly stable in a variety of conditions and exhibit superior toughness and strength. Liquid feed flame spray pyrolysis techniques form a plurality of nanoparticles ( e.g ., powder), each having a core region including a first metal oxide composition comprising Ce and/or Zr or other metals and a shell region including a second metal oxide composition comprising Al or other metals. In certain aspects, the core region comprises a partially stabilized tetragonal ZrO 2 and the shell region comprises an α-Al 2 O 3 phase. The average actual density of the ceramic after sintering is greater than 50% and up to or exceeding 90% of a theoretical density of the ceramic.
摘要翻译：制造和组合致密烧结陶瓷纳米和微米复合材料的方法，其在各种条件下高度稳定并且表现出优异的韧性和强度。液体进料火焰喷雾热解技术形成多个纳米颗粒（例如粉末），每个纳米颗粒具有包含含Ce和/或Zr或其它金属的第一金属氧化物组合物的芯区和包含壳区包含Al或其他金属的第二金属氧化物组合物。在某些方面，核心区域包含部分稳定的四方ZrO 2和壳区域包含α-Al 2 O 3相。烧结后陶瓷的平均实际密度大于50％并且高达或超过陶瓷理论密度的90％。

6. 发明申请

WO2005039744A2 FACILE SYNTHESIS OF POLYHEDRAL SILSESQUIOXANE ANIONS AND USE THEREOF 审中-公开
标题翻译：多孔珊瑚十字烷阴离子的容易合成及其用途
公开(公告)号：WO2005039744A2
公开(公告)日：2005-05-06
申请号：PCT/US2004/035314
申请日：2004-10-25
申请人： THE REGENTS OF THE UNIVERSITY OF MICHIGAN , HASEGAWA, Isao , LAINE, Richard, M. , ASUNCION, Michael, Z. , TAKAMURA, Norihiro
发明人： HASEGAWA, Isao , LAINE, Richard, M. , ASUNCION, Michael, Z. , TAKAMURA, Norihiro
IPC分类号： B01F
CPC分类号： C08G77/04 , B27K3/153 , C07F7/21 , C08G77/02 , C08G77/045 , C08G77/08 , C08L83/04 , C08L97/02
摘要： Polyhedral silsesquioxane anions are economically prepared by reaction of a silica source derived from combusted organic material with a quaternary ammonium hydroxide compound. Reaction of the resulting anions with chlorosilanes may be effected in near stoichiometric fashion in organic solvent containing reactive quantities of organic acids such as formic acid. The functional groups on the resulting functionalized silsesquioxanes may be substituted for other functional groups by reaction with di- or polysiloxanes in the presence of a synthetic ion exchange resin.
摘要翻译：多面体倍半硅氧烷阴离子通过来源于燃烧有机材料的二氧化硅源与季铵氢氧化物化合物的反应而经济地制备。所得阴离子与氯硅烷的反应可以以接近化学计量的方式在含有反应性量的有机酸如甲酸的有机溶剂中进行。所得官能化倍半硅氧烷上的官能团可通过在合成离子交换树脂存在下与二硅氧烷或聚硅氧烷反应而取代其他官能团。

7. 发明申请

WO2013109787A1 GLYCOXY SILANES AS A SOURCE OF SILICA AND SILICATE PRECIPITATES 审中-公开
标题翻译： GLYCOXY SILANES作为二氧化硅和硅酸盐原料的来源
公开(公告)号：WO2013109787A1
公开(公告)日：2013-07-25
申请号：PCT/US2013/021991
申请日：2013-01-17
申请人： LAINE, Richard, M. , MARCHAL, Julien, C. , POPOVA, Vera , KRUG, David, J.
发明人： LAINE, Richard, M. , MARCHAL, Julien, C. , POPOVA, Vera , KRUG, David, J.
IPC分类号： C01B33/18 , B01J21/08 , B01J29/04 , B82B3/00
CPC分类号： C01B33/193 , C01B33/18 , C01B33/187 , C01B39/02 , C01P2006/12 , C01P2006/14 , C01P2006/80
摘要： The present invention discloses glycoxy silanes as a source of silica and silica precipitated by advantageous chemical reactions preferably beginning with biogenic silica. Alkoxy C-O-S 1 are hydrolyzed in a controlled fashion to nucleate formation of nanoparticles of silica. The growth rate of the particles is controlled by various parameters such that particles of known sizes, size distributions, specific surface areas and pore sizes and size distributions are recovered.
摘要翻译：本发明公开了作为二氧化硅和二氧化硅来源的糖羟基硅烷，通过有利的化学反应沉淀，优选从生物二氧化硅开始。烷氧基C-O-S1以受控的方式水解，以形成二氧化硅纳米颗粒。颗粒的生长速率由各种参数控制，从而回收已知尺寸，尺寸分布，比表面积，孔径和尺寸分布的颗粒。

8. 发明申请

WO2010017373A2 PLASMA PROCESSES FOR PRODUCING SILANES AND DERIVATIVES THEREOF 审中-公开
标题翻译：用于生产硅烷及其衍生物的等离子体方法
公开(公告)号：WO2010017373A2
公开(公告)日：2010-02-11
申请号：PCT/US2009/052981
申请日：2009-08-06
申请人： ELECTRODYNAMIC APPLICATIONS, INC. , LAINE, Richard, M. , MASSEY, Dean, Richard , PETERSON, Peter, Young
发明人： LAINE, Richard, M. , MASSEY, Dean, Richard , PETERSON, Peter, Young
IPC分类号： C01B33/04 , B01J19/08 , H05H1/00 , H01L31/20
CPC分类号： C22B7/001 , C01B33/023 , C01B33/025 , C01B33/037 , C22B1/02 , C22B1/244 , C22B5/10 , C22B61/00 , Y02P10/122 , Y02P10/214
摘要： The invention is generally related to process for generating one or more molecules having the formula Si x H y , where x and y are integers ≥1, such as silane, comprising the steps of: providing a silicon containing material, wherein the silicon containing material includes at least 20 weight percent silicon atoms based on the total weight of the silicon containing material; generating a plasma capable of vaporizing a silicon atom, sputtering a silicon atom, or both using a plasma generating device; and contacting the plasma to the silicon containing material in a chamber having an atmosphere that includes at least about 0.5 mole percent hydrogen atoms based on the total moles of atoms in the atmosphere; so that a molecule having the formula Si x H y; (e.g., silane) is generated. The process preferably includes a step of removing one or more impurities from the Si x H y (e.g., the silane) to form a clean Si x H y (e.g., silane). The process may also include a step of reacting the Si x H y (e.g., the silane) to produce a high purity silicon containing material such as electronic grade metallic silicon, photovoltaic grade metallic silicon, or both.
摘要翻译：本发明通常涉及用于产生具有式SixHy的一种或多种分子的方法，其中x和y是整数= 1，例如硅烷，包括以下步骤：提供含硅材料，其中含硅材料至少包括基于含硅材料的总重量的20重量％的硅原子; 产生能够蒸发硅原子的等离子体，使用等离子体发生装置溅射硅原子或二者; 并且基于气氛中的原子总摩尔数，在具有包括至少约0.5摩尔百分比的氢原子的气氛的室中将等离子体接触到含硅材料; 使得具有式SixHy的分子; （例如硅烷）。该方法优选包括从SixHy（例如硅烷）中除去一种或多种杂质以形成干净的SixHy（例如硅烷）的步骤。该方法还可以包括使SixHy（例如，硅烷）反应以产生高纯度含硅材料如电子级金属硅，光伏级金属硅或两者的步骤。

9. 发明申请

WO2006023299A1 UV-ABSORBING COATINGS AND METHODS OF MAKING THE SAME 审中-公开
标题翻译：紫外线吸收涂料及其制备方法
公开(公告)号：WO2006023299A1
公开(公告)日：2006-03-02
申请号：PCT/US2005/027985
申请日：2005-08-04
申请人： GUARDIAN INDUSTRIES CORP. , WANG, Yei-ping , LAINE, Richard, M.
发明人： WANG, Yei-ping , LAINE, Richard, M.
IPC分类号： C09D183/06
CPC分类号： C09D183/04 , C08G77/16 , C08G77/52 , Y10T428/31511 , Y10T428/31663
摘要： Methods of forming UV-absorbent transparent coatings and transparent substrates coated with the same allow for a relatively lower temperature cross-linkage reaction between a UV-absorbent compound and an epoxy-alkoxysilane. More specifically, UV-absorbent coatings on transparent substrates are formed by prepolymerizing a mixture consisting essentially of a benzophenone, an epoxy alkoxysilane and an organic catalyst at a temperature of between about 40°C to about 130°C and for a time sufficient such that between about 30% to about 70% of the epoxy alkoxysilane has been converted to a ring-opened oligomer or polymer. Such prepolymerized mixture may then be hydrolyzed and coated onto the surface of a transparent substrate, and thereafter cured at a temperature of less than about 200°C for a time sufficient to cross-link the hydrolyzed alkoxysilane with itself and the glass surface. Most preferably , the prepolymerized mixture is hydrolyzed prior to being coated onto the substrate in an acidic alcoholic solution. Preferred for use in the present invention as a UV-absorbent compound is tetrahydroxybenzophenone. The preferred epoxy alkoxysilane is 3-glycidoxypropyl trimethoxysilane. It is especially preferred that prepolymerization be effected in the presence of an organic catalyst, such as triethylamine (TEA).
摘要翻译：形成紫外线吸收透明涂层的方法和用其涂覆的透明基材允许紫外线吸收剂化合物和环氧烷氧基硅烷之间的相对较低的温度交联反应。更具体地说，在约40℃至约130℃的温度下，通过将基本上由二苯甲酮，环氧烷氧基硅烷和有机催化剂组成的混合物预聚合，形成透明基材上的紫外线吸收涂层，时间足够长，约30％至约70％的环氧烷氧基硅烷已经转化成开环的低聚物或聚合物。然后将这样的预聚合的混合物水解并涂覆在透明基材的表面上，然后在小于约200℃的温度下固化足够的时间以使水解的烷氧基硅烷与其自身和玻璃表面交联。最优选地，将预聚合的混合物在用酸性醇溶液涂覆在基材上之前水解。作为UV吸收剂化合物优选用于本发明的是四羟基二苯甲酮。优选的环氧烷氧基硅烷是3-缩水甘油氧基丙基三甲氧基硅烷。特别优选的是，在有机催化剂如三乙胺（TEA）的存在下进行预聚合。

10. 发明申请

WO2010017364A2 LOW COST ROUTES TO HIGH PURITY SILICON AND DERIVATIVES THEREOF 审中-公开
标题翻译：低成本的路线到高纯硅及其衍生物
公开(公告)号：WO2010017364A2
公开(公告)日：2010-02-11
申请号：PCT/US2009/052965
申请日：2009-08-06
申请人： MAYATERIALS, INC. , LAINE, Richard, M. , KRUG, David, James , MARCHAL, Julien, Claudius , MCCOLM, Andrew, Stewart
发明人： LAINE, Richard, M. , KRUG, David, James , MARCHAL, Julien, Claudius , MCCOLM, Andrew, Stewart
IPC分类号： C01B33/037 , B09B3/00 , C22B7/00
CPC分类号： C22B7/001 , C01B33/023 , C01B33/025 , C01B33/037 , C22B1/02 , C22B1/244 , C22B5/10 , C22B61/00 , Y02P10/122 , Y02P10/214
摘要： The present invention is directed to a method for providing an agricultural waste product having amorphous silica, carbon, and impurities; extracting from the agricultural waste product an amount of the impurities; changing the ratio of carbon to silica; and reducing the silica to a high purity silicon (e.g., to photovoltaic silicon).
摘要翻译：本发明涉及提供具有无定形二氧化硅，碳和杂质的农业废弃物的方法; 从农业废弃物中提取一定量的杂质; 改变碳与二氧化硅的比例; 并将二氧化硅还原成高纯度硅（例如还原成光伏硅）。

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