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    • 5. 发明申请
    • PROCESS FOR CHARACTERIZATION OF MICRO AND MESO POROUS MATERIALS
    • 微孔和多孔材料表征的方法
    • WO2015002687A1
    • 2015-01-08
    • PCT/US2014/034513
    • 2014-04-17
    • THE PENN STATE RESEARCH FOUNDATION
    • QAJAR, AliRAJAGOPALAN, RamakrishnanFOLEY, Henry, C.
    • G01N15/02G01N5/02G01N9/02B01D53/02
    • G01N15/088
    • A process for characterizing micro, meso, and/or macro porous materials is provided. The process includes providing a volumetric and/or gravimetric adsorption system, the adsorption system having an adsorption chamber and a probe gas at a first temperature. In addition, a porous material to be characterized is provided and placed within the adsorption chamber. Thereafter, a porosimetry run is conducted on the porous material. The porosimetry run includes: (a) selecting an uptake target value; (b) selecting a target interval bounding the target uptake target value; (c) adjusting pressure within the adsorption chamber in order for the porous sample to reach the target uptake value; (d) adjusting pressure within the adsorption chamber until the pressure within the adsorption chamber is within the target interval for a predetermined amount of time; and (e) repeating steps (a)-(d) until the porosimetry run is complete.
    • 提供了表征微观,中观和/或大孔多孔材料的方法。 该方法包括提供体积和/或重量吸附系统,吸附系统在第一温度下具有吸附室和探针气体。 此外,要表征的多孔材料被提供并放置在吸附室内。 此后,在多孔材料上进行孔隙率测定。 孔隙率测定法包括:(a)选择摄取目标值; (b)选择限定目标摄取目标值的目标间隔; (c)调节吸附室内的压力以使多孔样品达到目标吸收值; (d)调节吸附室内的压力,直到吸附室内的压力达到目标间隔预定时间为止; 和(e)重复步骤(a) - (d)直到孔隙率测定运行完成。