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1. 发明申请

WO2012134643A2 PREPARATION OF ANTIPLASTICIZERS FOR THERMOPLASTIC POLYESTERS 审中-公开
标题翻译：热塑性聚酯抗菌剂的制备
公开(公告)号：WO2012134643A2
公开(公告)日：2012-10-04
申请号：PCT/US2012/024554
申请日：2012-02-09
申请人： STEPAN COMPANY , TABOR, Rick , MIROUS, Brian, K. , LAMBERT, Timothy, L. , O'BRIEN, Michael, E. , LEVINSON, Matthew, I. , DERSHOWITZ, Daniel, J.
发明人： TABOR, Rick , MIROUS, Brian, K. , LAMBERT, Timothy, L. , O'BRIEN, Michael, E. , LEVINSON, Matthew, I. , DERSHOWITZ, Daniel, J.
IPC分类号： C08K5/12 , C08L67/02 , C07C69/82
CPC分类号： C08K5/1345 , C07C67/03 , C07C67/29 , C07C69/82 , C08K5/12 , Y02P20/582
摘要： A process for making bis(aryloxyalkyl)terephthalates useful as antiplasticizers for thermoplastic polyesters is disclosed. Dimethyl terephthalate is reacted with an excess of an aryloxyalkanol in the presence of a condensation catalyst to produce an intermediate mixture comprising a bis(aryloxyaIkyl)terephthalate, a mono(aryloxyalkyl)terephthalate, and unreacted aryloxyalkanol. This mixture continues to react at reduced pressure while unreacted aryloxyalkanol is removed and the mono-ester content is reduced to less than 1 mole % based on the combined amounts of mono- and bis-esters. Both steps are performed substantially in the absence of oxygen. Additional unreacted aryloxyalkanol is then removed to provide a purified bis(aryloxyalkyl)terephthalate having an overall purity of at least 98 mole % and a yellowness index less than 10. Careful control over catalysis, exposure to air, and other process conditions enables the preparation of high yields of bis(aryloxyalkyl)terephthalates that have low color and other valuable attributes. A method of producing bis(aryloxyalkyl)terephthalate articles having improved compressive strength is also disclosed.
摘要翻译：公开了一种制备用作热塑性聚酯的抗增塑剂的双（芳氧基烷基）对苯二甲酸酯的方法。在缩合催化剂的存在下，对苯二甲酸二甲酯与过量的芳氧基烷醇反应生成包含双（芳氧基烷基）对苯二甲酸酯，单（芳氧基烷基）对苯二甲酸酯和未反应的芳氧基烷醇的中间体混合物。该混合物在减压下继续反应，同时除去未反应的芳氧基烷醇，并且基于单酯和双酯的组合量，单酯含量降低至小于1摩尔％。两个步骤基本上在不存在氧的情况下进行。然后除去另外的未反应的芳氧基烷醇，以提供纯度为至少98摩尔％，黄度指数小于10的纯化双（芳氧基烷基）对苯二甲酸酯。小心控制催化，暴露于空气和其它工艺条件使得能够制备具有低颜色和其他有价值属性的双（芳氧基烷基）对苯二甲酸酯的高收率。还公开了一种制备具有改善的抗压强度的双（芳氧基烷基）对苯二甲酸酯制品的方法。

2. 发明申请

WO2009045926A1 AROMATIC POLYESTER POLYOLS AND AROMATIC POLYESTER POLYOL BLENDS CONTAINING BIORENEWABLE COMPONENTS AND METHODS OF MAKING 审中-公开
标题翻译：含有可生物组分的芳族聚酯多元醇和芳香族聚酯多元醇共混物及其制备方法
公开(公告)号：WO2009045926A1
公开(公告)日：2009-04-09
申请号：PCT/US2008/077993
申请日：2008-09-26
申请人： STEPAN COMPANY , LAMBERT, Timothy, L. , HICKEY, Leo, F. , YAO, Chunhua
发明人： LAMBERT, Timothy, L. , HICKEY, Leo, F. , YAO, Chunhua
IPC分类号： C08L63/00
CPC分类号： C08G18/06 , C08G18/36 , C08G18/4288 , C08G18/6662 , C08G63/20 , C08G63/668 , C08G63/916 , C08G2101/0025 , C08G2101/005 , C08G2105/02 , C08J9/141 , C08J2375/06
摘要： The present invention generally relates to natural oil derived raw materials reacted with aromatic polyester polyols. There are provided aromatic polyester polyol compositions comprising: (i) at least one aromatic acid component; (H) at least one hydroxylated component; (iii) at least one functionalized natural oil component; and (iv) optionally at least one catalyst component. The aromatic polyester polyo compositions can be formed by esterification and/or transesterification.
摘要翻译：本发明一般涉及与芳族聚酯多元醇反应的天然油衍生的原料。提供了芳族聚酯多元醇组合物，其包含：（i）至少一种芳族酸组分; （H）至少一个羟基化成分; （iii）至少一种官能化天然油组分; 和（iv）任选的至少一种催化剂组分。芳族聚酯多元组合物可以通过酯化和/或酯交换形成。

3. 发明申请

WO2005049551A1 METHOD OF PURIFYING HYDROXYALKYL AMIDE 审中-公开
标题翻译：纯化羟基谷氨酰胺的方法
公开(公告)号：WO2005049551A1
公开(公告)日：2005-06-02
申请号：PCT/US2004/036552
申请日：2004-11-01
申请人： CROMPTON CORPORATION , FOX, Brian, E. , LAMBERT, Timothy, L.
发明人： FOX, Brian, E. , LAMBERT, Timothy, L.
IPC分类号： C07C231/24
CPC分类号： C10L10/08 , C07C231/24 , C10L1/224 , C07C233/18 , C07C233/20
摘要： A method for purifying hydroxyalkyl amide of residual alkanolamine by using nonpolar solvent, an acidic Ph, salt solutions and an elevated temperature.
摘要翻译：通过使用非极性溶剂，酸性Ph盐溶液和升高的温度来纯化残余链烷醇胺的羟烷基酰胺的方法。

4. 发明申请

WO2004089870A2 DIPHENYLAMINE ALKYLATED WITH OLEFIN MIXTURES CONTAINING FRACTIONS WITH VARYING DEGREES OF ACTIVITY 审中-公开
标题翻译：含烯烃混合物烷基化二苯胺，活性不同
公开(公告)号：WO2004089870A2
公开(公告)日：2004-10-21
申请号：PCT/US2004/010417
申请日：2004-04-02
申请人： CROMPTON CORPORATION , DUYCK, Karl, J. , LAMBERT, Timothy, L.
发明人： DUYCK, Karl, J. , LAMBERT, Timothy, L.
IPC分类号： C07C209/00
CPC分类号： C08K5/18 , C07C211/55 , C10L1/223 , C10L1/2383 , C10M133/14 , C10M133/54 , C10M2203/1006 , C10M2205/02 , C10M2207/16 , C10M2215/064 , C10M2215/26 , C10M2215/28 , C10M2219/044 , C10M2219/046 , C10M2223/045 , C10N2230/10 , C10N2240/10 , C08L21/00 , C10N2210/08 , C10N2210/02
摘要： Disclosed herein is a process for the preparation of alkylated diarylamines comprising adding said diarylamine an olefin mixture containing highly reactive fractions, as well as fractions exhibiting a relatively lower chemical reactivity, in the presence of an acidic clay catalyst at a temperature low enough to prevent substantial deactivation of the catalyst until the addition is complete and then increasing the temperature to increase the alkylation rate of the less reactive fractions.
摘要翻译：本文公开了制备烷基化二芳基胺的方法，其包括在酸性粘土催化剂存在下将包含高反应性级分的烯烃混合物以及表现出相对较低化学反应性的级分加入所述二芳基胺在足够低的温度下以防止催化剂实质性失活，直到加入完成，然后升高温度以提高反应性较低的馏分的烷基化速率。

5. 发明申请

WO2005049550A1 METHOD OF MAKING HYDROXYALKYL AMIDE CONTAINING REDUCED LEVEL OF UNREACTED ALKANOLAMINE 审中-公开
标题翻译：制备含有降低的非线性烷醇胺水平的羟基甲基酰胺的方法
公开(公告)号：WO2005049550A1
公开(公告)日：2005-06-02
申请号：PCT/US2004/036553
申请日：2004-11-01
申请人： CROMPTON CORPORATION , FOX, Brian, E. , LAMBERT, Timothy, L.
发明人： FOX, Brian, E. , LAMBERT, Timothy, L.
IPC分类号： C07C231/02
CPC分类号： C07B43/06 , C07C231/02 , C10L1/221 , C10L1/224 , C10L10/08 , C07C233/18
摘要： A method for reacting alkanolamine with ester in the presence of a metal silicate compound and, optionally, a catalyst, to produce a hydroxyalkyl amide composition with a decreased level of alkanolamine and residual catalyst.
摘要翻译：在金属硅酸盐化合物和任选的催化剂的存在下使链烷醇胺与酯反应的方法，以产生具有降低的链烷醇胺和残余催化剂水平的羟烷基酰胺组合物。

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