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1. 发明申请

WO2012084219A1 PREPARATION OF A FAC-ISOMER FOR A TRIS HOMOLEPTIC METAL COMPLEX 审中-公开
标题翻译：用于TRIS HOMOLEPTIC金属复合物的FAC-ISOMER的制备
公开(公告)号：WO2012084219A1
公开(公告)日：2012-06-28
申请号：PCT/EP2011/006465
申请日：2011-12-21
申请人： SOLVAY SA , VAN PEE, Véronique , CATINAT, Jean-Pierre
发明人： VAN PEE, Véronique , CATINAT, Jean-Pierre
IPC分类号： C07F15/00
CPC分类号： C07F15/0033 , C07F15/0086
摘要： The present application provides a use of a mixture comprising less than 75 vol.% of an organic solvent and more than 25 vol.% of water in a preparation of a fac -isomei of a tris homoleptic metal complex, in the presence or the absence of an added salt, and with the proviso that when an added salt contains at least two oxygen atoms, it is used in an amount such that the molar ratio of the salt to the metal in a metal compound used as starting material is less than 1. The present application also provides a method of preparing a fac -isomer for a tris homoleptic metal complex using the mixture.
摘要翻译：本申请提供了在存在或不存在的情况下，在制备三顺反异构金属络合物的制剂中使用包含少于75体积％的有机溶剂和大于25体积％的水的混合物的附加盐，条件是当加入的盐含有至少两个氧原子时，其用量使得用作原料的金属化合物中的盐与金属的摩尔比小于1 本申请还提供了一种使用该混合物制备三异亮氨酸金属络合物的聚合物异构体的方法。

2. 发明申请

WO2009106554A1 POLYMER COMPOSITION, POLYMER MEMBRANE COMPRISING THE POLYMER COMPOSITION, PROCESS FOR PREPARING IT AND FUEL CELL COMPRISING THE MEMBRANE 审中-公开
标题翻译：聚合物组合物，包含聚合物组合物的聚合物膜，其制备方法和包含膜的燃料电池
公开(公告)号：WO2009106554A1
公开(公告)日：2009-09-03
申请号：PCT/EP2009/052250
申请日：2009-02-26
申请人： SOLVAY (Société Anonyme) , MARTIN, Roland , CATINAT, Jean-Pierre , CAILLE, Jean-Raphael , VAN PEE, Véronique
发明人： MARTIN, Roland , CATINAT, Jean-Pierre , CAILLE, Jean-Raphael , VAN PEE, Véronique
IPC分类号： C08G73/18 , B01D71/62 , B01D71/82 , H01B1/12 , H01M8/10 , B01D67/00
CPC分类号： C08L79/04 , B01D71/62 , B01D71/82 , B01D2325/26 , C08J5/2256 , C08J2379/04 , H01B1/122 , H01M8/103 , H01M8/1048 , H01M8/1067 , H01M8/1072 , H01M2300/0082 , H01M2300/0091 , Y02P70/56
摘要： The invention relates to: - a polymer composition comprising (a) a polybenzimidazole derived from (a1) at least one bis-(ortho-diamino) aromatic compound and (a2) at least one aromatic carboxylic acid or derivative thereof, each containing at least two acid groups and at least one hydroxyl group in α - position of a carboxylic group; (b) orthophosphoric acid; and (c) polyphosphoric acids of the formula (I) HO [P(O) (OH)]n H, wherein n is an integer from 2 to 20, wherein the polyphosphoric acids of formula (I) are present in an amount of less than 2 mol %, based upon the sum of moles of orthophosphoric acid (b) and polyphosphoric acids (c), and wherein (b) is present in an amount of 1 to 75 moles per mol of a benzimidazole group formed from (al) and (a2), - a polymer membrane comprising the polymer composition, - a preferred process for preparing the membrane, and - a fuel cell comprising the membrane.
摘要翻译：本发明涉及： - 聚合物组合物，其包含（a）衍生自（a1）至少一种双 - （邻 - 二氨基）芳族化合物的聚苯并咪唑和（a2）至少一种芳族羧酸或其衍生物，其至少包含两个酸基和至少一个位于羧基的位置的羟基; （b）正磷酸; 和（c）式（I）HO [P（O）（OH）] n H的多磷酸，其中n是2至20的整数，其中式（I）的多磷酸以基于正磷酸（b）和多磷酸（c）的摩尔数之和小于2摩尔％，并且其中（b）的存在量为每摩尔由（a1）形成的苯并咪唑基1至75摩尔）和（a2）， - 包含聚合物组合物的聚合物膜， - 制备膜的优选方法，和 - 包含该膜的燃料电池。

3. 发明申请

WO2013098189A1 PREPARATION OF HETEROLEPTIC METAL COMPLEXES 审中-公开
标题翻译：异种金属复合物的制备
公开(公告)号：WO2013098189A1
公开(公告)日：2013-07-04
申请号：PCT/EP2012/076396
申请日：2012-12-20
申请人： SOLVAY SA , CATINAT, Jean-Pierre
发明人： CATINAT, Jean-Pierre
IPC分类号： C07F15/00
CPC分类号： H01L51/0085 , C07F15/0033 , H01L51/5012
摘要： A process for the manufacture of heteroleptic complexes of a transition metal M having the general formula [M(L) n L'] wherein M is Ir, Rh, Pt or Pd and n is 2 for M = Ir or Rh and n is 1 for M = Pt or Pd and L is a bidentate cyclometallated ligand coordinated to the metal M through covalent metal-C and dative donor-atom-metal bonds,by reacting a halo-bridged dimer of general formula [L n M(µ-X) 2 )ML n ] with a bidentate ligand compound of formula L'-H or a halo-bridged dimer of general formula [L' n M(µ-X) 2 -ML' n ] with a ligand compound of formula L-H where (µ-X) represents a bridging halide in a solvent mixture of an organic solvent and water comprising more than 25 vol% of water at a temperature of from 50 to 260°C in the presence of from 0 to 5 molar equivalents relative to the number of moles of halide X-ion introduced into the reaction mixture through the halo-bridged dimer of a scavenger for halide X-ion and in the presence of from 0 to 0.8 moles, based on the molar amount of transition metal in the halo-bridged dimer of an added salt and of from 0 to 10 vol%, based on the total volume of the solvent mixture, of a solubilisation agent increasing the solubility of the halo-bridged dimer in the reaction mixture.
摘要翻译：制备具有通式[M（L）nL']的过渡金属M的杂光配合物的方法，其中M为Ir，Rh，Pt或Pd，对于M = Ir或Rh，n为2，n为1，n为1， M = Pt或Pd，L是通过共价金属-C和二价供体 - 原子 - 金属键与金属M配位的二齿环金属化配体，通过使通式[LnM（μ-X）2）的卤代桥连的二聚体， MLn]与式L'-H的双齿配体化合物或通式[L'nM（μ-X）2-ML'n]的卤代桥连二聚体与式LH的配体化合物反应，其中（μ-X）在相对于卤化物的摩尔数为0至5摩尔当量的存在下，在50至260℃的温度下，在有机溶剂和包含超过25体积％的水的溶剂混合物中的桥联卤化物通过用于卤化物X离子的清除剂的卤代桥连的二聚体将X离子引入反应混合物中，并且在0至0.8摩尔存在下，基于反式摩尔数在加成盐的卤代桥连二聚体中的金属和基于溶剂混合物的总体积的0至10体积％的增溶剂，其增加了卤代桥连二聚体在反应混合物中的溶解度。

4. 发明申请

WO2013045402A1 LIGHT EMITTING MATERIAL 审中-公开
标题翻译：发光材料
公开(公告)号：WO2013045402A1
公开(公告)日：2013-04-04
申请号：PCT/EP2012/068791
申请日：2012-09-24
申请人： SOLVAY SA , CATINAT, Jean-Pierre , MAUNOURY, Jonathan
发明人： CATINAT, Jean-Pierre , MAUNOURY, Jonathan
IPC分类号： C09K11/06 , H01L51/50
CPC分类号： C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1044 , C09K2211/185 , H01L51/0067 , H01L51/0085 , H01L51/5016
摘要： This invention pertains to novel phosphorescent light emitting materials and more particularly to blue-emitting materials involving metallic complexes wherein at least one ligand comprises a 9,9'-spirobifluorenyl and/or a 9,9-diphenyl-9H-fluorenyl moiety.
摘要翻译：本发明涉及新型磷光发光材料，更具体地涉及涉及金属络合物的蓝色发射材料，其中至少一种配体包含9,9'-螺二芴基和/或9,9-二苯基-9H-芴基部分。

5. 发明申请

WO2013098177A1 HETEROLEPTIC LIGHT-EMIITING COMPLEXES 审中-公开
标题翻译：异常光敏复合物
公开(公告)号：WO2013098177A1
公开(公告)日：2013-07-04
申请号：PCT/EP2012/076329
申请日：2012-12-20
申请人： SOLVAY SA , CATINAT, Jean-Pierre
发明人： CATINAT, Jean-Pierre
IPC分类号： C09K11/06 , H05B33/14 , H01L51/00 , C07F15/00 , H05B33/18
CPC分类号： H01L51/0085 , C07F5/069 , C07F15/0033 , C09K11/06 , C09K2211/1029 , C09K2211/1044 , C09K2211/185 , C09K2211/188 , H01L51/5012 , H01L51/5016 , H05B33/14 , H05B33/18
摘要： Heteroleptic light emitting complexes having the general formula M(L 1 ) n (L 2 ) m wherein a) L 1 has the formula E1 -E2, wherein E1 is a 6-membered heteroaryl ring bound to the metal atom M by a dative bond and containing at least one donor hetero atom and E2 is bound to the metal atom by covalent or dative bonds and is selected from the group consisting of substituted or un-substituted C 5 -C 30 aryl and substituted or un-substituted C 2 -C 30 heteroaryl groups, b) ligand L 2 is selected from the group consisting of 1 -(2,6 disubstituted phenyl)-2- phenyl-1 H- imidazole ligands or 5-(2,6 disubstituted phenyl)-1-phenyl-1 H- pyrazole ligands, and c) M is a non-radioactive transition metal with an atomic number of at least 40 and the sum of m and n is equal to half of the bond valency of metal M
摘要翻译：具有通式M（L1）n（L2）m的异烟光发光配合物，其中a）L1具有式E1 -E2，其中E1是通过分层键与金属原子M结合并含有至少一个供体杂原子和E2通过共价或二价键与金属原子结合，并且选自取代或未取代的C 5 -C 30芳基和取代或未取代的C 2 -C 30杂芳基，b）配体 L2选自1-（2,6-二取代苯基）-2-苯基-1H-咪唑配体或5-（2,6-二取代苯基）-1-苯基-1H-吡唑配体，c ）M是原子序数至少为40的非放射性过渡金属，m和n之和等于金属M的键合价的一半

6. 发明申请

WO2004043941A1 PROCESS FOR THE MANUFACTURE OF 1,2-EPOXY-3-CHLOROPROPANE 审中-公开
标题翻译： 1,2-环氧-3-氯代壬烯的制备方法
公开(公告)号：WO2004043941A1
公开(公告)日：2004-05-27
申请号：PCT/EP2003/012519
申请日：2003-11-10
申请人： SOLVAY (SOCIÉTÉ ANONYME) , STREBELLE, Michel , CATINAT, Jean-Pierre
发明人： STREBELLE, Michel , CATINAT, Jean-Pierre
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , C07D303/08
摘要： Process for the manufacture of 1,2-epoxy-3-chloropropane by reaction between allyl chloride and hydrogen peroxide in the presence of a catalyst and in the possible presence of at least one solvent, in which the allyl chloride employed comprises less than 2000 ppm by weight of 1,5-hexadiene.
摘要翻译：在催化剂存在下和在至少一种溶剂的存在下，烯丙基氯和过氧化氢之间的反应制备1,2-环氧-3-氯丙烷的方法，其中使用的烯丙基氯含量小于2000ppm 的1,5-己二烯。

7. 发明申请

WO2002092586A1 PROCESS FOR MANUFACTURING AN OXIRANE 审中-公开
标题翻译：制造OXIRANE的方法
公开(公告)号：WO2002092586A1
公开(公告)日：2002-11-21
申请号：PCT/EP2002/007251
申请日：2002-05-10
申请人： SOLVAY (SOCIÉTÉ ANONYME) , CATINAT, Jean-Pierre , STREBELLE, Michel
发明人： CATINAT, Jean-Pierre , STREBELLE, Michel
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for manufacturing an oxirane by reaction between an olefin and a peroxide compound in a reactor containing a liquid phase, in the presence of water, one or more organic solvents, a catalyst and one or more compounds for increasing the selectivity of the catalyst toward epoxidation reactions, in which: if the process is performed in batchwise mode, the liquid phase present in the reactor when the reaction starts, if the process is performed continuously, all of the liquid phases that are fed continuously into the reactor has/have a total organic solvent content of at least 0.1 g/kg and of not more than 675 g/kg.
摘要翻译：在含有液相的反应器中，在水存在下，一种或多种有机溶剂，催化剂和一种或多种用于提高催化剂对环氧化的选择性的化合物的烯烃与过氧化物之间的反应制备环氧乙烷的方法反应，其中：如果该方法以间歇模式进行，则当反应开始时存在于反应器中的液相，如果连续进行该过程，则连续进料到反应器中的所有液相具有总共有机溶剂含量为至少0.1g / kg且不大于675g / kg。

8. 发明申请

WO2008122503A1 AQUEOUS HYDROGEN PEROXIDE SOLUTION, PROCESS FOR ITS PREPARATION AND USE THEREOF 审中-公开
标题翻译：过氧化氢水溶液，其制备方法及其用途
公开(公告)号：WO2008122503A1
公开(公告)日：2008-10-16
申请号：PCT/EP2008/053423
申请日：2008-03-20
申请人： SOLVAY (Société Anonyme) , LIEBENS, Armin T. , GANHY, Jean-Pierre , CATINAT, Jean-Pierre , VERMEIREN, Koen
发明人： LIEBENS, Armin T. , GANHY, Jean-Pierre , CATINAT, Jean-Pierre , VERMEIREN, Koen
IPC分类号： C01B15/01 , C01B15/023 , C07D301/12
CPC分类号： C01B15/01 , C01B15/023 , C07D301/12
摘要： The present invention refers to an aqueous hydrogen peroxide solution having a hydrogen peroxide concentration [H 2 O 2 ] expressed as % by weight of the solution and an apparent pH of from pHmin to pHmax, such that pH min = 3.45 - 0.0377 x [H 2 O 2 ] pH max = 3.76 - 0.0379 x [H 2 O 2 ]. The present invention also relates to a process for the preparation of said hydrogen peroxide solution and the use of said solution in a process for the epoxidation of olefins.
摘要翻译：本发明涉及以过氧化氢浓度[H 2 O 2 O 2]表示的过氧化氢水溶液，其表示为溶液的重量％，pH值为pHmin 至pHmax，使得pH = 3.45-0.07377×（2H 2 O 2）pH最大值= 3.76 - 0.0379×[H 2 O 2 O]。本发明还涉及制备所述过氧化氢溶液的方法和所述溶液在烯烃环氧化方法中的用途。

9. 发明申请

WO2012048819A1 NOVEL SPIROBIFLUORENE COMPOUNDS 审中-公开
标题翻译：新型螺旋体化合物
公开(公告)号：WO2012048819A1
公开(公告)日：2012-04-19
申请号：PCT/EP2011/005013
申请日：2011-10-07
申请人： SOLVAY (SOCIETE ANONYME) , BASCOUR, Dominique , CATINAT, Jean-Pierre
发明人： BASCOUR, Dominique , CATINAT, Jean-Pierre
IPC分类号： C09K11/06 , H05B33/14 , H05B33/20 , H01L51/00 , C07C25/22 , H01L51/50
CPC分类号： H01L51/0058 , C07C25/22 , C07C255/52 , C07C2603/94 , C07F5/025 , C09K2211/185 , H01L51/0072 , H01L51/0073 , H01L51/5016 , H01L51/5048 , H05B33/20
摘要： Novel substituted spirobifluorene compounds useful as intermediates for materials in organic electronics devices
摘要翻译：新型取代的螺二芴化合物可用作有机电子器件材料的中间体

10. 发明申请

WO2004048353A1 PROCESS FOR THE MANUFACTURE OF 1,2-EPOXY-3-CHLOROPROPANE 审中-公开
标题翻译： 1,2-环氧-3-氯代壬烯的制备方法
公开(公告)号：WO2004048353A1
公开(公告)日：2004-06-10
申请号：PCT/EP2003/012506
申请日：2003-11-10
申请人： SOLVAY (SOCIÉTÉ ANONYME) , CATINAT, Jean-Pierre , STREBELLE, Michel
发明人： CATINAT, Jean-Pierre , STREBELLE, Michel
IPC分类号： C07D301/12
CPC分类号： C07D301/12
摘要： Process for the manufacture of 1,2-epoxy-3-chloropropane by reaction between allyl chloride and hydrogen peroxide in the presence of a catalyst and in the possible presence of at least one solvent in an epoxidation medium comprising at least one liquid phase, in which process the pH of the liquid phase is controlled and maintained at a value of greater than or equal to 1.5 and less than 4.8.
摘要翻译：在烯丙基氯和过氧化氢之间，在催化剂的存在下和在至少一种溶剂的存在下，在包含至少一个液相的环氧化介质中，通过在烯丙基氯和过氧化氢之间的反应制备1,2-环氧-3-氯丙烷的方法，其处理液相的pH被控制并保持在大于或等于1.5且小于4.8的值。

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