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1. 发明申请

WO2007093225A1 PROCESS FOR THE REMOVAL OF CONTAMINANTS 审中-公开
标题翻译：去除污染物的方法
公开(公告)号：WO2007093225A1
公开(公告)日：2007-08-23
申请号：PCT/EP2006/062484
申请日：2006-05-22
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , GOUMAN, Rudolf Robert , HEROLD, Rudolf Henri Max , LAST, Thijme , MANSHANDE, Bernardus Josephus Maria , SMIT, Cornelis Jacobus
发明人： GOUMAN, Rudolf Robert , HEROLD, Rudolf Henri Max , LAST, Thijme , MANSHANDE, Bernardus Josephus Maria , SMIT, Cornelis Jacobus
IPC分类号： B01D53/02 , B01D53/48 , B01D53/86 , C07C7/12 , C07C9/04 , C01B3/56
CPC分类号： C01B3/56 , B01D53/02 , B01D53/485 , B01D53/8606 , B01D2257/308 , C01B2203/042 , C01B2203/0485 , C01B2203/062 , C10K1/32
摘要： A process for the reduction of carbonyl sulfide (COS) in a gas stream is described. It comprises contacting the gas stream with an iron oxide-based material. The present invention relates to the removal of COS from any type of gas stream, in particular those which include one or more of the group comprising ethane, methane, hydrogen, carbon dioxide, hydrogen cyanide, ammonia, hydrogen sulfide, and noble gases. These include natural gas, and in particular syngas. Syngas is useable in a Fischer-Tropsch process. The present invention provides a simple but effective process for the reduction of COS, especially with a material that can easily be located in existing guard beds - avoiding any re-engineering time and costs. The iron oxide-based materials can also be useable against other impurities, providing a single bed solution.
摘要翻译：描述了一种在气流中还原羰基硫（COS）的方法。它包括使气流与氧化铁基材料接触。本发明涉及从任何类型的气流中除去COS，特别是包括乙烷，甲烷，氢气，二氧化碳，氰化氢，氨，硫化氢和惰性气体中的一种或多种的那些。这些包括天然气，特别是合成气。合成气可用于费 - 托法。本发明提供了一种简单但有效的减少COS的方法，特别是使用可以容易地位于现有保护床中的材料，避免了任何重新设计的时间和成本。氧化铁基材料也可用于抵抗其他杂质，提供单一床层溶液。

2. 发明申请

WO2007082896A1 PROCESS FOR REMOVING CARBONYL SULPHIDE AND HYDROGEN SULPHIDE FROM A SYNTHESIS GAS STREAM 审中-公开
标题翻译：从合成气流中除去硫化碳和硫化氢的方法
公开(公告)号：WO2007082896A1
公开(公告)日：2007-07-26
申请号：PCT/EP2007/050439
申请日：2007-01-17
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , HEROLD, Rudolf Henri Max , LAST, Thijme , MANSHANDE, Bernardus Josephus Maria , SMIT, Cornelis Jacobus
发明人： HEROLD, Rudolf Henri Max , LAST, Thijme , MANSHANDE, Bernardus Josephus Maria , SMIT, Cornelis Jacobus
IPC分类号： C01B3/56 , B01D53/04 , B01D53/48 , B01D53/14
CPC分类号： B01D53/04 , B01D53/14 , B01D2253/104 , B01D2253/112 , B01D2257/304 , B01D2257/308 , B01D2257/406 , B01D2257/408 , C01B3/56 , C01B2203/0415 , C01B2203/042 , C01B2203/0465 , C01B2203/0485 , C01B2203/062
摘要： The invention provides a process for removing COS and H 2 S from a feed synthesis gas stream comprising COS and H 2 S, the process comprising contacting the feed synthesis gas stream with solid adsorbent at a temperature in the range of from 100 to 240 °C to remove carbonyl sulphide and hydrogen sulphide, thereby obtaining a purified synthesis gas stream, wherein the solid adsorbent comprises one or more metals or oxides of the metals or combinations thereof and the metals are selected from the group of Ag, Sn, Mo, Fe and Zn.
摘要翻译：本发明提供了从包含COS和H 2 S的原料合成气流中除去COS和H 2 S的方法，该方法包括使原料合成气流与固体吸附剂在100至240℃的温度范围内以除去羰基硫化物和硫化氢，从而获得纯化的合成气流，其中固体吸附剂包括一种或多种金属或金属的氧化物或其组合，以及金属选自Ag，Sn，Mo，Fe和Zn。

3. 发明申请

WO2008155305A1 PROCESS FOR REMOVAL OF HYDROGEN CYANIDE AND AMMONIA FROM SYNTHESIS GAS 审中-公开
标题翻译：从合成气中去除氢氰化物和氨的方法
公开(公告)号：WO2008155305A1
公开(公告)日：2008-12-24
申请号：PCT/EP2008/057527
申请日：2008-06-16
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , HEROLD, Rudolf Henri Max , LAST, Thijme , SMIT, Cornelis Jacobus
发明人： HEROLD, Rudolf Henri Max , LAST, Thijme , SMIT, Cornelis Jacobus
IPC分类号： C01B3/56 , C01B3/58
CPC分类号： C01B3/58 , C01B3/56 , C01B2203/042 , C01B2203/0435 , C01B2203/0465 , C01B2203/048 , C01B2203/0485
摘要： The invention provides a process for removal of HCN and NH 3 from synthesis gas, the process comprising the steps of: (a) contacting feed synthesis gas comprising HCN with a HCN hydrolysis sorbent in the presence of water, thereby obtaining synthesis gas comprising NH 3 ; (b) contacting the synthesis gas comprising NH 3 with an acidic cation exchange resin in the presence of water to remove NH 3 , thereby obtaining purified synthesis gas.
摘要翻译：本发明提供从合成气中除去HCN和NH 3的方法，该方法包括以下步骤：（a）在水存在下使包含HCN的进料合成气与HCN水解吸附剂接触，从而获得包含NH 3的合成气; （b）在水存在下使包含NH 3的合成气与酸性阳离子交换树脂接触以除去NH 3，从而获得纯化的合成气。

4. 发明申请

WO2006008317A1 PROCESS FOR THE REMOVAL OF COS FROM A SYNTHESIS GAS STREAM COMPRISING H2S AND COS 审中-公开
标题翻译：从包含H2S和COS的合成气流中去除COS的方法
公开(公告)号：WO2006008317A1
公开(公告)日：2006-01-26
申请号：PCT/EP2005/053563
申请日：2005-07-22
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , GOUMAN, Rudolf Robert , VAN HARDEVELD, Robert Martijn , HEROLD, Rudolf Henri , KODDE, Adriaan Johannes , LAST, Thijme , SMIT, Cornelis Jacobus
发明人： VAN HARDEVELD, Robert Martijn , HEROLD, Rudolf Henri , KODDE, Adriaan Johannes , LAST, Thijme , SMIT, Cornelis Jacobus
IPC分类号： B01D53/86
CPC分类号： B01D53/8606 , B01D53/04 , B01D2253/112 , B01D2255/20707 , B01D2255/30 , B01D2256/00 , B01D2257/306 , C01B3/54 , C01B3/56 , C01B2203/042 , C01B2203/0435 , C01B2203/0485
摘要： The invention provides a process for the removal of COS from a first synthesis gas stream comprising COS and H 2 S, the process having the steps of: (a) converting COS in the first synthesis gas stream to H 2 S by contacting the first synthesis gas stream with a COS-hydrolysing catalyst in the presence of water in a hydrolysis zone to obtain a second synthesis gas stream depleted of COS and enriched in H 2 S; (b) removing H 2 S from the second synthesis gas stream by contacting the second synthesis gas stream with a solid adsorbent in a H 2 S removal zone to obtain a third synthesis gas stream depleted of H 2 S and depleted of COS
摘要翻译：本发明提供了从包含COS和H 2 S的第一合成气流中除去COS的方法，该方法具有以下步骤：（a）将第一合成气流中的COS转化为H 通过在水解区中在水的存在下使第一合成气流与COS-水解催化剂接触以获得消耗COS并富集H 2的第二合成气流， / SUB> S; （b）通过使第二合成气流与H 2 S 2去除区中的固体吸附剂接触，从第二合成气流中除去H 2 S，得到第三合成物耗尽H 2 S且耗尽COS的气流

5. 发明申请

WO2005090269A2 PROCESS FOR TREATING A LOADED SOLVENT STREAM HAVING A TIME-VARYING CONCENTRATION OF CONTAMINANT 审中-公开
标题翻译：处理污染物时变浓度的负载溶剂流的方法
公开(公告)号：WO2005090269A2
公开(公告)日：2005-09-29
申请号：PCT/EP2005/051187
申请日：2005-03-16
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL CANADA LIMITED , CARLSSON, Anders , VAN HEERINGEN, Gijsbert Jan , LAST, Thijme
发明人： CARLSSON, Anders , VAN HEERINGEN, Gijsbert Jan , LAST, Thijme
IPC分类号： C07C7/00
CPC分类号： B01D53/1425 , B01D53/1412
摘要： The invention provides a process for treating a loaded solvent stream having a time-varying contaminant concentration, the process comprising the steps of: (a) providing a plurality of hold-up tanks; (b) feeding the loaded solvent s - ream in dependence on its contaminant concentration to one or more of the hold-up tanks and; (c) allowing lowed solvent to flow from the plurality of hold-up tanks to obtain a smoothed loaded solvent stream having a reduced time-varying contaminant concentration. The inventio further provides a treating unit comprising a circuit for circulating a solvent stream, which circuit includes a device for smoothing contaminant peak concentrations, said device comprising a plurality of hold-up tanks each hold-up tank having at least one inlet and an outlet equipped with an outlet valve, the device further comprising an inlet distributor allowing the control of solvent flow to one or more of the hold-up tanks.
摘要翻译：本发明提供了一种用于处理具有时变污染物浓度的负载溶剂流的方法，该方法包括以下步骤：（a）提供多个保持罐; （b）根据其对一个或多个保持箱的污染物浓度将装载的溶剂送入; （c）允许低浓度的溶剂从多个保持槽流出，以获得具有降低的时变污染物浓度的平滑的负载溶剂流。本发明还提供了一种处理单元，其包括用于使溶剂流循环的回路，该回路包括用于平滑污染物峰值浓度的装置，所述装置包括多个滞留槽，每个滞留槽具有至少一个入口和出口配备有出口阀，该装置还包括允许控制溶剂流到一个或多个保持箱的入口分配器。

6. 发明申请

WO2007009943A1 PROCESS FOR PRODUCING A GAS STREAM DEPLETED OF HYDROGEN SULPHIDE AND OF MERCAPTANS 审中-公开
标题翻译：用于生产硫化氢和三聚氰胺的气体流的方法
公开(公告)号：WO2007009943A1
公开(公告)日：2007-01-25
申请号：PCT/EP2006/064241
申请日：2006-07-13
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL CANADA LIMITED , LAST, Thijme , CARLSSON, Anders
发明人： LAST, Thijme , CARLSSON, Anders
IPC分类号： B01D53/52 , B01D53/14
CPC分类号： B01D53/1487 , B01D53/52 , B01D53/77 , B01D2257/304 , B01D2257/306
摘要： The invention provides a process for producing a gas stream depleted of H 2 S and of RSH from a feed gas stream comprising H 2 S and RSH, the process comprising the steps of : (a) contacting the feed gas stream with absorbing liquid in a H 2 S removal zone to obtain a gas stream depleted of H 2 S; (b) contacting the gas stream obtained in step (a) with aqueous scrubbing solution comprising CUSO 4 in a RSH removal zone to obtain a mixture comprising Cu-alkylsulphide products and the gas stream depleted of H 2 S and depleted of RSH.
摘要翻译：本发明提供了一种从包含H 2 S和RSH的进料气流生产缺乏H 2 S和RSH的气流的方法，该方法包括以下步骤：：（a）使进料气流与H 2 S 2 S去除区中的吸收液体接触以获得消耗H 2 S的气流; （b）将在步骤（a）中获得的气流与RSH去除区中含有CUSO 4的含水洗涤溶液接触，得到包含Cu-烷基硫化物产物和H _{2 S并耗尽RSH。}

7. 发明申请

WO2007003618A1 PROCESS FOR PRODUCING A GAS STREAM DEPLETED OF MERCAPTANS 审中-公开
标题翻译：生产墨西哥湾流域的过程
公开(公告)号：WO2007003618A1
公开(公告)日：2007-01-11
申请号：PCT/EP2006/063786
申请日：2006-07-03
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL CANADA LIMITED , CARLSSON, Anders , LAST, Thijme , RAJANI, Jayantilal Bhagvanji
发明人： CARLSSON, Anders , LAST, Thijme , RAJANI, Jayantilal Bhagvanji
IPC分类号： B01D53/04 , B01D53/14
CPC分类号： B01D53/04 , B01D53/1487 , B01D53/1493 , B01D2253/108 , B01D2253/308 , B01D2257/306 , B01D2257/7027
摘要： The invention provides a process for producing a gas stream depleted of RSH from a feed gas stream comprising natural gas, RSH and aromatic compounds selected from the group of benzene, toluene, o-xylene, m-xylene and p-xylene, the process comprising the steps of: (a) contacting the feed gas stream with absorbing liquid comprising a physical solvent in an aromatic compound removal zone to obtain loaded absorbing liquid comprising aromatic compounds selected from the group of benzene, toluene, o-xylene, m-xylene and p-xylene and a gas stream depleted of these aromatic compounds; (b) contacting the gas stream obtained in step (a) with solid adsorbent in a mercaptan removal zone to obtain solid adsorbent loaded with RSH and the gas stream depleted of RSH.
摘要翻译：本发明提供了一种从包含天然气，RSH和选自苯，甲苯，邻二甲苯，间二甲苯和对二甲苯的芳族化合物的进料气流中生产缺乏RSH的气流的方法，该方法包括步骤：（a）将进料气流与包含物理溶剂的吸收液体接触在芳族化合物去除区中以获得负载的吸收液体，其包含选自苯，甲苯，邻二甲苯，间二甲苯和对二甲苯和贫的这些芳族化合物的气流; （b）将步骤（a）中获得的气流与硫醇去除区中的固体吸附剂接触，以获得负载有RSH的固体吸附剂和贫化的RSH的气流。

8. 发明申请

WO2004039926A1 REMOVAL OF SULPHUR COMPOUNDS FROM HYDROCARBON STREAMS USING ADSORBENTS AND REGENERATION OF THE LOADED ADSORBENTS 审中-公开
标题翻译：使用吸附剂和加载的吸附剂的再生来从碳氢化合物流中除去硫化合物
公开(公告)号：WO2004039926A1
公开(公告)日：2004-05-13
申请号：PCT/EP2003/050765
申请日：2003-10-29
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , VAN DE GRAAF, Jolinde, Machteld , LAST, Thijme
发明人： VAN DE GRAAF, Jolinde, Machteld , LAST, Thijme
IPC分类号： C10L3/06
CPC分类号： C10L3/102 , B01D53/04 , B01D2253/108 , B01D2253/308 , B01D2256/24 , B01D2257/30 , B01D2257/304 , B01D2257/306 , B01D2258/06 , B01D2259/40086 , C10G25/12 , C10L3/10 , Y02C10/08
摘要： The invention concerns a process for the removal of sulphur compounds from a hydrocarbon stream, especially a gaseous hydrocarbon gas stream, comprising said sulphur compounds, which process comprises contacting said gas stream with an adsorbent comprising a zeolite having a pore diameter of at least 5 Å to adsorb the sulphur compounds thereon, the adsorption process followed by a regeneration process of used, loaded adsorbent by contacting the said loaded adsorbent with a regeneration gas stream having a relative water humidity less than 100 %, especially less than 80 %. Suitably the regeneration is followed by a dry regeneration treatment. The invention further relates to a process for the regeneration of adsorbent comprising a zeolite having a pore diameter of at least 5 Å loaded with sulphur compounds by contacting the adsorbent with a regeneration gas stream having a relative water humidity less than 100 %, especially less than 80 %. Suitably the regeneration is followed by a dry regeneration treatment.
摘要翻译：本发明涉及从包含所述硫化合物的烃流，特别是气态烃气流中除去硫化合物的方法，该方法包括使所述气流与包含孔径至少为5埃的沸石的吸附剂接触在其上吸附硫化合物，吸附过程接着是使用的负载吸附剂的再生过程，其通过使所加载的吸附剂与相对水分湿度小于100％，特别是小于80％的再生气流接触。适当地，再生之后是干再生处理。本发明还涉及一种用于再生吸附剂的方法，该方法包括通过使吸附剂与相对湿度小于100％，特别是小于100％的再生气流接触，使孔径至少为5埃的沸石， 80％。适当地，再生之后是干再生处理。

9. 发明申请

WO2015004130A1 PROCESS FOR REMOVING ACIDIC CONTAMINANTS FROM A GAS STREAM 审中-公开
标题翻译：从气体流中除去酸性污染物的方法
公开(公告)号：WO2015004130A1
公开(公告)日：2015-01-15
申请号：PCT/EP2014/064598
申请日：2014-07-08
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： LAST, Thijme , SCHNEIDER, Armin , WIJNTJE, Renze
IPC分类号： B01D53/14 , B01D53/18 , C10L3/10
CPC分类号： B01D53/1456 , B01D53/1425 , B01D53/18 , B01D2252/204 , B01D2252/602 , B01D2256/24 , B01D2257/304 , B01D2257/306 , B01D2257/308 , B01D2257/504 , B01D2258/0283 , B01D2258/06 , C10L3/102 , C10L2290/06 , C10L2290/12 , C10L2290/541
摘要： The invention provides a process for removing acidic contaminants from a gas stream wherein: a) the gas stream is contacted (1) with an aqueous absorbent solution to obtain an acidic contaminants-enriched aqueous absorbent solution (5) and an acidic contaminants-depleted gas stream (4); b) the acidic contaminants-enriched absorbent solution is allowed to form a multi-phase mixture which comprises an acidic contaminants-enriched gaseous phase, an acidic contaminants-depleted liquid phase and an acidic contaminants-enriched liquid phase; c) the multi-phase mixture is subjected to a regeneration treatment (12) to obtain an acidic contaminants-enriched gas stream, an acidic contaminants-depleted liquid phase and an acidic contaminants-enriched liquid phase; d) the acidic contaminants-enriched gas stream is cooled (15) to obtain a cooled mixture comprising an acidic contaminants-enriched gaseous phase and a condensate liquid phase; e) the cooled mixture is separated into an acidic contaminants-enriched gaseous phase (28) and a condensate liquid phase (29); f) the condensate liquid phase is withdrawn; g) a part (30) of the condensate liquid phase is recycled to step (c); and h) a part (31) of the condensate liquid phase is used in step (e).
摘要翻译：本发明提供了一种从气流中除去酸性污染物的方法，其中：a）使气流与水性吸收剂溶液接触（1），以获得酸性污染物富集的吸收水溶液（5）和酸性污染物贫化气体流（4）; b）允许酸性污染物富集的吸收剂溶液形成多相混合物，其包含酸性污染物富集的气相，酸性污染物贫乏的液相和酸性污染物富集的液相; c）将多相混合物进行再生处理（12）以获得酸性污染物富集气流，酸性污染物贫乏液相和酸性污染物富集液相; d）将富含酸性污染物的气流冷却（15）以获得包含富含酸性污染物的气相和冷凝液体相的冷却混合物; e）将冷却的混合物分离成富含酸性污染物的气相（28）和冷凝液体相（29）; f）冷凝液体相被取出; g）将冷凝物液相的一部分（30）再循环至步骤（c）; 和h）在步骤（e）中使用冷凝物液相的一部分（31）。

10. 发明申请

WO2014095812A1 METHOD FOR REMOVING A CONTAMINANT FROM A CONTAMINATED STREAM 审中-公开
标题翻译：从污染物流中除去污染物的方法
公开(公告)号：WO2014095812A1
公开(公告)日：2014-06-26
申请号：PCT/EP2013/076836
申请日：2013-12-17
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： LAST, Thijme , MADERA, Martin , HANAMANT RAO, Patil Prashant , SCHNEIDER, Tanja , WIJNTJE, Renze
IPC分类号： B01D53/14 , B01D53/78 , B01D53/96
CPC分类号： B01D53/1425 , B01D19/0015 , B01D53/1462 , B01D53/1493 , B01D2256/245 , B01D2257/304 , B01D2257/504
摘要： The present invention provides a method of removing a contaminant, e.g. CO 2 and/or H 2 S, from a contaminated stream (10). The contaminated stream (10) is contacted in an absorber (2) with an absorbent solution (80), thereby obtaining a contaminant-depleted stream (20) and a contaminant-enriched absorbent stream (30). The contaminant-enriched absorbent stream (30) is separated in a regenerator (3), thereby obtaining a contaminant- depleted absorbent stream (60) at a bottom of the regenerator (3), and a contaminant-enriched stream (50). The contaminant-depleted absorbent stream (60) forms a lower layer of a first liquid phase (A) and a higher layer of a second liquid phase (B). The first liquid phase (A) and the second liquid phase (B) are removed simultaneously at the interface (X) of these liquid phases. The contaminant-depleted absorbent stream (60) is reused.
摘要翻译：本发明提供了一种去除污染物的方法，例如， CO 2和/或H 2 S，来自受污染的流（10）。受污染的流（10）在吸收器（2）中与吸收剂溶液（80）接触，从而获得污染物流（20）和富含污染物的吸收剂流（30）。富含污染物的吸收剂流（30）在再生器（3）中分离，从而在再生器（3）的底部获得污染物贫乏的吸收剂流（60）和富含污染物质的物流（50）。污染物贫乏的吸收剂流（60）形成第一液相（A）的下层和第二液相（B）的较高层。在这些液相的界面（X）处同时除去第一液相（A）和第二液相（B）。污染物贫乏的吸收剂流（60）被再利用。

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