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1. 发明申请

WO2015160935A1 METHODS OF MANUFACTURE OF BIS(PHTHALIMIDE)S 审中-公开
标题翻译： BIS（PHTHALIMIDE）S制造方法
公开(公告)号：WO2015160935A1
公开(公告)日：2015-10-22
申请号：PCT/US2015/025950
申请日：2015-04-15
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , CHAULAGAIN, Mani Raj
发明人： CHAULAGAIN, Mani Raj , GUGGENHEIM, Thomas Link , ODLE, Roy Ray
IPC分类号： C08G73/10
CPC分类号： C07D209/48 , C08G73/1021 , C08G73/1032 , C08G73/1046 , C08G73/1064
摘要： A method of manufacture of a bis(phthalimide) composition includes reacting, in the presence of molten diphenyl sulfone, sulfolane, or a combination comprising at least one of the foregoing, a substituted phthalic anhydride with an organic diamine. The product mixture can be directly employed in the preparation of polyetherimides and other polyether polymers.
摘要翻译：制备双（邻苯二甲酰亚胺）组合物的方法包括在熔融二苯砜存在下，环丁砜或包含至少一种上述物质的组合物，取代的邻苯二甲酸酐与有机二胺反应。产物混合物可直接用于制备聚醚酰亚胺和其他聚醚聚合物。

2. 发明申请

WO2015160933A1 METHODS OF MANUFACTURE OF POLYETHERIMIDES 审中-公开
标题翻译：聚乙二醇的制备方法
公开(公告)号：WO2015160933A1
公开(公告)日：2015-10-22
申请号：PCT/US2015/025948
申请日：2015-04-15
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , CHAULAGAIN, Mani Raj
发明人： CHAULAGAIN, Mani Raj , GUGGENHEIM, Thomas Link , ODLE, Roy Ray
IPC分类号： C08G73/10
CPC分类号： C08G73/1032 , C08G73/1021 , C08G73/1046 , C08G73/1064
摘要： A method of manufacture of a polyetherimide composition includes contacting a substituted phthalic anhydride and an organic diamine in the presence of diphenyl sulfone, sulfolane, or a combination comprising at least one of the foregoing solvents at a temperature of greater than 130°C to provide a bis(phthalimide) composition comprising diphenyl sulfone, sulfolane, or a combination comprising at least one of the foregoing solvents and a bis(phthalimide); and polymerizing the bis(phthalimide) and an alkali metal salt of a dihydroxy aromatic compound in the presence of diphenyl sulfone, sulfolane, or a combination comprising at least one of the foregoing to form a polyetherimide. The method does not require any catalyst either for the imidization or the polymerization.
摘要翻译：一种制备聚醚酰亚胺组合物的方法包括在二苯基砜，环丁砜或包含至少一种上述溶剂的组合的存在下，在大于130℃的温度下使取代的邻苯二甲酸酐和有机二胺接触，以提供包含二苯基砜，环丁砜或包含至少一种上述溶剂和双（邻苯二甲酰亚胺））的组合物的双（邻苯二甲酰亚胺）组合物。在二苯基砜，环丁砜或包含至少一种前述物质的组合的存在下，使双（邻苯二甲酰亚胺）和二羟基芳族化合物的碱金属盐聚合形成聚醚酰亚胺。该方法不需要用于酰亚胺化或聚合的任何催化剂。

3. 发明申请

WO2018126110A1 METHOD OF MAKING A POLYETHERIMIDE AND POLYETHERIMIDE PRODUCED THEREBY 审中-公开
公开(公告)号：WO2018126110A1
公开(公告)日：2018-07-05
申请号：PCT/US2017/068895
申请日：2017-12-29
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , CHAULAGAIN, Mani Raj
发明人： CHAULAGAIN, Mani Raj , ODLE, Roy Ray , GUGGENHEIM, Thomas Link
IPC分类号： C08G73/10 , C08G65/40 , C08J5/00
摘要： A one-pot method for making a polyetherimide includes contacting in a reaction vessel a reactive substituted phthalic anhydride and an organic diamine in a polar aprotic solvent to provide a reaction mixture including a substituted bisphthalimide. The method further includes adding to the reaction mixture in the same reaction vessel an aromatic dihydroxy compound, a base, and optionally, a phase transfer catalyst to provide a product mixture including the polyetherimide. A polyetherimide made by the method is also described.

4. 发明申请

WO2020028460A1 COPOLYCARBONATE COMPOSITIONS AND ARTICLES 审中-公开
公开(公告)号：WO2020028460A1
公开(公告)日：2020-02-06
申请号：PCT/US2019/044277
申请日：2019-07-31
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , ZHAO, Wei
发明人： ZHAO, Wei , ODLE, Roy Ray , SYBERT, Paul Dean
IPC分类号： C08K3/32 , C08K5/42 , C08K5/524
摘要： Provided are copolycarbonate compositions including a stabilizer package which comprise a phosphorus-containing acid, an ester of phosphorus-containing acid, and an organosulfonic stabilizer where the phosphorus-containing acid and the ester of a phosphorus-containing acid are present in a molar ratio of 1 to 2. The total stabilization package is for example, in the amount by weight of 4 to 32 ppm, 8 to 24 ppm, or 8 to 16 ppm and the organosulfonic stabilizer is, e.g., of 2 to 30 ppm, or 4 to 24 ppm, or 8 to 16 ppm.

5. 发明申请

WO2018126154A1 LINEAR AND BRANCHED POLYIMIDE COMPOSITION 审中-公开
公开(公告)号：WO2018126154A1
公开(公告)日：2018-07-05
申请号：PCT/US2017/068984
申请日：2017-12-29
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , ODLE, Roy Ray
发明人： ODLE, Roy Ray , JOHNSON, Peter , CHELLAMUTHU, Manojkumar , KONG, Hee Won , LONG, Timothy Edward
IPC分类号： C08G73/10 , C08L79/08
摘要： A polyimide composition includes 1 to 99 weight percent, preferably 70 to 99 weight percent, more preferably 75 to 95 weight percent of a first polyimide; and 1 to 99 weight percent, preferably 1 to 30 weight percent, more preferably 2 to 25 weight percent of a second polyimide, wherein the first polyimide and the second polyimide are different, and wherein the polyimide composition has a melt flow rate that is greater than a melt flow rate of the first polyimide and less than a melt flow rate of the second polyimide; an apparent viscosity that is less than an apparent viscosity of the first polyimide and less than an apparent viscosity of the second polyimide; and a notched Izod impact strength that is greater than a notched Izod impact strength of the first polyimide and greater than a notched Izod impact strength of the second polyimide.

6. 发明申请

WO2018126141A1 BRANCHED POLYIMIDE COMPOSITIONS, METHOD OF MANUFACTURE, AND USES THEREOF 审中-公开
公开(公告)号：WO2018126141A1
公开(公告)日：2018-07-05
申请号：PCT/US2017/068966
申请日：2017-12-29
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , ODLE, Roy Ray
发明人： ODLE, Roy Ray , GUGGENHEIM, Thomas Link , KLOPPENBURG, Lioba Maria , LONG, Timothy Edward , DENNIS, Joseph Michael
IPC分类号： C08G73/10
摘要： A branched polyimide of the formula (I) wherein G is a group having a valence of t present in an amount 0.01 to 20 mol%, each Q is independently the same or different, and is a divalent C 1-60 hydrocarbon group, each M is independently the same or different, and is -O-, -C(O)-, -OC(O)-, -OC(O)O-, -NHC(O), -(O)CNH-, -S-, -S(O)-, or -S(O) 2 -, D is a phenylene, each V is independently the same or different, and is a tetravalent C 4-40 hydrocarbon group, each R is independently the same or different, and is a C 1-20 divalent hydrocarbon group, q is 0 or 1, m is 0 or 1, d is 0 or 1, p is 1 or 2, t is 2 to 6, and each n is independently the same or different, and is 1 to 1,000, provided that the total of all values of n is greater than 4.

7. 发明申请

WO2018126162A1 COMPOSITIONS AND ARTICLES MADE FROM BRANCHED POLYETHERIMIDES 审中-公开
公开(公告)号：WO2018126162A1
公开(公告)日：2018-07-05
申请号：PCT/US2017/068998
申请日：2017-12-29
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , ODLE, Roy Ray
发明人： ODLE, Roy Ray , JOHNSON, Peter , CHELLAMUTHU, Manojkumar , KONG, Hee Won
IPC分类号： C08G73/10
摘要： A branched polyimide of the formula (I) wherein G is a group having a valence of t, present in an amount of 0.01 to 10 mol%, or 0.05 to 5 mol%, or 0.1 to 4 mol%, or 0.1 to 3 mol%, each of Q, M, D, V, and R are as defined herein, q is 0 or 1, m is 0 or 1, d is 0 or 1, p is 1 or 2, t is 2 to 6, preferably 2 to 4, and each n is independently the same or different, and is 1 to 1,000, provided that the total of all values of n is greater than 4, wherein the branched polyimide has a zero-shear viscosity in a range from 500 to 15,000 Pa•s, a rheology ratio of 1.1 to 5, and a strain hardening ratio of 1 to 6.

8. 发明申请

WO2018126146A1 POLYIMIDE OLIGOMERS, COMPOSITIONS, METHOD OF MANUFACTURE, AND USES THEREOF 审中-公开
公开(公告)号：WO2018126146A1
公开(公告)日：2018-07-05
申请号：PCT/US2017/068974
申请日：2017-12-29
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , ODLE, Roy Ray
发明人： ODLE, Roy Ray , CAO, Ke , LIU, Guoliang , LONG, Timothy Edward , DENNIS, Joseph Michael
IPC分类号： C08G73/10
摘要： A polyimide oligomer has the formula (I) wherein G is a group having a valence of t, each Q, M, D, and V are as defined herein, each R is independently the same or different, and is a C 1-20 divalent hydrocarbon, a C 1-20 alkylene-X, or a C 6-30 arylene-X wherein -X is -O-M, -C(O)O-M, -OC(O)O-M, -S-M, -S(O) 2 -M, -S(O) 3 -M, -OS(O) 3 -M, or -OP(O) 3 -M, and wherein M is a cation, preferably Na, K, Cs, Mg, Ca, Ti, Zr, Cr, Bi, Mn, Fe, Co, Ni, Cu, Zn, Cd, Ge, B, Al, Ga, In, Sn, Pb, As, Sb, ammonium, phosphonium, imidazolium, guanidinium, or pyridinium, q is 0 or 1, m is 0 or 1, d is 0 or 1, p is 1 or 2, t is 1 to 6, and each n is independently the same or different, and is 1 to 1,000, provided that the total of all values of n is greater than 4.

9. 发明申请

WO2018094028A1 TELECHELIC POLY(IMIDE) OLIGOMERS, METHODS OF MANUFACTURE, AND USES THEREOF 审中-公开
公开(公告)号：WO2018094028A1
公开(公告)日：2018-05-24
申请号：PCT/US2017/061986
申请日：2017-11-16
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , ODLE, Roy Ray
发明人： ODLE, Roy Ray , LIU, Guoliang , CAO, Ke , LONG, Timothy Edward , DENNIS, Joseph Michael
IPC分类号： C08G73/10 , C07D239/48
摘要： A ureido-pyrimidinone oligomer having the formula (I) wherein each Z' is independently the same or different, and is a substituted or unsubstituted straight or branched chain C 1-10 alkyl, each R 1 is independently the same or different, and is a substituted or unsubstituted straight or branched chain C 1-20 alkylene, substituted or unsubstituted C 2-20 alkenylene, substituted or unsubstituted C 3-8 cycloalkylene, or substituted or unsubstituted C 6-18 arylene, each V is independently the same or different, and is a substituted or unsubstituted tetravalent C 4-40 hydrocarbon group, each R is independently the same or different, and is a substituted or unsubstituted C 1-24 divalent hydrocarbon group; and n has an average value of 2 to 50, preferably 3 to 40, more preferably 5 to 30.

10. 发明申请

WO2017117449A1 METHODS FOR THE MANUFACTURE OF AN AROMATIC BISIMIDE AND A POLYETHERIMIDE 审中-公开
标题翻译：制备芳香族双苯亚酰胺和聚醚酰亚胺的方法
公开(公告)号：WO2017117449A1
公开(公告)日：2017-07-06
申请号：PCT/US2016/069309
申请日：2016-12-29
申请人： SABIC GLOBAL TECHNOLOGIES B.V. , GUGGENHEIM, Thomas Link
发明人： GUGGENHEIM, Thomas Link , ODLE, Roy Ray , CHAULAGAIN, Mani Raj
IPC分类号： C07D403/12 , C07D209/34
CPC分类号： C07D209/34 , C07D403/12
摘要： A method for producing an aromatic bisimide includes reacting a dialkali metal salt of a dihydroxy aromatic compound with an N-alkyl nitrophthalimide to form a product mixture including the aromatic bisimide. The N-alkyl nitrophthalimide includes 4-nitro-N-(C 1-13 alkyl)phthalimide, 3-nitro-N-(C 1-13 alkyl)phthalimide, or a combination including at least one of the foregoing, and 4-hydroxy-3,5-dinitro-N-(C 1-13 alkyl)phthalimide in an amount of 1-10000 ppm. The aromatic bisimide can be obtained in a yield of greater than 75%, or 90-99.8%. A method for the manufacture of a polyetherimide, a polyetherimide, and an article including the polyetherimide are also disclosed. A mixed acid nitration process for the preparation of an N-alkyl nitrophthalimide is also described.
摘要翻译：生产芳族双酰亚胺的方法包括使二羟基芳族化合物的二碱金属盐与N-烷基硝基邻苯二甲酰亚胺反应以形成包含芳族双酰亚胺的产物混合物。 N-烷基硝基邻苯二甲酰亚胺包括4-硝基-N-（C 1〜13烷基）邻苯二甲酰亚胺，3-硝基-N-（C 1〜13烷基）邻苯二甲酰亚胺，或包含至少一种前述物质的组合和1-1,000ppm量的4-羟基-3,5-二硝基-N-（C 1-13烷基）邻苯二甲酰亚胺。芳族双酰亚胺可以以大于75％或90-99.8％的收率获得。还公开了制造聚醚酰亚胺，聚醚酰亚胺和包含聚醚酰亚胺的制品的方法。还描述了用于制备N-烷基硝基邻苯二甲酰亚胺的混合酸硝化方法。

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