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    • 2. 发明申请
    • METHOD AND ARRANGEMENT FOR SEPARATING TWO SOLUTIONS MIXED IN DISPERSION INTO TWO SOLUTION PHASES IN A LIQUID-LIQUID EXTRACTION SEPARATION CELL
    • 用于分离混合在液体萃取分离单元中的两种溶液相中的两种溶液的方法和装置
    • WO2010089462A1
    • 2010-08-12
    • PCT/FI2010/050081
    • 2010-02-08
    • OUTOTEC OYJNYMAN, BrorEKMAN, EeroPEKKALA, PerttiLAITALA, HannuSAARIO, Rami
    • NYMAN, BrorEKMAN, EeroPEKKALA, PerttiLAITALA, HannuSAARIO, Rami
    • B01D11/04C22B3/02
    • B01D11/0453B01D11/0449B01D17/0211B01D17/0214B01D2011/005C22B3/0005C22B3/005C22B3/02Y02P10/234
    • The invention relates to a method and arrangement for separating two solutions mixed in dispersion into two solution phases in a liquid-liquid extraction separation cell (1). The arrangement includes a first guide wall (4), which is arranged at a distance from that end wall (15) of the cell (1) that is located on the side of the feed end (2), in order to extend along the whole width of the cell with respect to the vertical direction at an inclined angle (α). The first guide wall includes a bottom edge (5), which is located at a distance (H 1 ...H 2 ) from the cell bottom, so that in between the bottom edge (5) and the cell bottom (3), there is left a clearance gap (6) widening from the center towards the cell sides. The second guide wall (7) is essentially parallel with the first guide wall (4) and placed at a distance (L1) therefrom, so that in between the first guide wall (4) and the second guide wall (7), there is formed an uptake shaft (8) extending diagonally upwards at an inclined angle (α). The second guide wall (7) includes a bottom edge (13), which is pressed tightly against the cell bottom (3), a number vertical slots (9), which are arranged as a horizontal line (10) of vertical slots, said line extending along the width of the second guide wall at a distance from the bottom edge (13), and a slanting plate (11), which is attached to the second guide wall (7), in the vicinity of the top part of the line (10)of vertical slots.
    • 本发明涉及将分散液中混合的两种溶液分离成液 - 液萃取分离池(1)中的两个溶液相的方法和装置。 该装置包括第一引导壁(4),该第一引导壁(4)布置在位于馈电端(2)一侧的电池(1)的端壁(15)的一定距离处,以便沿着 电池相对于垂直方向的整个宽度为倾斜角(a)。 第一引导壁包括底部边缘(5),其位于与单元底部相距一定距离(H1 ... H2)处,使得在底部边缘(5)和单元底部(3)之间存在 留下间隙(6)从中心向细胞侧扩宽。 第二引导壁(7)基本上与第一引导壁(4)平行并且与其间距离(L1)放置,使得在第一引导壁(4)和第二引导壁(7)之间存在 形成以倾斜角(a)斜向上延伸的吸收轴(8)。 所述第二引导壁(7)包括被紧紧压靠在所述电池单元底部(3)上的底部边缘(13),垂直槽(9)布置成垂直槽的水平线(10),所述垂直槽 沿着第二引导壁的宽度与底部边缘(13)一定距离延伸的线,以及在第二引导壁(7)的顶部附近附接的倾斜板(11) (10)垂直槽。
    • 3. 发明申请
    • METHOD AND ARRANGEMENT FOR SEPARATING TWO SOLUTIONS MIXED IN DISPERSION INTO TWO SOLUTION PHASES IN A LIQUID-LIQUID EXTRACTION SEPARATION CELL
    • 用于分离混合在液体萃取分离单元中的两种溶液相中的两种溶液的方法和装置
    • WO2010089456A1
    • 2010-08-12
    • PCT/FI2010/050070
    • 2010-02-05
    • OUTOTEC OYJNYMAN, BrorEKMAN, EeroPEKKALA, PerttiLAITALA, HannuSAARIO, Rami
    • NYMAN, BrorEKMAN, EeroPEKKALA, PerttiLAITALA, HannuSAARIO, Rami
    • B01D11/04C22B3/02
    • B01D11/0453B01D17/0211B01D17/0214C22B3/0005C22B3/02Y02P10/234
    • The invention relates to a method and arrangement for separating two solutions mixed in dispersion into two solution phases in a liquid-liquid extraction separation cell (1). The shut-off element (3, 4, 5) comprises a front panel (8) that extends along the whole width of the cell. The front panel (8) includes a bottom edge (9), which is arranged at a distance (H1 H2 H3) from the cell bottom (7), so that the front panel (8) allows an unobstructed flow of the heavier solution phase directly forwards underneath the bottom edge (9). In the vertical direction, the front panel extends to such a height that it forces the lighter solution phase placed on the heavier solution phase to flow as a thin overflow layer over the top edge (12) of the front panel (8) and forces the dispersion to thicken in front of the front panel. The rear panel (15) is essentially parallel with the front panel (8) and placed at a distance (S) therefrom, so that in between the front panel and the rear panel, there is formed an uptake shaft (14) extending essentially vertically upwards, along which uptake shaft the thickened dispersion can rise upwardly and be compressed. At least one slanting plate (16) is in the direction of the flow placed at an inclined angle (δ), inclined upwardly with respect to the horizontal plane. The slanting plate attenuates and slows down the vertical component of the rising compressed dispersion flow and guides the dispersion essentially in the lengthwise direction of the cell as a dispersion flow to the successive separator part.
    • 本发明涉及将分散液中混合的两种溶液分离成液 - 液萃取分离池(1)中的两个溶液相的方法和装置。 截止元件(3,4,5)包括沿着电池的整个宽度延伸的前面板(8)。 前面板(8)包括与细胞底部(7)相距一定距离(H1 H2 H3)设置的底边缘(9),使得前面板(8)允许较重溶液相的通畅流动 直接在底边(9)的下方。 在垂直方向上,前面板延伸到这样一个高度,使其强制放置在较重的溶液相上的较轻的溶液相作为薄的溢流层流过前面板(8)的顶部边缘(12),并迫使 分散在前面板前面加厚。 后面板(15)基本上与前面板(8)平行并且与其间距离(S)放置,使得在前面板和后面板之间形成有基本垂直延伸的上升轴(14) 向上,上升轴,增稠的分散体可以向上升起并被压缩。 至少一个倾斜板(16)沿着相对于水平面向上倾斜的倾斜角(d)的流动方向。 倾斜板使上升的压缩分散体流的垂直分量衰减并减慢,并且使分散体基本上沿着细胞的长度方向作为分散流引导到连续分离器部分。
    • 7. 发明申请
    • PROCESS AND EQUIPMENT FOR PRODUCING PURE LITHIUM-CONTAINING SOLUTION
    • 生产纯含锂的溶液的工艺和设备
    • WO2013182749A1
    • 2013-12-12
    • PCT/FI2013/050603
    • 2013-06-04
    • OUTOTEC OYJ
    • LAITALA, HannuKARONEN, JanneHAAVANLAMMI, Liisa
    • C01D15/08C22B26/12
    • C22B26/12C01D15/00C01D15/08C22B3/44C22B7/006Y02P10/234
    • The invention relates to a process for producing a lithium-containing solution from a lithium-containing raw-material solution, the process comprising the following steps: a) precipitation step, in which a first part of magnesium and calcium is removed from the lithium-containing raw-material solution by precipitation,b) extraction step, in which a second part of calcium and magnesium is removed from the lithium-containing solution obtained from the precipitation step by liquid-liquid extraction, a resultant product being a lithium-containing solution. The invention also relates to equipment for producing a lithium-containing solution from a lithium-containing raw-material solution, the equipment comprising :a precipitation unit arranged to remove a predetermined first part of magnesium and calcium from the lithium-containing raw-material solution by precipitating them,an extraction unit arranged to receive from the precipitation unit the lithium-containing raw-material solution and to remove therefrom a second part of calcium and magnesium by liquid-liquid extraction, the resultant product being a lithium-containing solution, and control means for controlling the operation of the precipitation unit to remove from the lithium-containing raw-material solution said predetermined first part of magnesium and calcium.
    • 本发明涉及一种由含锂原料溶液制备含锂溶液的方法,该方法包括以下步骤:a)沉淀步骤,其中镁和钙的第一部分从锂 - b)提取步骤,其中通过液 - 液萃取从沉淀步骤获得的含锂溶液中除去第二部分的钙和镁,得到的产物为含锂溶液 。 本发明还涉及从含锂原料溶液制备含锂溶液的设备,该设备包括:沉淀单元,其被布置成从含锂原料溶液中除去预定的第一部分镁和钙 通过沉淀,提取单元布置成从沉淀单元接收含锂原料溶液,并通过液 - 液萃取从其中除去第二部分钙和镁,所得产物为含锂溶液,以及 控制装置,用于控制沉淀单元的操作以从含锂原料溶液中除去所述预定的第一部分镁和钙。