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1. 发明申请

WO2007035845A2 COMPOSITIONS AND METHODS FOR HYDROGEN GENERATION 审中-公开
标题翻译：氢生成的组成和方法
公开(公告)号：WO2007035845A2
公开(公告)日：2007-03-29
申请号：PCT/US2006/036761
申请日：2006-09-21
申请人： MILLENNIUM CELL, INC. , KELLY, Michael, T. , MCNAMARA, Kevin, W. , SUN, Xiaolei
发明人： KELLY, Michael, T. , MCNAMARA, Kevin, W. , SUN, Xiaolei
IPC分类号： C07C11/24
CPC分类号： C01B3/065 , C10L1/00 , Y02E60/362
摘要： Hydrogen storage fuel compositions comprising a mixture of at least one chemical hydride compound and at least one compound, polymer, or salt that acts as a water surrogate source, and methods for thermally initiated hydrogen generation from fuel compositions, are disclosed. The water surrogate source/chemical hydride compositions are preferably solids, and may be powders, caplets, tablets, pellets or granules, for example. The water surrogate source/chemical hydride compositions may comprise alternating layers of the chemical hydride and of the water, surrogate source.
摘要翻译：包含至少一种化学氢化物化合物和至少一种充当水替代源的化合物，聚合物或盐的混合物的氢储存燃料组合物以及从燃料组合物中热引发氢生成的方法，被披露。水替代源/化学氢化物组合物优选为固体，并且例如可以是粉末，囊片，片剂，丸粒或颗粒。水替代源/化学氢化物组合物可以包含化学氢化物和水替代源的交替层。

2. 发明申请

WO2005065118A2 TRIBOROHYDRIDE SALTS AS HYDROGEN STORAGE MATERIALS AND PREPARATION THEREOF 审中-公开
标题翻译：三硼酸盐盐作为氢储存材料及其制备
公开(公告)号：WO2005065118A2
公开(公告)日：2005-07-21
申请号：PCT/US2004/040614
申请日：2004-12-03
申请人： MILLENNIUM CELL, INC. , ORTEGA, Jeffrey, V. , KELLY, Michael, T. , SNOVER, Jonathan, L. , BRADY, Jason, C. , WU, Ying
发明人： ORTEGA, Jeffrey, V. , KELLY, Michael, T. , SNOVER, Jonathan, L. , BRADY, Jason, C. , WU, Ying
IPC分类号： C01B3/06 , C01B6/21
CPC分类号： C01B3/065 , C01B6/21 , F17C11/005 , Y02E60/362
摘要： The present invention relates to the use of triborohydride salts as hydrogen storage materials. The present invention also relates to a system of using triborohydride salts to generate hydrogen gas for use in a fuel cell or other hydrogen-consuming device. A novel method of preparing triborohydride salts is also disclosed, wherein gaseous diborane is reacted with a carbonate suspended in a non-aqueous solvent in a suitable vessel with agitation. The process is typically carried out utilizing sodium carbonate to form sodium triborohydride. Other triborohydride salts can then be formed by cationic exchange. Hydrogen generating fuels according to the present invention include aqueous or hydroalcoholic solutions or slurries of a triborohydride salt, which may additionally contain a borohydride salt to provide operation over a broader temperature range.
摘要翻译：本发明涉及使用三氢化铈盐作为储氢材料。本发明还涉及一种使用三氢化烃盐产生用于燃料电池或其它耗氢装置的氢气的系统。还公开了一种制备三氢化硼盐的新方法，其中将气态乙硼烷与悬浮在非水溶剂中的碳酸酯在合适的容器中与搅拌反应。该方法通常使用碳酸钠进行以形成三氢化钠。然后可以通过阳离子交换形成其它三氯化硼盐。根据本发明的产生氢的燃料包括三氢化烃盐的水溶液或水醇溶液或浆液，其可另外含有硼氢化物盐以在更宽的温度范围内提供操作。

3. 发明申请

WO2008118438A1 COMPOSITIONS, DEVICES AND METHODS FOR HYDROGEN GENERATION 审中-公开
标题翻译：用于氢生成的组合物，装置和方法
公开(公告)号：WO2008118438A1
公开(公告)日：2008-10-02
申请号：PCT/US2008/003913
申请日：2008-03-26
申请人： MILLENNIUM CELL, INC. , KELLY, Michael, T. , ORTEGA, Jeffrey, V. , MOHRING, Richard, M.
发明人： KELLY, Michael, T. , ORTEGA, Jeffrey, V. , MOHRING, Richard, M.
IPC分类号： C01B3/02
CPC分类号： C01B3/26 , C01B3/02 , C01B3/065 , C01B3/24 , C01B2203/0838 , Y02E60/362
摘要： Methods and systems for hydrogen generation from solid hydrogen storage compositions which generate hydrogen in an exothermic reaction wherein the heat released can be absorbed by solid endothermic compositions are disclosed. The solid hydrogen storage compositions comprise mixtures of chemical hydrides and water surrogate compounds. Fuel cartridges suitable for use with compositions which generate hydrogen upon the application of thermal initiation and methods for operating the fuel cartridges are also disclosed.
摘要翻译：公开了在放热反应中产生氢的固体储氢组合物产生氢气的方法和系统，其中释放的热量可被固体吸热组合物吸收。固体储氢组合物包含化学氢化物和水替代化合物的混合物。还公开了适用于在施加热引发时产生氢气的组合物的燃料盒和用于操作燃料盒的方法。

4. 发明申请

WO2005065119A2 FUEL BLENDS FOR HYDROGEN GENERATORS 审中-公开
标题翻译：氢发生器的燃料混合物
公开(公告)号：WO2005065119A2
公开(公告)日：2005-07-21
申请号：PCT/US2004/040691
申请日：2004-12-03
申请人： MILLENNIUM CELL, INC. , KELLY, Michael, T. , WU, Ying , BRADY, Jason, C. , HAWTHORNE, Frederick, M.
发明人： KELLY, Michael, T. , WU, Ying , BRADY, Jason, C. , HAWTHORNE, Frederick, M.
IPC分类号： C01B3/06 , C10L1/32
CPC分类号： C01B3/065 , Y02E60/362
摘要： The present invention relates to improved aqueous fuels for hydrogen generators and a method for using them in the production of hydrogen. The present invention also relates to a system of using the subject aqueous fuels to generate hydrogen gas for use in a fuel cell or other device. The subject fuels contain a mixture of boron hydrides, at least one of which is a metal salt, including metal borohydrides, higher boranes and metal higher boron hydrides. The subject aqueous fuels contain a mixture of boron hydrides having a positive ionic charge ( + IC) to boron ratio of between 0.2 and 0.4 or between 0.6 and 0.99. Preferred fuels contain a mixture of boron hydrides having an ( + IC) to boron ratio between 0.2 and 0.3 or between 0.7 and 0.8. Mixtures containing a metal borohydride also contain a metal hydroxide to stability it against premature hydrolysis in the aqueous fuel media.
摘要翻译：本发明涉及用于氢气发生器的改进的含水燃料及其在生产氢气中的使用方法。本发明还涉及使用本发明的含水燃料产生用于燃料电池或其它装置的氢气的系统。目标燃料含有氢化硼的混合物，其中至少一种是金属盐，包括金属硼氢化物，较高硼烷和较高级的氢化金属氢化物。本发明的含水燃料包含具有正离子电荷（<+> IC）与硼比为0.2-0.4或0.6-0.99的硼氢化物的混合物。优选的燃料包含具有0.2-0.3或0.7和0.8之间（（+）IC）与硼的比例的硼氢化物的混合物。含有金属硼氢化物的混合物还含有金属氢氧化物以稳定其在水性燃料介质中的过早水解。

5. 发明申请

WO2008118437A3 COMPOSITIONS, DEVICES AND METHODS FOR HYDROGEN GENERATION 审中-公开
标题翻译：氢发生的组合物，装置和方法
公开(公告)号：WO2008118437A3
公开(公告)日：2008-10-02
申请号：PCT/US2008/003912
申请日：2008-03-26
申请人： MILLENNIUM CELL, INC. , KELLY, Michael, T. , ORTEGA, Jeffrey, V.
发明人： KELLY, Michael, T. , ORTEGA, Jeffrey, V.
IPC分类号： C01B3/02
摘要： Hydrogen storage fuel compositions and devices comprising a mixture of at least one chemical hydride compound and at least one proton source, and methods for thermally initiated hydrogen generation from fuel compositions are disclosed. The fuel compositions comprise an excess of hydridic hydogens relative to protic hydrogens. Fuel cartridges suitable for use with compositions which generate hydrogen upon the application of thermal initiation and methods for operating the fuel cartridges are also disclosed.
摘要翻译：公开了包含至少一种化学氢化物化合物和至少一种质子源的混合物的氢储存燃料组合物和装置，以及从燃料组合物热生成氢的方法。燃料组合物包含相对于质子氢过量的氢化物含氢原子。还公开了适用于在施加热启动时产生氢气的组合物的燃料盒和用于操作燃料盒的方法。

6. 发明申请

WO2007024688A3 HYBRID HYDROGEN FUEL SYSTEMS AND METHODS 审中-公开
公开(公告)号：WO2007024688A3
公开(公告)日：2007-03-01
申请号：PCT/US2006/032327
申请日：2006-08-18
申请人： MILLENNIUM CELL, INC. , SPALOONE, John , EASON, Ian , MOHRING, Richard, M. , FENNIMORE, Keith, A. , KELLY, Michael, T.
发明人： SPALOONE, John , EASON, Ian , MOHRING, Richard, M. , FENNIMORE, Keith, A. , KELLY, Michael, T.
IPC分类号： H01M8/06 , H01M8/18
摘要： Hybrid systems and methods for managing hydrogen system pressure and providing continuous electrical power during startup and hydrogen flow transients in an electrical power system are disclosed. The hybrid systems of the present invention comprise a hydrogen gas generator, an electricity producing hydrogen consuming device, and an auxiliary power source wherein the auxiliary power source is capable of storing energy produced by hydrogen produced by the generator, and the electricity producing hydrogen consuming device and the auxiliary power source are connected in parallel to an energy consuming device.

7. 发明申请

WO2006062672A2 APPARATUS AND PROCESS FOR THE PRODUCTION OF METALS IN STACKED ELECTROLYTIC CELLS 审中-公开
标题翻译：在堆积电解槽中生产金属的装置和方法
公开(公告)号：WO2006062672A2
公开(公告)日：2006-06-15
申请号：PCT/US2005/040761
申请日：2005-11-10
申请人： MILLENNIUM CELL, INC. , KELLY, Michael, T.
发明人： KELLY, Michael, T.
IPC分类号： C25B11/02
CPC分类号： C25C1/02 , C25C3/02 , C25C7/00 , C25C7/005
摘要： A process and apparatus for reducing an alkali metal salt to an alkali metal through electrolysis in a series of electrolytic cells are disclosed. The process employs as a separator between anode and cathode compartments a material that is both an ionic conductor of the metal ion and an electrical insulator. Preferred metals are sodium, lithium and potassium.
摘要翻译：公开了一系列电解池中通过电解将碱金属盐还原成碱金属的方法和装置。该方法在阳极和阴极隔室之间用作隔离物，其是金属离子的离子导体和电绝缘体的材料。优选的金属是钠，锂和钾。

8. 发明申请

WO2008118436A1 TECHNIQUES FOR PACKAGING AND UTILIZING SOLID HYDROGEN-PRODUCING FUEL 审中-公开
标题翻译：包装和利用固体氢生产燃料的技术
公开(公告)号：WO2008118436A1
公开(公告)日：2008-10-02
申请号：PCT/US2008/003911
申请日：2008-03-26
申请人： MILLENNIUM CELL, INC. , KELLY, Michael, T. , ORTEGA, Jeffrey, V.
发明人： KELLY, Michael, T. , ORTEGA, Jeffrey, V.
IPC分类号： H01M8/00
CPC分类号： H01M8/0606 , C01B3/065 , C01B3/503 , C01B2203/0405 , C01B2203/047 , C01B2203/0475 , C01B2203/048 , H01M8/04014 , H01M8/04089 , H01M8/04208 , H01M8/04216 , H01M8/0612 , H01M8/065 , Y02E60/362 , Y10T29/49108 , Y10T29/49808
摘要： Techniques for packaging and utilizing solid hydrogen-producing fuel are described herein. The fuel may be in the form of a bonded/compressed powder, granules, or pellets. The fuel is packaged in cartridges having hydrogen-permeable enclosures. In operation, the fuel undergoes a hydrogen-releasing Thermally Initiated Hydrolysis (TIH) reaction. A cartridge may comprise one or more fuel chambers, and several cartridges may be assembled together.
摘要翻译：本文描述了用于包装和利用固体产氢燃料的技术。燃料可以是粘合/压缩粉末，颗粒或丸粒的形式。燃料包装在具有氢气可渗透外壳的盒中。在操作中，燃料经历氢释放热起始水解（TIH）反应。墨盒可以包括一个或多个燃料室，并且几个墨盒可以组装在一起。

9. 发明申请

WO2006062673A3 PROCESSES FOR SEPARATING METALS FROM METAL SALTS 审中-公开
公开(公告)号：WO2006062673A3
公开(公告)日：2006-06-15
申请号：PCT/US2005/040762
申请日：2005-11-10
申请人： MILLENNIUM CELL, INC. , KELLY, Michael, T. , BRADY, Jason, C.
发明人： KELLY, Michael, T. , BRADY, Jason, C.
IPC分类号： C25C3/02 , C25C1/02
摘要： Electrochemical processes and apparatus for obtaining metals from metal salts, particularly separating alkali metal and borate ions from alkali metal borate compounds, are disclosed. Aqueous solutions of metal borates or metal carbonates are converted to metals by preferred electrochemical processes. These electrochemical processes also may be integrated into processes for the production of borohydrides, such as sodium borohydride.

10. 发明申请

WO2003051957A1 PROCESSES FOR SYNTHESIZING ALKALI METAL BOROHYDRIDE COMPOUNDS 审中-公开
标题翻译：合成碱金属硼氢化合物的方法
公开(公告)号：WO2003051957A1
公开(公告)日：2003-06-26
申请号：PCT/US2002/040252
申请日：2002-12-16
申请人： MILLENNIUM CELL, INC.
发明人： ORTEGA, Jeffrey, V. , WU, Ying , AMENDOLA, Steven, C. , KELLY, Michael, T.
IPC分类号： C08G63/00
CPC分类号： C01B6/23 , C01B6/21
摘要： Processes for synthesizing borohydride compounds with reduced energy requirements and high efficiency are disclosed. The processes include the reaction of a base with a borane complex to produce a borohydride compound of formula YBH 4 , where Y is a monovalent cationic moiety.
摘要翻译：公开了具有降低的能量需求和高效率合成硼氢化合物的方法。所述方法包括碱与硼烷络合物的反应以制备式YBH4的硼氢化合物，其中Y是一价阳离子部分。

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