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1. 发明申请

WO2013130450A3 SELF-REDUCING METAL COMPLEX INKS SOLUBLE IN POLAR PROTIC SOLVENTS AND IMPROVED CURING METHODS 审中-公开
标题翻译：自我还原金属络合物可溶于极性溶剂和改进的固化方法
公开(公告)号：WO2013130450A3
公开(公告)日：2013-11-21
申请号：PCT/US2013027768
申请日：2013-02-26
申请人： LIQUID X PRINTED METALS INC , MCCULLOUGH RICHARD D , BELOT JOHN , POTASH REBECCA , SEFTON ELIZABETH , COX CHRISTIANA
发明人： MCCULLOUGH RICHARD D , BELOT JOHN , POTASH REBECCA , SEFTON ELIZABETH , COX CHRISTIANA
IPC分类号： C09D11/00 , H05K1/09 , H05K3/10
CPC分类号： C09D11/52 , C07F1/10 , C09D11/322 , H05K1/092 , H05K1/16 , H05K3/105
摘要： Metal complexes adapted to form metallic conductive films upon deposition and treatment. The complexes can have a high concentration of metal and can be soluble in polar protic solvent including ethanol and water. The metal complex can be a covalent complex and can comprise a first and second ligand. Low temperature treatment can be used to convert the complex to a metal. The metallic conductive film can have low resistivity and work function close to pure metal. Coinage metals can be used (e.g., Ag). The ligands can be dative bonding ligands including amines and carboxylate ligands. The ligands can be adapted to volatilize well. High yields of metal can be achieve with high conductivity.
摘要翻译：金属络合物适于在沉积和处理时形成金属导电膜。配合物可以具有高浓度的金属并且可以溶于包括乙醇和水的极性质子溶剂中。该金属络合物可以是共价络合物并且可以包含第一和第二配体。低温处理可用于将复合物转化为金属。金属导电膜可以具有接近纯金属的低电阻率和功函数。可以使用硬币金属（例如Ag）。配体可以是配位键合配体，包括胺和羧酸酯配体。配体可适应挥发。高导电率可以实现高产量的金属。

2. 发明申请

WO2012151500A1 METAL ALLOYS FROM MOLECULAR INKS 审中-公开
标题翻译：分子油中的金属合金
公开(公告)号：WO2012151500A1
公开(公告)日：2012-11-08
申请号：PCT/US2012036549
申请日：2012-05-04
申请人： LIQUID X PRINTED METALS INC , MCCULLOUGH RICHARD D , BELOT JOHN , POTASH REBECCA
发明人： MCCULLOUGH RICHARD D , BELOT JOHN , POTASH REBECCA
IPC分类号： H05K3/10 , C09D11/00 , H05K1/09 , H05K3/12
CPC分类号： C09D11/52 , B01J23/52 , B01J37/0219 , B01J37/086 , B41F17/00 , B41J2/01 , C09D11/322 , C09D11/36 , H01B1/02 , H05K1/092 , H05K3/105 , H05K3/1283 , H05K2203/1476
摘要： Low temperature processes for converting mixtures of metal inks into alloys. The alloys can be dealloyed by etching. A method comprising: depositing at least one precursor composition on at least one substrate to form at least one deposited structure, wherein the precursor composition comprises at least two metal complexes, including at least one first metal complex comprising at least one first metal and at least one second metal complex different from the first metal complex and comprising at least one second metal different from the first metal, treating the deposited structure so that the first metal and the second metal form elemental forms of the first metal and the second metal in a treated structure. Further, one can remove at least some of the first metal to leave a nanoporous material comprising at least the second metal. Precursor compositions can be formulated to be homogeneous compositions. Applications include electrodes, organic electronic devices, catalysis, fuel cells, metal grids, and biodiagnostics.
摘要翻译：将金属油墨混合物转化成合金的低温工艺。合金可以通过蚀刻来脱模。一种方法，包括：在至少一个底物上沉积至少一种前体组合物以形成至少一种沉积结构，其中所述前体组合物包含至少两种金属络合物，包括至少一种包含至少一种第一金属和至少一种第一金属的第一金属络合物与第一金属络合物不同的第二金属络合物，并且包含不同于第一金属的至少一种第二金属，处理沉积结构，使得第一金属和第二金属在处理过的第一金属和第二金属中形成元素形式的第一金属和第二金属结构体。此外，可以去除至少一些第一金属以留下至少包含第二金属的纳米多孔材料。前体组合物可以配制成均匀的组合物。应用包括电极，有机电子器件，催化，燃料电池，金属网格和生物诊断。

3. 发明申请

WO2011057218A3 METAL INK COMPOSITIONS, CONDUCTIVE PATTERNS, METHODS, AND DEVICES 审中-公开
标题翻译：金属墨水组合物，导电图案，方法和装置
公开(公告)号：WO2011057218A3
公开(公告)日：2012-04-19
申请号：PCT/US2010055874
申请日：2010-11-08
申请人： UNIV CARNEGIE MELLON , MCCULLOUGH RICHARD D , BELOT JOHN A , JAVIER ANNA , POTASH REBECCA
发明人： MCCULLOUGH RICHARD D , BELOT JOHN A , JAVIER ANNA , POTASH REBECCA
IPC分类号： C23C18/06 , C07F1/00 , C07F9/50 , C09D11/00 , C09D11/10 , C23C18/08
CPC分类号： C23C18/06 , C07F1/005 , C07F9/5045 , C09D11/101 , C09D11/322 , C09D11/52 , C23C18/08 , H05K3/105 , H05K3/125 , H05K2203/121
摘要： Metal complexes adapted to form conductive metal films and lines upon deposition and treatment. The metal complex can be a covalent complex and can comprise a first and second ligand. Low temperature treatment can be used to convert the complex to a metal. The metal films and lines can have low resistivity and work function similar to pure metal. Coinage metals can be used (e.g., Ag, Au, Cu). The ligands can be dative bonding ligands including amines, unsymmetrical amines, and carboxylate ligands. Sulfur complexes can be used. Carboxylate ligands can be used. The complexes can have a high concentration of metal and can be soluble in aromatic hydrocarbon solvent. The ligands can be adapted to volatilize well. Inkjet printing can be carried out. High yields of metal can be achieve with high conductivity.
摘要翻译：适于在沉积和处理时形成导电金属膜和管线的金属络合物。金属络合物可以是共价复合物，并且可以包含第一和第二配体。低温处理可用于将络合物转化为金属。金属膜和管线可以具有与纯金属相似的低电阻率和功函数。可以使用钴矿金属（例如Ag，Au，Cu）。配体可以是配位键配体，包括胺，不对称胺和羧酸盐配体。可以使用硫络合物。可以使用羧酸盐配体。络合物可以具有高浓度的金属，并且可溶于芳族烃溶剂。配体可适应于挥发良好。喷墨打印可以进行。金属的高产量可以实现高导电性。

4. 发明申请

WO2007025189A3 ELECTRICALLY CONDUCTIVE BLOCKCOPOLYMERS AND CONTROLLED RADICAL POLYMERIZATION 审中-公开
标题翻译：电导电阻聚物和控制的放射性聚合
公开(公告)号：WO2007025189A3
公开(公告)日：2007-05-18
申请号：PCT/US2006033324
申请日：2006-08-25
申请人： UNIV CARNEGIE MELLON , MCCULLOUGH RICHARD D , IOVU MICHAEL C
发明人： MCCULLOUGH RICHARD D , IOVU MICHAEL C
IPC分类号： H01B1/12 , H01L51/30
CPC分类号： H01L51/0036 , C08F293/005 , C08F2438/03 , C08G61/126 , H01B1/127 , H01L51/0043
摘要： Electrically conductive polymers including block copolymers, polythiophene copolymers, and regioregular polythiophene copolymers, prepared by controlled radical polymerization including RAPT and NMP polymerization methods. Polymers having low metal content can be prepared. Method of synthesizing polythiophene polymers and copolymers using RAFT and NMP polymerization are also provided. Regioregular polythiophenes are preferred. Blends with polythiophenes and non-conducting polymers can be prepared. Applications include PLEDs, sensors, and optoelectronics.
摘要翻译：包括嵌段共聚物，聚噻吩共聚物和区域定向聚噻吩共聚物的导电聚合物，其通过包括RAPT和NMP聚合方法的受控自由基聚合制备。可以制备具有低金属含量的聚合物。还提供了使用RAFT和NMP聚合合成聚噻吩聚合物和共聚物的方法。区域聚噻吩是优选的。可以制备与聚噻吩和非导电聚合物的共混物。应用包括PLED，传感器和光电子。

5. 发明申请

WO2006107740A2 LIVING SYNTHESIS OF CONDUCTING POLYMERS INCLUDING REGIOREGULAR POLYMERS, POLYTHIOPHENES, AND BLOCK COPOLYMERS 审中-公开
标题翻译：导电聚合物的生物合成，包括后续聚合物，聚乙烯和嵌段共聚物
公开(公告)号：WO2006107740A2
公开(公告)日：2006-10-12
申请号：PCT/US2006011840
申请日：2006-03-31
申请人： UNIV CARNEGIE MELLON , MCCULLOUGH RICHARD D , IOVU MIHAELA C , SHEINA ELENA E
发明人： MCCULLOUGH RICHARD D , IOVU MIHAELA C , SHEINA ELENA E
IPC分类号： H01L29/24
CPC分类号： C08G61/126 , B01J31/2409 , B01J2231/4205 , B01J2531/847 , H01L51/0036 , H01L51/0043
摘要： Regioregular poly(3-alkylthiophenes) and other polythiophenes can be prepared by living polymerization which have good solubility, processability and environmental stability. The polymerization method can afford regioregular poly(3-alkylthiophenes) in high yields. Kinetic study of polymerization revealed the living character of this process. The molecular weight of ?oly(3-alkylthiophenes) is a function of the molar ratio of the monomer to nickel initiator, and conducting polymers with relatively narrow molecular weight distribution (PDKl.5) are now readily available. Sequential monomer addition resulted in new block copolymers containing different poly(3-alkylthiophene) segments, which further confirms the "livingness" of this system. Other synthetic methods can be used as well to conduct living polymerization. Blends and electronic devices can be prepared.
摘要翻译：方位聚（3-烷基噻吩）和其它聚噻吩可以通过具有良好的溶解性，加工性和环境稳定性的活性聚合来制备。聚合方法可以高收率地提供区域性聚（3-烷基噻吩）。聚合的动力学研究揭示了这一过程的生命特征。丙烯酸（3-烷基噻吩）的分子量是单体与镍引发剂的摩尔比的函数，而具有相对较窄分子量分布的导电聚合物（PDK1.5）现在是容易获得的。顺序单体加成产生含有不同聚（3-烷基噻吩）链段的新嵌段共聚物，这进一步证实了该体系的“活性”。也可以使用其它合成方法进行活性聚合。可以制备混合物和电子装置。

6. 发明申请

WO2008063731A2 PURIFICATION METHODS AND PURIFIED POLYMERS 审中-公开
标题翻译：纯化方法和纯化聚合物
公开(公告)号：WO2008063731A2
公开(公告)日：2008-05-29
申请号：PCT/US2007077456
申请日：2007-08-31
申请人： UNIV CARNEGIE MELLON , MCCULLOUGH RICHARD D , IOVU MIHAELA C
发明人： MCCULLOUGH RICHARD D , IOVU MIHAELA C
CPC分类号： H01L51/0025 , C08G61/08 , C08G61/126 , H01B1/127 , H01L51/0036 , Y02E10/549
摘要： Metal complexing agents are used to purify polymers including conducting polymers to provide very low metal content. The process comprises precipitating the polymer in solution into a solvent system comprising the metal complexing agent. Very low levels including undetectable levels of metals such as nickel and magnesium can be achieved. High purity polymers are used in electronics and photovoltaic applications.
摘要翻译：金属络合剂用于纯化包括导电聚合物在内的聚合物以提供非常低的金属含量。该方法包括将溶液中的聚合物沉淀到包含金属络合剂的溶剂体系中。可以实现非常低的含量，例如不可检测的金属如镍和镁。高纯度聚合物用于电子和光伏应用。

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