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1. 发明申请

WO2012148695A2 INTEGRATED PROCESS TO CO-PRODUCE 1,1,1,3,3-PENTAFLUOROPROPANE, TRANS-1-CHLORO-3,3,3-TRIFLUOROPROPENE and TRANS-1,3,3,3-TETRAFLUOROPROPENE 审中-公开
标题翻译：合成方法共同生产1,1,1,3,3-三氟硼酸，反式-1-氯代-3,3,3-三氟丙烯和TRANS-1,3,3,3-四氯丙烯
公开(公告)号：WO2012148695A2
公开(公告)日：2012-11-01
申请号：PCT/US2012/033419
申请日：2012-04-13
申请人： HONEYWELL INTERNATIONAL INC. , WANG, Haiyou , MERKEL, Daniel C. , POKROVSKI, Konstantin A. , TUNG, Hsueh Sung , SHANKLAND, Ian
发明人： WANG, Haiyou , MERKEL, Daniel C. , POKROVSKI, Konstantin A. , TUNG, Hsueh Sung , SHANKLAND, Ian
IPC分类号： C07C17/087 , C07C21/18 , B01J23/18 , B01J21/06
CPC分类号： C07C17/206 , C07B2200/09 , C07C17/087 , C07C17/25 , C07C17/383 , Y02P20/125 , C07C19/10 , C07C19/08 , C07C21/18
摘要： Disclosed is a fully integrated process for making 1,1,1,3,3-pentafluoropropane (HFC-245fa), trans-1-chloro-3,3,3-trifluoropropene (HCFO-1233zd(E)), and trans-1,3,3,3-tetrafluoropropene (HFO-1234ze(E)). The chemistry involves (a) the reaction of 1,1,1,3,3-pentachloropropane (HCC-240fa), or a derivative thereof selected from 1,1,3,3-tetrachloropropene and 1,3,3,3-tetrachloropropene, with anhydrous HF in excess in the presence of a catalyst in a liquid-phase reactor in such a way as to co-produce HCFO-1233zd, HFO-1234ze, HCFC-244fa (3-chloro-1,1,1,3-tetrafluoropropane), and HFC-245fa in a first reactor; (b) the reaction of HCFO-1233zd and HFO-1234ze with HCl in excess in the presence of a catalyst in a second reactor to convert these two olefins into HCFC-243fa and HCFC-244fa, respectively; (c) the reaction of HCFC-243fa and HCFC-244fa over a dehydrochlorination catalyst or in a caustic solution in a third reactor to form HCFO-1233zd and HFO-1234ze; and (d) the reaction of HCFO-1233zd(Z) and HFO-1234ze(Z) in the presence of a catalyst in a fourth reactor to form trans-1233zd and trans-1234ze, respectively.
摘要翻译：公开了制备1,1,1,3,3-五氟丙烷（HFC-245fa），反式-1-氯-3,3,3-三氟丙烯（HCFO-1233zd（E））的完全一体化方法， 1,3,3,3-四氟丙烯（HFO-1234ze（E））。该化学方法包括（a）1,1,1,3,3-五氯丙烷（HCC-240fa）或其衍生物选自1,1,3,3-四氯丙烯和1,3,3,3-四氯丙烯的反应，四氯丙烯，在催化剂存在下，在液相反应器中以无水HF过剩，以共同生产HCFO-1233zd，HFO-1234ze，HCFC-244fa（3-氯-1,1,1， 3-四氟丙烷）和HFC-245fa在第一反应器中; （b）HCFO-1233zd和HFO-1234ze与HCl在过渡催化剂存在下在第二反应器中的反应，分别将这两种烯烃转化为HCFC-243fa和HCFC-244fa; （c）HCFC-243fa和HCFC-244fa在脱氯化氢催化剂或第三反应器中的苛性碱溶液中的反应，形成HCFO-1233zd和HFO-1234ze; 和（d）HCFO-1233zd（Z）和HFO-1234ze（Z）在催化剂存在下在第四反应器中的反应分别形成反式-1233zd和反式1234ze。

2. 发明申请

WO2012154227A2 INTEGRATED PROCESS TO CO-PRODUCE TRANS-1-CHLORO-3,3,3-TRIFLUOROPROPENE, TRANS-1,3,3,3-TETRAFLUOROPROPENE, AND 1,1,1,3,3-PENTAFLUOROPROPANE 审中-公开
标题翻译：共同生产转化-1-氯代-3,3,3-三氟丙烯的方法，反式-1,3,3,3-四氢呋喃和1,1,1,3,3-三氟硼烷
公开(公告)号：WO2012154227A2
公开(公告)日：2012-11-15
申请号：PCT/US2012/021061
申请日：2012-01-12
申请人： HONEYWELL INTERNATIONAL INC. , MERKEL, Daniel C. , WANG, Haiyou , POKROVSKI, Konstantin A. , TUNG, Hsueh Sung , SHANKLAND, Ian
发明人： MERKEL, Daniel C. , WANG, Haiyou , POKROVSKI, Konstantin A. , TUNG, Hsueh Sung , SHANKLAND, Ian
IPC分类号： C07C17/20 , C07C17/42 , C07C21/18 , B01J19/24
CPC分类号： C07C17/25 , C07C17/087 , C07C17/206 , Y02P20/125 , Y02P20/582 , C07C21/18 , C07C19/10 , C07C19/08
摘要： Disclosed is an integrated process to co-produce trans-1-chloro-3,3,3-trifluoro- propene (1233zd(E)), trans-1,3,3,3-tetrafluoropropene (1234ze(E)), and 1,1,1,3,3- pentafluoropropane (245fa). Overall the co-production is a three-step process. The chemistry involves the steps of: (1) the reaction of 240fa with anhydrous HF in excess in a liquid-phase catalyzed reactor in such a way as to co-produce primarily 1233zd(E) and 244fa (plus byproduct HC1); (2) the 244fa stream can then be used to directly produce any of the three desired products; (3 a) the 244fa stream can be dehydrochlorinated to produce the desired second product 1234ze(E); and/or (3b) the 244fa stream can be dehydrofluorinated to produce 1233zd(E) if more of that product is desired; and/or (3 c) the 244fa stream can be further fluorinated to form 245 fa.
摘要翻译：公开了共反应产生反式-1-氯-3,3,3-三氟丙烯（1233zd（E）），反式-1,3,3,3-四氟丙烯（1234ze（E））和 1,1,1,3,3-五氟丙烷（245fa）。总的来说，联合制作是一个三步骤的过程。该化学方法包括以下步骤：（1）在液相催化反应器中240fa与无水HF过量反应，主要共同生产1233zd（E）和244fa（加副产物HC1）; （2）然后可以使用244fa流直接生产三种所需产物中的任何一种; （3a）244fa流可以脱氯化氢以产生所需的第二产物1234ze（E）; 和/或（3b）如果需要更多的该产物，则244fa流可以被脱氟化氢以产生1233zd（E）和/或（3c）244fa流可以进一步氟化以形成245fa。

3. 发明申请

WO2012094288A2 HIGH PURITY E-1-CHLORO-3,3,3-TRIFLUOROPROPENE AND METHODS OF MAKING THE SAME 审中-公开
标题翻译：高纯E-1-氯-3,3,3-三氟丙烯及其制备方法
公开(公告)号：WO2012094288A2
公开(公告)日：2012-07-12
申请号：PCT/US2012/020035
申请日：2012-01-03
申请人： HONEYWELL INTERNATIONAL INC. , POKROVSKI, Konstantin A. , SINGH, Rajiv Ratna , SHANKLAND, Ian , TUNG, Hsueh Sung
发明人： POKROVSKI, Konstantin A. , SINGH, Rajiv Ratna , SHANKLAND, Ian , TUNG, Hsueh Sung
IPC分类号： C07C17/20 , C07C19/10 , C07C21/18 , C07B39/00
CPC分类号： C07C17/361 , C07B2200/09 , C07C17/206 , C07C17/25 , C07C19/10 , C07C21/18
摘要： The present invention discloses high purity E-1-chloro-3,3,3-trifluoropropene (1233zd(E)) and methods to produce the same. More specifically, the present invention discloses the methods of making 1233zd(E) essentially free of toxic impurities (e.g. 2-chloro-3,3,3-trifluoropropene (1233xf), chlorotetrafluoro-propene (1224), and 3,3,3-trifluoropropyne). The present invention further provides methods for making high purity 1233zd(E) with concentration of 1233xf and 1224 at or below 200 parts per million (ppm) and 3,3,3-trifluoropropyne impurities at or below 20 ppm. Formation of 1233xf impurity can be avoided if pure 1,1,1,3,3-pentachloropropane is used as a starting material. It was also found that formation of 1233xf is avoided if a liquid phase manufacturing process is used.
摘要翻译：本发明公开了高纯度E-1-氯-3,3,3-三氟丙烯（1233zd（E））及其制备方法。更具体地说，本发明公开了制备1233zd（E）的方法基本上不含有毒杂质（例如2-氯-3,3,3-三氟丙烯（1233xf），氯四氟丙烯（1224）和3,3,3 -trifluoropropyne）。本发明进一步提供了制备浓度为1233xf和1224的高纯度1233zd（E）等于或低于百万分之200（ppm）和低于20ppm的3,3,3-三氟丙炔杂质的方法。如果使用纯1,1,1,3,3-五氯丙烷作为原料，则可避免形成1233xf杂质。还发现如果使用液相制造工艺，则避免形成1233xf。

4. 发明申请

WO2008057794A1 PROCESS FOR THE MANUFACTURE OF FLUORINATED OLEFINS 审中-公开
标题翻译：氟化烯烃的制备方法
公开(公告)号：WO2008057794A1
公开(公告)日：2008-05-15
申请号：PCT/US2007/082601
申请日：2007-10-26
申请人： HONEYWELL INTERNATIONAL INC. , VANDERPUY, Michael , COOK, George R. , SCHEIDLE, Peter H. , ULRICH, Kevin D. , WANG, Haiyou , TUNG, Hsueh Sung , SHANKLAND, Ian
发明人： VANDERPUY, Michael , COOK, George R. , SCHEIDLE, Peter H. , ULRICH, Kevin D. , WANG, Haiyou , TUNG, Hsueh Sung , SHANKLAND, Ian
IPC分类号： C07C17/25 , C07C17/354 , C07C19/08 , C07C19/10 , C07C19/14 , C07C21/18
CPC分类号： C07C17/25 , C07C17/354 , C07C17/38 , C07C19/14 , C07C19/08
摘要： A process for the production of fluorinated olefins, preferably fluorinated propenes, by contacting a feed stream containing a fluorinated olefin and hydrogen with a first amount of catalyst to produce the hydrofluorocarbon, wherein a first exit stream contains unreacted fluorinated olefin and hydrogen; contacting the first exit stream with a second amount of catalyst to produce a hydrofluorocarbon, wherein the second amount of catalyst is preferably greater than the first amount of catalyst; and contacting the hydrofluorocarbon with a catalyst for dehydrohalogenation to produce a product stream of fluorinated olefin.
摘要翻译：通过使包含氟化烯烃和氢气的进料流与第一量催化剂接触以产生氢氟烃来生产氟化烯烃，优选氟化丙烯的方法，其中第一出口流含有未反应的氟化烯烃和氢; 使第一出口流与第二量的催化剂接触以产生氢氟烃，其中第二量的催化剂优选大于第一量的催化剂; 并将氢氟烃与用于脱卤化氢的催化剂接触以产生氟化烯烃的产物流。

5. 发明申请

WO2010088196A2 AZEOTROPE-LIKE COMPOSITIONS OF PENTAFLUOROPROPANE, CHLOROTRIFLUOROPROPENE, AND HYDROGEN FLUORIDE 审中-公开
标题翻译： P OR OP E IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE IDE
公开(公告)号：WO2010088196A2
公开(公告)日：2010-08-05
申请号：PCT/US2010/022053
申请日：2010-01-26
申请人： HONEYWELL INTERNATIONAL INC. , HULSE, Ryan , SINGH, Rajiv Ratna , TUNG, Hsueh Sung , SHANKLAND, Ian
发明人： HULSE, Ryan , SINGH, Rajiv Ratna , TUNG, Hsueh Sung , SHANKLAND, Ian
IPC分类号： C11D7/50 , C11D7/30 , C07C17/25 , C07C21/18 , C07C19/08 , C01B7/19
CPC分类号： C07C19/08 , C07C17/206 , C07C17/25 , C07C17/383 , C07C21/18
摘要： The invention is directed to a ternary azeotrope-like mixture consisting essentially of effective amounts of 1,1,1,3,3-pentafluoropropane, 1-chloro-3,3,3-trifluoropropene, and hydrogen fluoride.
摘要翻译：本发明涉及基本上由有效量的1,1,1,3,3-五氟丙烷，1-氯-3,3,3-三氟丙烯和氟化氢组成的三元共沸混合物。

6. 发明申请

WO2005097716A1 METHOD OF MAKING DIFLUOROMETHANE, 1,1,1-TRIFLUOROETHANE AND 1,2-DIFLUOROETHANE 审中-公开
标题翻译：制备二氟甲磺酸的方法，1,1,1-三氟乙基和1,2-二氟乙基
公开(公告)号：WO2005097716A1
公开(公告)日：2005-10-20
申请号：PCT/US2005/011125
申请日：2005-03-31
申请人： HONEYWELL INTERNATIONAL INC. , MERKEL, Daniel, C. , SHANKLAND, Ian , TUNG, Hsuehsung
发明人： MERKEL, Daniel, C. , SHANKLAND, Ian , TUNG, Hsuehsung
IPC分类号： C07C17/20
CPC分类号： B01J27/125 , B01J21/18 , B01J27/08 , B01J27/135 , B01J37/26 , C07C17/206 , C07C17/208 , C07C17/21 , C07C19/08 , Y02P20/582
摘要： A process for the production of difluoromethane (HFC-32), 1,1,1-trifluoroethane (HFC-143a) and 1,1-difluoroethane (HFC-152a). In the process the following steps are employed: (a) providing a reaction vessel, (b) providing in the reaction vessel activated carbon impregnated with a strong Lewis acid fluorination catalyst selected from halides of As, Sb, Al, TI, In, V, Nb, Ta, Ti, Zr and Hf, (c) activating the catalyst by passing through the activated carbon impregnated with a strong Lewis acid fluorination catalyst anhydrous hydrogen fluoride gas and chlorine gas, (d) contacting, in vapor state in the reaction vessel containing the activated catalyst, hydrogen fluoride and one or more halogenated hydrocarbons selected from chlorofluoromethane, dichloromethane, 1,1,1-trichloroethane, vinyl chloride, 1,1-dichloroethylene, 1.2-dichloroethylene, 1,2-dichloroethane, and 1,1-dichloroethane for a time and at a temperature to produce a product stream comprising hydrofluorocarbon product(s) corresponding to the chlorinated hydrocarbon reactant(s), and one or more of hydrogen chloride, unreactacted chlorinated hydrocarbon reactant(s), under-fluorinated intermediates, and unreacted hydrogen fluoride, and (e) separating the hydrofluorocarbon product(s) from the product stream.
摘要翻译：制备二氟甲烷（HFC-32），1,1,1-三氟乙烷（HFC-143a）和1,1-二氟乙烷（HFC-152a）的方法。在该过程中，采用以下步骤：（a）提供反应容器，（b）在反应容器中提供用强路易斯酸氟化催化剂浸渍的活性炭，该催化剂选自As，Sb，Al，TI，In，V ，Nb，Ta，Ti，Zr和Hf，（c）通过浸渍有强力路易斯酸氟化催化剂的无水氟化氢气体和氯气的活性炭活化催化剂，（d）在反应中以气态接触含有活化催化剂的容器，氟化氢和选自氯氟甲烷，二氯甲烷，1,1,1-三氯乙烷，氯乙烯，1,1-二氯乙烯，1,2-二氯乙烯，1,2-二氯乙烷和1,1-二氯乙烷的一种或多种卤代烃，在一个温度下产生包含对应于氯代烃反应物的氢氟烃产物的产物流，以及一种或多种氯化氢，未反应的氯化氢化碳氢化合物 n反应物，非氟化中间体和未反应的氟化氢，和（e）从产物流中分离氢氟烃产物。

7. 发明申请

WO2009151764A3 CARRIER SOLVENT FOR FINGERPRINT FORMULATIONS 审中-公开
公开(公告)号：WO2009151764A3
公开(公告)日：2009-12-17
申请号：PCT/US2009/040422
申请日：2009-04-14
申请人： HONEYWELL INTERNATIONAL INC. , NALEWAJEK, David , CANTLON, Cheryl L. , POSS, Andrew J. , SINGH, Rajiv Ratna , SHANKLAND, Ian
发明人： NALEWAJEK, David , CANTLON, Cheryl L. , POSS, Andrew J. , SINGH, Rajiv Ratna , SHANKLAND, Ian
IPC分类号： A61B5/117 , G05F1/00
摘要： A method and composition for transforming a latent physiological biometric into a visible physiological biometric are provided, the method comprising: providing a latent biometric disposed on a surface of an article, wherein said biometric comprises at least one eccrine-derived compound; contacting said latent biometric with a developing solution, wherein said developing solution comprises at least one imaging reagent selected from ninhydrin and 1,8-diazafluoren-9-one and a carrier solvent comprising at least one C 3 - C 4 hydrofluorocarbon; and reacting said imaging reagent with said eccrine-derived compound to produce a visible physiological biometric.

8. 发明申请

WO2009132242A2 BLOWING AGENTS FOR POLYMERIC FOAMS 审中-公开
标题翻译：用于聚合物泡沫的吹制剂
公开(公告)号：WO2009132242A2
公开(公告)日：2009-10-29
申请号：PCT/US2009/041615
申请日：2009-04-24
申请人： HONEYWELL INTERNATIONAL INC. , SINGH, Rajiv, R. , SHANKLAND, Ian , BOWMAN, James, M. , WILLIAMS, David, J.
发明人： SINGH, Rajiv, R. , SHANKLAND, Ian , BOWMAN, James, M. , WILLIAMS, David, J.
IPC分类号： C08J9/06 , C08J9/04 , C08K5/02 , C08L75/04 , C08L61/04 , C08L25/04 , C08L23/04 , C08L23/10 , C08J9/00
CPC分类号： C07C21/18 , C08G2101/00 , C08J9/144 , C08J9/147 , C08J2205/052
摘要： Provided are foam blowing agents comprising one or more chlorofluoroolefins selected from 1,2-dichloro-1,2-difluoroethene, 3,3-dichloro-3-fluoropropene, 2-chloro-1,1,1,3,4,4,4-heptafluoro-2-butene, and 2-chloro-1,1,1,4,4,4-hexafluoro-2-butene, as well as foams produced therefrom.
摘要翻译：提供了包含一种或多种选自1,2-二氯-1,2-二氟乙烯，3,3-二氯-3-氟丙烯，2-氯-1,1,1,2-四氟乙烯， 1,3,4,4,4-七氟-2-丁烯和2-氯-1,1,1,4,4,4-六氟-2-丁烯，以及由其生产的泡沫。

9. 发明申请

WO2009025921A3 METHOD AND SYSTEM FOR RESTRAINING A CHEMICAL DISCHARGE 审中-公开
公开(公告)号：WO2009025921A3
公开(公告)日：2009-02-26
申请号：PCT/US2008/065926
申请日：2008-06-05
申请人： HONEYWELL INTERNATIONAL INC. , SINGH, Rajiv, R. , SHANKLAND, Ian , SZUCH, Colleen, D.
发明人： SINGH, Rajiv, R. , SHANKLAND, Ian , SZUCH, Colleen, D.
IPC分类号： B09B3/00 , B01J19/00
摘要： A method for restraining a chemical discharge comprising (a) deploying a binding agent into a receptacle containing a hazardous material in a liquid state upon the occurrence of at least one predetermined event that increases the risk of accidentally discharging or leaking the hazardous material from the receptacle; and (b) contacting the hazardous material with the binding agent to form a composition comprising at least a portion of the hazardous material and the binding agent and having at least one property selected from a solid or semisolid state, a viscosity greater than the hazardous material's viscosity at ambient conditions, a vapor pressure lower than the hazardous material's vapor pressure at ambient conditions, and a surface tension greater that the hazardous material's surface tension.

10. 发明申请

WO2009151764A2 CARRIER SOLVENT FOR FINGERPRINT FORMULATIONS 审中-公开
标题翻译：载体溶液用于指纹制剂
公开(公告)号：WO2009151764A2
公开(公告)日：2009-12-17
申请号：PCT/US2009/040422
申请日：2009-04-14
申请人： HONEYWELL INTERNATIONAL INC. , NALEWAJEK, David , CANTLON, Cheryl L. , POSS, Andrew J. , SINGH, Rajiv Ratna , SHANKLAND, Ian
发明人： NALEWAJEK, David , CANTLON, Cheryl L. , POSS, Andrew J. , SINGH, Rajiv Ratna , SHANKLAND, Ian
IPC分类号： A61B5/117
CPC分类号： A61B5/1172
摘要： A method and composition for transforming a latent physiological biometric into a visible physiological biometric are provided, the method comprising: providing a latent biometric disposed on a surface of an article, wherein said biometric comprises at least one eccrine-derived compound; contacting said latent biometric with a developing solution, wherein said developing solution comprises at least one imaging reagent selected from ninhydrin and 1,8-diazafluoren-9-one and a carrier solvent comprising at least one C 3 - C 4 hydrofluorocarbon; and reacting said imaging reagent with said eccrine-derived compound to produce a visible physiological biometric.
摘要翻译：提供了一种用于将潜在生理学生物转化为可见生理生物学的方法和组合物，所述方法包括：提供设置在制品表面上的潜伏生物测定，其中所述生物测定法包含至少一种衍生化合物; 使所述潜在生物测定与显影溶液接触，其中所述显影溶液包含至少一种选自茚三酮和1,8-二氮杂芴-9-酮的成像剂和包含至少一种C 3 -C 4氢氟烃的载体溶剂; 并使所述成像试剂与所述外分泌衍生的化合物反应以产生可见的生理学生物学特征。

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