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1. 发明申请

WO2007058836A2 1,1,1,3,3,3-HEXAFLUOROPROPANE PURIFICATION WITH PHOTOCHLORINATION EQUIPMENT 审中-公开
标题翻译： 1,1,1,3,3,3-HEXAFLORORROPANE用光电设备进行纯化
公开(公告)号：WO2007058836A2
公开(公告)日：2007-05-24
申请号：PCT/US2006043417
申请日：2006-11-08
申请人： HONEYWELL INT INC , CHIU YUON , DAVID MERKEL , HSUEHSUNG TUNG
发明人： CHIU YUON , DAVID MERKEL , HSUEHSUNG TUNG
CPC分类号： C07C17/38 , C07C17/395 , C07C19/08
摘要： A continuous, vapor phase method for purifying a crude mixture of 1 ,1 ,1 ,3,3,3-hexafluoropropane and one or more unsaturated fluorocarbon compounds, the process comprising: a) providing a photochlorinator vessel comprising : 1) a UV lamp unit comprising a UV lamp located in a transparent inner well, the transparent inner well being located within a transparent outer well, the outer well being provided with material for cooling walls of the inner and outer wells; the inner well and the outer well defining separate chambers isolated from each other; and 2) a reaction vessel into which the UV lamp unit has been inserted; b) introducing into the reaction vessel a gaseous mixture of Cb and a distillation inseparable mixture of 1 ,1 ,1,3,3,3-hexafluoropropane and one or more unsaturated fluorocarbon compdunds; c) reacting, in the gaseous state and in the presence of UV light from the photochlorinator, the mixture with CI2 with the distillation inseparable mixture of 1 ,1 ,1 ,3,3,3-hexafluoropropane and one or more unsaturated compounds to saturate unsaturated fluorocarbons into a reacted mixture, and d) separating a purified 1 , 1 ,1 , 3,3, 3-hexafluoroporpane product containing less than 1000 ppm, most preferably less than 100 ppm unsaturated fluorocarbons.
摘要翻译：一种用于纯化1,1,1,3,3,3-六氟丙烷和一种或多种不饱和碳氟化合物的粗混合物的连续气相法，该方法包括：a）提供光氯化器容器，包括：1）UV灯该单元包括位于透明内部井中的UV灯，所述透明内部井位于透明外部井内，所述外部井具有用于冷却所述内部和外部井的壁的材料; 所述内部井和所述外部井定义分离的彼此隔离的室; 和2）UV灯单元插入其中的反应容器; b）向反应容器中引入Cb的气态混合物和1,1,1,3,3,3-六氟丙烷与一种或多种不饱和氟碳化合物的蒸馏不可分离的混合物; c）在气态下和在来自光氯离子的UV光的存在下，将CI2与1,1,1,3,3,3-六氟丙烷和一种或多种不饱和化合物的蒸馏不可分离的混合物与CI2的混合物反应以饱和不饱和碳氟化合物转化成反应混合物，和d）分离纯化的1,1,1,3,3,3-六氟丙烷产物，其含有小于1000ppm，最优选小于100ppm的不饱和碳氟化合物。

2. 发明申请

WO2006104742A3 METHANE AND METHYL CHLORIDE AS SELECTIVE REDUCING AGENT IN THE TRANSFORMATION OF HYDROCHLOROFLUOROCARBONS OR CHLOROFLUORCARBONS TO HYDROCHLOROFLUOROCARBONS 审中-公开
标题翻译：甲基和甲基氯化物作为选择性还原剂转化氢氯氟烃或氯氟碳化合物转化为氢氯氟烃
公开(公告)号：WO2006104742A3
公开(公告)日：2006-11-30
申请号：PCT/US2006009998
申请日：2006-03-16
申请人： HONEYWELL INT INC , MUKHOPADHYAY SUDIP , MERKEL DAVID C , HSUEHSUNG TUNG
发明人： MUKHOPADHYAY SUDIP , MERKEL DAVID C , HSUEHSUNG TUNG
IPC分类号： C07C17/23 , C07C19/08
CPC分类号： B01J23/04 , B01J23/02 , B01J37/0201 , C07C17/23 , C07C19/08
摘要： A gas phase reaction process for producing a hydrofluorocarbon from a hydrochlorofluorocarbon or chlorofluorocarbon reactant by contacting, in the presence of a catalyst, the hydrochlorofluorocarbon or chlorofluorocarbon reactant with a reducing agent selected from methane, methyl chloride and mixtures thereof, to produce the hydrofluorocarbon.
摘要翻译：一种用于由氢氯氟烃或氯氟烃反应物生产氢氟烃的气相反应方法，其中在催化剂存在下，将氢氯氟烃或氯氟烃反应物与选自甲烷，氯甲烷及其混合物的还原剂接触，制备氢氟烃。

3. 发明申请

WO2006063241A3 DIRECT ONE-STEP SYNTHESIS FROM CF3-I 审中-公开
标题翻译：直接从CF3-I一步合成
公开(公告)号：WO2006063241A3
公开(公告)日：2006-07-27
申请号：PCT/US2005044638
申请日：2005-12-09
申请人： HONEYWELL INT INC , MUKHOPADHYAY SUDIP , HSUEHSUNG TUNG
发明人： MUKHOPADHYAY SUDIP , HSUEHSUNG TUNG
IPC分类号： C07C17/158 , C07C17/20 , C07C17/361 , C07C19/16
CPC分类号： C07C17/093 , C07C17/158 , C07C17/204 , C07C19/16
摘要： The present invention provides a process for the preparation of trifluoromethyl iodide. The process includes the step of: contacting in a reactor a compound represented by the formula: CF 3 -W and a compound represented by the formula: Z-I wherein W is selected from CF 3 , hydrogen and bromine; Z is selected from hydrogen, iodine and chlorine. The step of contacting is carried out, optionally in the presence of a catalyst and further optionally in the presence of air, at a temperature, pressure and for a length of time sufficient to produce the trifluoromethyl iodide.
摘要翻译：本发明提供了制备三氟甲基碘的方法。该方法包括以下步骤：在反应器中使由式：CF 3 3 -W表示的化合物与由式：Z 1表示的化合物在反应器中接触，其中W选自CF 3，氢和溴; Z选自氢，碘和氯。接触步骤任选在催化剂存在下进一步任选地在空气存在下在温度，压力和足以产生三氟甲基碘的一段时间内进行。

4. 发明申请

WO2006063184A2 DIRECT ONE-STEP SYNTHESIS OF TRIFLUOROMETHYL IODIDE 审中-公开
标题翻译：直接一步合成三氟甲基碘
公开(公告)号：WO2006063184A2
公开(公告)日：2006-06-15
申请号：PCT/US2005044510
申请日：2005-12-07
申请人： HONEYWELL INT INC , MUKHOPADHAY SUDIP , HSUEHSUNG TUNG
发明人： MUKHOPADHAY SUDIP , HSUEHSUNG TUNG
IPC分类号： C07C17/093 , C07C17/361 , C07C19/16
CPC分类号： C07C19/16 , C07C17/093 , C07C17/361
摘要： A catalytic one-step process for the production of CF 3 I by reacting, preferably in the presence of a source of oxygen, a source of iodine with a reactant of the formula: CF 3 R where R is -SH, -S-S-CF 3 , -S-phenyl, or -S-Si-(CH 3 ) 3 . The catalyst may be a metal salt such as salts of Cu, Hg, Pt, Pd, Co, Mn, Rh, Ni, V, TI, Ba, Cs, Ca, K and Ge and mixtures thereof, preferably on a support. such as MgO, BaO and CaO, BaCO 3 , CsNO 3 , Ba (NO 3 ) 2 , activated carbon, basic alumina, and ZrO 2 .
摘要翻译：通过优选在氧源下，碘源与下式反应物反应制备CF 3 I的催化一步法：其中R是-SH，-SS-CF 3，-S-苯基或-S-Si-（CH 3）3， / SUB>。催化剂可以是金属盐，例如Cu，Hg，Pt，Pd，Co，Mn，Rh，Ni，V，TI，Ba，Cs，Ca，K和Ge的盐以及它们的混合物，优选在载体上。如MgO，BaO和CaO，BaCO 3，CsNO 3，Ba（NO 3，SUB 2），活化的碳，碱性氧化铝和ZrO 2。

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