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1. 发明申请

WO2007109458A3 STABLE CONCENTRATED METAL COLLOIDS AND METHODS OF MAKING SAME 审中-公开
标题翻译：稳定的浓缩金属胶体及其制备方法
公开(公告)号：WO2007109458A3
公开(公告)日：2008-06-26
申请号：PCT/US2007063879
申请日：2007-03-13
申请人： HEADWATERS TECH INNOVATION LLC , PARASHER SUKESH , REUTER MICHAEL , ZHANG CHENG , ZHOU BING
发明人： PARASHER SUKESH , REUTER MICHAEL , ZHANG CHENG , ZHOU BING
IPC分类号： B01J23/40 , B01J23/42 , B01J23/44 , C01B15/029
CPC分类号： B01J35/0013 , B01J13/0043 , B01J23/40 , B01J37/18 , B82Y30/00
摘要： Metal-containing colloids are manufactured by reacting a plurality of metal ions and a plurality of organic agent molecules to form metal complexes in a mixture having a pH greater than about 4.25. The metal complexes are reduced for at least 0.5 hour to form stable colloidal nanoparticles. The extended reduction time improves the stability of the colloidal particles as compared to shorter reduction times. The stability of the colloidal particles allows for colloids with higher concentrations of metal to be formed. The concentration of metal in the colloid is preferably at least about 150 ppm by weight.
摘要翻译：含金属胶体通过使多种金属离子和多种有机试剂分子反应，在pH大于约4.25的混合物中形成金属络合物来制造。将金属络合物还原至少0.5小时以形成稳定的胶体纳米颗粒。与较短的还原时间相比，延长的还原时间提高了胶体颗粒的稳定性。胶体颗粒的稳定性允许形成具有较高浓度金属的胶体。胶体中金属的浓度优选为至少约150ppm重量。

2. 发明申请

WO2007109457A2 STABLE CONCENTRATED METAL COLLOIDS AND METHODS OF MAKING SAME 审中-公开
标题翻译：稳定的浓缩金属胶体及其制备方法
公开(公告)号：WO2007109457A2
公开(公告)日：2007-09-27
申请号：PCT/US2007063874
申请日：2007-03-13
申请人： HEADWATERS TECH INNOVATION LLC , PARASHER SUKESH , ZHANG CHENG , RUETER MICHAEL A , ZHOU BING
发明人： PARASHER SUKESH , ZHANG CHENG , RUETER MICHAEL A , ZHOU BING
IPC分类号： B01J31/00 , B01F3/12 , B01F17/00
CPC分类号： B01J23/40 , B01J13/0034 , B01J13/0039 , B01J13/0043 , B01J35/0013 , B22F1/0022 , B22F9/26 , B22F2999/00 , B82Y30/00 , B22F2201/013
摘要： A method for manufacturing stable concentrated colloids containing metal nanoparticles in which the colloid is stabilized by adding a base. This allows the metal particles to be formed in higher concentration without forming larger agglomerates and/or precipitating. The method of manufacturing the stable colloidal metal nanoparticles of the present invention generally includes (i) providing a solution comprising a plurality of metal atoms, (ii) providing a solution comprising a plurality of organic agent molecules, each organic agent molecule comprising at least one functional group capable of bonding to the metal atoms, (iii) reacting the metal atoms in solution with the organic agent molecules in solution to form a mixture comprising a plurality of complexed metal atoms, (iv) reducing the complexed metal atoms in the mixture using a reducing agent to form a plurality of nanoparticles, and (v) adding an amount of a base to the mixture, thereby improving the stability of the nanoparticles in the mixture. The base may be added before or after forming the nanoparticles.
摘要翻译：一种制备含有金属纳米粒子的稳定浓缩胶体的方法，其中胶体通过加入碱稳定。这允许金属颗粒以更高的浓度形成，而不形成较大的附聚物和/或沉淀。制备本发明的稳定胶体金属纳米粒子的方法通常包括（i）提供包含多个金属原子的溶液，（ii）提供包含多个有机试剂分子的溶液，每个有机试剂分子包含至少一个能够与金属原子键合的官能团，（iii）使溶液中的金属原子与溶液中的有机试剂分子反应，形成包含多个络合金属原子的混合物，（iv）使用还原剂形成多个纳米颗粒，和（v）向混合物中加入一定量的碱，从而提高混合物中纳米颗粒的稳定性。可以在形成纳米颗粒之前或之后加入碱。

3. 发明申请

WO2012012292A2 HIGH TEMPERATURE REDUCTION OF HYDROGEN PEROXIDE CATALYST FOR IMPROVED SELECTIVITY 审中-公开
标题翻译：过氧化氢催化剂的高温降低提高了选择性
公开(公告)号：WO2012012292A2
公开(公告)日：2012-01-26
申请号：PCT/US2011044239
申请日：2011-07-15
申请人： HEADWATERS TECH INNOVATION LLC , PARASHER SUKESH , RUETER MICHAEL A , ZHOU BING
发明人： PARASHER SUKESH , RUETER MICHAEL A , ZHOU BING
IPC分类号： B01J23/38 , B01J23/44 , B01J37/02 , C01B15/029
CPC分类号： B01J35/0013 , B01J21/08 , B01J23/40 , B01J23/42 , B01J23/44 , B01J35/002 , B01J35/006 , B01J35/08 , B01J37/0203 , B01J37/16 , B01J37/18 , C01B15/029
摘要： Method for making a direct synthesis hydrogen peroxide catalyst includes (i) mixing together a solvent, a plurality of noble metal catalyst atoms, and a plurality of organic dispersing agent molecules, the organic dispersing agent molecules each including at least one functional group capable of bonding with the noble metal catalyst atoms; (ii) reacting the organic dispersing agent with the catalyst atoms to form complexed catalyst atoms and forming a plurality of catalytic nanoparticles from the complexed catalyst atoms; (iii) supporting the catalytic nanoparticles on a support material; and (iv) reducing the catalyst atoms at a temperature of at least 351 °C to yield a supported and activated direct synthesis hydrogen peroxide catalyst.
摘要翻译：用于制备直接合成过氧化氢催化剂的方法包括（i）将溶剂，多个贵金属催化剂原子和多个有机分散剂分子混合在一起，所述有机分散剂分子各自包含至少一个能够键合的官能团与贵金属催化剂原子; （ii）使有机分散剂与催化剂原子反应以形成络合的催化剂原子并由络合的催化剂原子形成多个催化剂纳米粒子; （iii）将催化纳米粒子负载在载体材料上; 和（iv）在至少351℃的温度下还原催化剂原子以产生负载和活化的直接合成过氧化氢催化剂。

4. 发明申请

WO2006121553A2 METHODS FOR MANUFACTURING SUPPORTED NANOCATALYSTS AND METHODS FOR USING SUPPORTED NANOCATALYSTS 审中-公开
标题翻译：用于制造支持的纳米结构的方法和使用支持的纳米结构的方法
公开(公告)号：WO2006121553A2
公开(公告)日：2006-11-16
申请号：PCT/US2006013227
申请日：2006-04-10
申请人： HEADWATERS NANOKINETIX INC , REYES CLEMENTINE , PARASHER SUKESH , ZHOU BING
发明人： REYES CLEMENTINE , PARASHER SUKESH , ZHOU BING
IPC分类号： B01J21/18 , B01J21/16 , B01J29/04 , B01J31/00
CPC分类号： B01J23/44 , B01J37/0203 , B01J37/0207 , B01J37/0211
摘要： Supported nanocatalysts are manufactured by reacting a functionalized support with a plurality of catalyst atoms in the presence of a solvent. Available functional groups on the support material bind to the catalyst atoms and influence nanoparticle formation and/or nanoparticle anchoring. The functionalized support can be manufactured from a support material and a functionalizing agent that has at least two functional groups for bonding individual functionalizing agent molecules both to the support and to the catalyst atoms. Supported palladium nanocatalysts manufactured using the methods of the present invention are particularly useful for performing Heck and Suzuki carbon-carbon coupling reactions.
摘要翻译：负载的纳米催化剂是通过在溶剂存在下使官能化的载体与多个催化剂原子反应制备的。支持材料上的可用官能团与催化剂原子结合并影响纳米颗粒的形成和/或纳米颗粒的固定。官能化载体可以由支持材料和官能化剂制备，所述官能化试剂具有至少两个官能团，用于将各个官能化剂分子与载体和催化剂原子结合。使用本发明的方法制造的负载钯纳米催化剂特别适用于进行Heck和Suzuki碳 - 碳偶联反应。

5. 发明申请

WO2007001418A2 MULTICOMPONENT NANOPARTICLES FORMED USING A DISPERSING AGENT 审中-公开
标题翻译：用分散剂形成多组分纳米粒子
公开(公告)号：WO2007001418A2
公开(公告)日：2007-01-04
申请号：PCT/US2005037545
申请日：2005-10-19
申请人： HEADWATERS NANOKINETIX INC , ZHOU BING , PARASHER SUKESH , RUETER MICHAEL
发明人： ZHOU BING , PARASHER SUKESH , RUETER MICHAEL
IPC分类号： B01J23/00
CPC分类号： B01J35/0013 , B01J21/18 , B01J23/8906 , B01J23/8933 , B01J23/8946 , B01J35/006 , B01J37/0203 , B01J37/18 , B82Y30/00 , B82Y40/00
摘要： Nanoparticles include a plurality of two or more dissimilar components selected from the group of noble metals, base transition metals, alkali earth metals, and rare earth metals and/or different groups of the periodic table of elements. The two or more dissimilar components are dispersed using a dispersing agent such that the nanoparticles have a substantially uniform distribution of the two or more dissimilar components. The dispersing agents can be poly functional small organic molecules, polymers, or oligomers, or salts of these. The molecules of the dispersing agent bind to the particle atoms to overcome same-component attractions, thereby allowing dissimilar components to form heterogeneous manoparticles. Dissimular components such as iron and platinum can be complexed using the dispersing agent to form sbstantially uniform heterogeneous nanoparticles. The nanoparticles can be used alone or applied to a support. At least a portion of the dispersing agent can be removed by reduction and/or oxidation.
摘要翻译：纳米颗粒包括多种选自贵金属，碱过渡金属，碱土金属和稀土金属和/或元素周期表的不同基团的两种或更多种不同组分。使用分散剂分散两种或更多种不同组分，使得纳米粒子具有两种或更多种不同组分的基本均匀分布。分散剂可以是多官能小有机分子，聚合物或低聚物或这些的盐。分散剂的分子与粒子原子结合以克服相同成分的吸引力，由此允许不相似的组分形成不均匀的人造粒子。可以使用分散剂使异物组分如铁和铂复合以形成基本均匀的非均相纳米粒子。纳米颗粒可以单独使用或应用于支持物。至少一部分分散剂可以通过还原和/或氧化除去。

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