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    • 3. 发明申请
    • HIGH ASPECT RATIO CELLULOSE NANOFILAMENTS AND METHOD FOR THEIR PRODUCTION
    • 高比例纤维素纳米纤维及其生产方法
    • WO2012097446A1
    • 2012-07-26
    • PCT/CA2012/000060
    • 2012-01-19
    • FPINNOVATIONSHUA, XujunLALEG, MakhloufMILES, KeithAMIRI, RezaETTALEB, LahoucineDORRIS, Gilles
    • HUA, XujunLALEG, MakhloufMILES, KeithAMIRI, RezaETTALEB, LahoucineDORRIS, Gilles
    • D21D1/30D01B9/00D21B1/38D21H11/16
    • D21D1/30D21D1/20D21H11/16D21H11/18Y10T428/298
    • A novel method is disclosed to produce on a commercial scale, high aspect ratio cellulose nanofilaments (CNF) from natural lignocellulosic fibers. The method consists of a multi-pass high consistency refining (HCR) of chemical or mechanical fibers using specific combinations of refining intensity and specific energy. The CNF produced by this invention represents a mixture of fine filaments with widths in the submicron and lengths from tens of micrometers to few millimeters. The resultant product is made of a population of free filaments and filaments bound to the fiber core from which they were produced. The proportion of free and bound filaments is governed in large part by total specific energy applied to the pulp in the refiner. These CNF products differ from other cellulose fibrillar materials by their higher aspect ratio and the preserved degree of polymerization (DP) of cellulose. The CNF products made by this invention are excellent additives for the reinforcement of paper, tissue, paperboard and packaging products, plastic composite materials and coating formulations. They display exceptional strengthening power for never-dried paper webs.
    • 公开了一种以商业规模生产来自天然木质纤维素纤维的高纵横比纤维素纳米丝(CNF)的新方法。 该方法由使用精炼强度和比能量的特定组合的化学或机械纤维的多遍高浓度精炼(HCR)组成。 本发明生产的CNF表示亚微米宽度为几十微米至几毫米的细丝的混合物。 所得产物由自由长丝和长丝的群体制成,纤维芯与其生成纤维核。 游离和结合长丝的比例在很大程度上由施加在精炼机中的纸浆的总比能来决定。 这些CNF产品与其它纤维素纤维材料的高宽比和纤维素的保留聚合度(DP)不同。 本发明制备的CNF产品是增强纸张,纸巾,纸板和包装产品,塑料复合材料和涂料配方的优良添加剂。 它们显示出非常干燥的纸幅的强化力。
    • 4. 发明申请
    • METHOD OF TRANSFORMING HIGH CONSISTENCY PULP FIBERS INTO PRE-DISPERSED SEMI-DRY AND DRY FIBROUS MATERIALS
    • 将高浓度纸浆纤维转变成预分散的半干和干燥纤维材料的方法
    • WO2018049522A1
    • 2018-03-22
    • PCT/CA2017/051079
    • 2017-09-14
    • FPINNOVATIONS
    • LALEG, MakhloufETTALEB, LahoucineSTACEY, Michael
    • D21C9/00D21C3/00D21D1/20
    • The present invention is directed to a method of transforming a pulp fibrous into a pre-dispersed semi-dry or dry fibrous material and to the material produced. The method opens, de-entangles and fibrillates the fibrous material of the input pulp. The method mixes the input fibrous with chemicals while evaporating moisture in an updated mechanical disc refiner process. The refiner operates to set three process variables: 1) applied refining specific energy; 2) refiner gap opening and 3) refiner output consistency. Depending on the feed pulp type and consistency, the refiner's output is a pre-dispersed semi-dry fibrous material of 30 to 99% solids with 70 to 100% of separated fibers that depending on chemical treatment are loosely entangled fibrous that disperse in water using common techniques. The pre-dispersed semi-dry output may be further processed inline or by batch process air agitation at velocities sufficient to further separate fibers and loosen fibrous entanglements.
    • 本发明涉及一种将纸浆纤维转变成预分散的半干或干燥的纤维材料并将其转化为所生产的材料的方法。 该方法打开,解缠和原纤化输入纸浆的纤维材料。 该方法将输入纤维与化学品混合,同时在更新的机械圆盘磨浆机过程中蒸发水分。 炼油厂操作以设定三个过程变量:1)应用精炼比能; 2)磨浆机开口和3)磨浆机输出一致性。 取决于进料纸浆类型和稠度,精炼机的输出量是30-99%固体的预分散半干燥纤维材料,其中70-100%分离纤维取决于化学处理是松散缠绕的纤维,其分散在水中 常见的技术。 预分散的半干输出物可以进一步在线处理或通过间歇处理空气搅拌以足以进一步分离纤维和松散纤维缠结的速度进行处理。