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1. 发明申请

WO2011140643A1 CELLULOSE NANOFILAMENTS AND METHOD TO PRODUCE SAME 审中-公开
标题翻译：纤维素纳米纤维及其生产方法
公开(公告)号：WO2011140643A1
公开(公告)日：2011-11-17
申请号：PCT/CA2011/000551
申请日：2011-05-11
申请人： FPINNOVATIONS , HUA, Xujun , LALEG, Makhlouf , OWSTON, Tom
发明人： HUA, Xujun , LALEG, Makhlouf , OWSTON, Tom
IPC分类号： D01F2/00 , D21D5/00 , D21H11/00 , D21H11/08
CPC分类号： D21H21/20 , D21B1/342 , D21H15/00 , D21H17/67 , D21H21/10 , D21H21/18 , Y10T428/298
摘要： Cellulose nanofilaments from cellulose fibers, a method and a device to produce them are disclosed. The nanofilaments are fine filaments with widths in the sub-micron range and lengths up to a couple of millimeters. These nanofilaments are made from natural fibers from wood and other plants. The surface of the nanofilaments can be modified to carry anionic, cationic, polar, hydrophobic or other functional groups. Addition of these nanofilaments to papermaking furnishes substantially improves the wet-web strength and dry sheet strength much better than existing natural and synthetic polymers. The cellulose nanofilaments produced by the present invention are excellent additives for reinforcement of paper and paperboard products and composite materials, and can be used to produce superabsorbent materials.
摘要翻译：公开了纤维素纤维的纤维素纳米丝，制造它们的方法和装置。纳米丝是具有亚微米范围宽度和长达几毫米的细丝。这些纳米丝由木材和其他植物的天然纤维制成。可以将纳米丝的表面改性为携带阴离子，阳离子，极性，疏水性或其它官能团。将这些纳米丝添加到造纸配料中大大提高了湿纸幅强度和干纸张强度，比现有的天然和合成聚合物好得多。本发明生产的纤维素纳米丝是增强纸和纸板产品和复合材料的优良添加剂，可用于生产超吸收材料。

2. 发明申请

WO2012097446A1 HIGH ASPECT RATIO CELLULOSE NANOFILAMENTS AND METHOD FOR THEIR PRODUCTION 审中-公开
标题翻译：高比例纤维素纳米纤维及其生产方法
公开(公告)号：WO2012097446A1
公开(公告)日：2012-07-26
申请号：PCT/CA2012/000060
申请日：2012-01-19
申请人： FPINNOVATIONS , HUA, Xujun , LALEG, Makhlouf , MILES, Keith , AMIRI, Reza , ETTALEB, Lahoucine , DORRIS, Gilles
发明人： HUA, Xujun , LALEG, Makhlouf , MILES, Keith , AMIRI, Reza , ETTALEB, Lahoucine , DORRIS, Gilles
IPC分类号： D21D1/30 , D01B9/00 , D21B1/38 , D21H11/16
CPC分类号： D21D1/30 , D21D1/20 , D21H11/16 , D21H11/18 , Y10T428/298
摘要： A novel method is disclosed to produce on a commercial scale, high aspect ratio cellulose nanofilaments (CNF) from natural lignocellulosic fibers. The method consists of a multi-pass high consistency refining (HCR) of chemical or mechanical fibers using specific combinations of refining intensity and specific energy. The CNF produced by this invention represents a mixture of fine filaments with widths in the submicron and lengths from tens of micrometers to few millimeters. The resultant product is made of a population of free filaments and filaments bound to the fiber core from which they were produced. The proportion of free and bound filaments is governed in large part by total specific energy applied to the pulp in the refiner. These CNF products differ from other cellulose fibrillar materials by their higher aspect ratio and the preserved degree of polymerization (DP) of cellulose. The CNF products made by this invention are excellent additives for the reinforcement of paper, tissue, paperboard and packaging products, plastic composite materials and coating formulations. They display exceptional strengthening power for never-dried paper webs.
摘要翻译：公开了一种以商业规模生产来自天然木质纤维素纤维的高纵横比纤维素纳米丝（CNF）的新方法。该方法由使用精炼强度和比能量的特定组合的化学或机械纤维的多遍高浓度精炼（HCR）组成。本发明生产的CNF表示亚微米宽度为几十微米至几毫米的细丝的混合物。所得产物由自由长丝和长丝的群体制成，纤维芯与其生成纤维核。游离和结合长丝的比例在很大程度上由施加在精炼机中的纸浆的总比能来决定。这些CNF产品与其它纤维素纤维材料的高宽比和纤维素的保留聚合度（DP）不同。本发明制备的CNF产品是增强纸张，纸巾，纸板和包装产品，塑料复合材料和涂料配方的优良添加剂。它们显示出非常干燥的纸幅的强化力。

3. 发明申请

WO2012040830A1 CELLULOSE-REINFORCED HIGH MINERAL CONTENT PRODUCTS AND METHODS OF MAKING THE SAME 审中-公开
标题翻译：纤维素增强的高矿物含量产品及其制备方法
公开(公告)号：WO2012040830A1
公开(公告)日：2012-04-05
申请号：PCT/CA2011/001097
申请日：2011-09-29
申请人： FPINNOVATIONS , LALEG, Makhlouf , HUA, Xujun
发明人： LALEG, Makhlouf , HUA, Xujun
IPC分类号： D21H17/67
CPC分类号： D21H11/18 , D21H15/00 , D21H17/25 , D21H17/63 , D21H17/74
摘要： This invention relates to a novel method to prepare aqueous furnishes useful as feedstock in the manufacture of very high-mineral content products, particularly paper sheets having mineral filler content up to 90% that display the required physical properties for the intended applications. The furnishes comprise fibrillated long fibres/mineral fillers mixed with anionic acrylic binders and co-additives, in presence or absence of cellulose fibrils. The fibrillated long fibres and cellulose fibrils provide high surface area for greater filler fixation and the reinforcement backbone network that ties all of the product components together. The anionic binders allow rapid and strong fixation of filler particles onto the surfaces of fibrils when mixing is conducted at temperatures higher than the glass transition temperature (T g ) of the binder. To the novel aqueous formulation can be added other functional and process additives commonly used in the manufacture of paper and paperboard packaging by single, multilayer and multiply papermaking forming processes. The aqueous formulation can also be used to fabricate shaped items by the known pulp moulding processes. The aqueous formulations provide excellent filler retention and drainage during product fabrication.
摘要翻译：本发明涉及一种制备用于制造非常高矿物质含量产品的含水原料的含水配料的新方法，特别是具有高达90％的矿物填料含量的纸张，其显示出所需应用的所需物理性能。这些配料包括在存在或不存在纤维素原纤维的情况下与阴离子丙烯酸粘合剂和共添加剂混合的原纤化长纤维/矿物填料。原纤化长纤维和纤维素原纤维提供高表面积用于更大的填料固定和将所有产物组分结合在一起的加强骨架网络。阴离子粘合剂允许在高于粘合剂的玻璃化转变温度（Tg）的温度下进行混合时，将填料颗粒快速且牢固地固定在原纤维表面上。对于新型含水制剂，可以通过单一，多层和多次造纸成型工艺添加通常用于制造纸和纸板包装的其它功能和加工添加剂。水性制剂也可用于通过已知的纸浆模制方法制造成型制品。含水配方在产品制造过程中提供优异的填料保留和排水。

4. 发明申请

WO2005082974A1 EPICHLOROHYDRIN BASED POLYMERS CONTAINING PRIMARY AMINO GROUPS AS ADDITIVES IN PAPERMAKING 审中-公开
标题翻译：含有基于丙氨酸的聚合物作为添加剂在原料中含有主要的氨基
公开(公告)号：WO2005082974A1
公开(公告)日：2005-09-09
申请号：PCT/CA2005/000260
申请日：2005-02-23
申请人： PULP AND PAPER RESEARCH INSTITUTE OF CANADA , ANTAL, Miroslav , PIKULIK, Ivan I. , HUA, Xujun
发明人： ANTAL, Miroslav , PIKULIK, Ivan I. , HUA, Xujun
IPC分类号： C08G73/02
CPC分类号： D21H17/56 , C08G73/02 , C08G73/0206 , C08G73/022 , C08G73/024 , C08G73/0286 , D21H17/10 , D21H17/52 , D21H21/10 , D21H23/04
摘要： Processes for preparing water-soluble papermaking polymer additives having a multitude of free amino groups effective to form cationically charged complexes with components of a pulp suspension are described, comprising: reacting ammonia and epichlorohydrin (ECH) with ammonia in excess to yield a starburst polymer with a molecular weight of 3000-10 6 ; reacting ECH and ammonia to produce tris(3-chloro-2-hydroxypropylamine) and reacting this with a diamine to yield a water-soluble branched polymer with a molecular weight of 3000-10 6 ; reacting polyepichlorohydrin with a variety of amines, a polyol or ammonia to yield linear polymers, cross-linked polymers and polyamines. The additives are used as agents for improving retention, drainage, product strength and paper machine operation in paper manufacture. Under neutral or acidic conditions these primary amino groups become cationic, which assures good adsorption of the polymer onto anionic fibres and fines used for production of paper or paperboard. By adsorbing on several fibres or fines, the polymer can increase the retention of fines and fillers. Primary amino groups of these polymers can also form chemical bonds with carbonyl groups of cellulose, lignin and hemicellulose, which are especially abundant in the fibres and fines of mechanical pulps. The cross-linking of fibres and fines by chemical bonds can increase the initial strength of wet web and the strength of rewetted paper.
摘要翻译：描述了制备具有多种游离氨基的水溶性造纸聚合物添加剂的方法，所述添加剂具有与纸浆悬浮液的组分有效形成阳离子带电荷的络合物，其包括：使氨和表氯醇（ECH）与氨过量反应，得到星爆聚合物，分子量为3000-10-6; 使ECH和氨反应生成三（3-氯-2-羟丙基胺），并与二胺反应得到分子量为3000-106的水溶性支链聚合物; 使聚表氯醇与多种胺，多元醇或氨反应，得到线性聚合物，交联聚合物和多胺。添加剂用作纸张制造中保留，排水，产品强度和造纸机操作的改进剂。在中性或酸性条件下，这些伯氨基变成阳离子，这确保了聚合物对用于生产纸或纸板的阴离子纤维和细粒的良好吸附。通过吸附在几根纤维或细粉上，聚合物可以增加细粒和填料的保留。这些聚合物的伯氨基也可与纤维素，木质素和半纤维素的羰基形成化学键，其在机械纸浆的纤维和细粉中特别丰富。通过化学键交联纤维和细粉可以增加湿网的初始强度和再润湿纸的强度。

5. 发明申请

WO2018049517A1 METHOD FOR PRODUCING CELLULOSE FILAMENTS WITH LESS REFINING ENERGY 审中-公开
标题翻译：生产炼油能力较低的纤维素纤维的方法
公开(公告)号：WO2018049517A1
公开(公告)日：2018-03-22
申请号：PCT/CA2017/051073
申请日：2017-09-13
申请人： FPINNOVATIONS
发明人： HUA, Xujun , NJAMEN TCHAPDA, Guy Roger , OWSTON, Tom , NEAULT, Patrick , HU, Thomas , BEN, Yuxia
IPC分类号： D21D1/00 , D21C3/00 , D21C9/00
摘要： A novel method is disclosed to make cellulose filaments (CF) from wood or other plant fibers with lower energy consumption. The method consists of multi-stage, high consistency refining, followed by low consistency refining or by low consistency, non-refining mechanical treatment, of wood or other plant fibers. The total specific refining energy for the multi-stage, high consistency refining is preferably 2, 000 - 18,000 kWh/t, and more preferably 2,000 - 12,000 kWh/t. The CF produced can be used as a superior reinforcement additive in the production of paper, tissue or paperboard and in the production of plastic composites. It can also be used as a viscosity or rheology modifier in food products, coatings or drilling muds. The CF produced can also be used to make strong films for application in packaging and in composites.
摘要翻译：公开了一种新型方法，用于以较低的能量消耗从木材或其他植物纤维制造纤维素长丝（CF）。该方法由多阶段，高浓度精炼，其次是低浓度精炼或低浓度，非精炼机械处理的木材或其他植物纤维组成。用于多级高浓度精炼的总特定精制能量优选为2,000-18,000kWh / t，并且更优选2,000-12,000kWh / t。所生产的CF可用作生产纸张，薄纸或纸板以及生产塑料复合材料的优质增强添加剂。它也可以用作食品，涂料或钻井泥浆中的粘度或流变改性剂。所生产的CF也可用于制造强力薄膜，以用于包装和复合材料。

6. 发明申请

WO2018209444A1 CELLULOSE FILAMENTS REINFORCED CEMENT COMPOSITE BOARD AND METHOD FOR THE MANUFACTURE OF THE SAME 审中-公开
公开(公告)号：WO2018209444A1
公开(公告)日：2018-11-22
申请号：PCT/CA2018/050586
申请日：2018-05-18
申请人： FPINNOVATIONS
发明人： CAI, Xiaolin , BEN, Yuxia , HUA, Xujun , RICARD, Michelle , LAROUCHE, Carole , WANG, Xiang-ming
IPC分类号： C04B16/02 , B28B1/52 , C04B16/06
摘要： Cement composite boards comprising cellulose filaments (CF) and/or CF-containing pulp, are described. The composite boards have at least an improved modulus of rupture when compared with similar board that are free of CF. Methods for producing the CF and/or CF-containing pulp reinforced cement boards are also described. The CF cement composite board comprises: cellulose filaments (CF) and/or CF-containing pulp, and cement, wherein the CF has an aspect ratio of 200 to 5000, comprising a weight% of CF is from 1% to 20% by weight of the composite board. The composite boards herein described may have a modulus of rupture of more than 7 MPa.

7. 发明申请

WO2016176759A1 A DRY MIXED RE-DISPERSIBLE CELLULOSE FILAMENT/CARRIER PRODUCT AND THE METHOD OF MAKING THE SAME 审中-公开
标题翻译：干燥混合的可重复使用的纤维素纤维素/载体产品及其制备方法
公开(公告)号：WO2016176759A1
公开(公告)日：2016-11-10
申请号：PCT/CA2016/050475
申请日：2016-04-25
申请人： FPINNOVATIONS
发明人： BEN, Yuxia , DORRIS, Gilles , CAI, Xiaolin , HUA, Xujun , YUAN, Zhirun , NEAULT, Patrick
IPC分类号： C08J3/05 , C08J3/20 , C08L1/02 , D21C5/02 , D21C9/00 , D21H27/00
CPC分类号： D21C9/18 , D21H11/02 , D21H11/08 , D21H11/10 , D21H15/06 , D21H27/02 , D21H27/10
摘要： The present description relates to a process of producing a dry mixed product comprising cellulose filament (CF) and a carrier fibre, and a dry mixed product of re-dispersible cellulose filament and a carrier fibre that permits the CF to retain its dispersibility in water and hence superior reinforcement ability in papermaking furnishes, composite materials, or other materials where CF is used. The process comprises mixing a water suspension of never-dried CF with a cellulose fibre pulp carrier followed by thickening to a suitable concentration so that it can be further processed and dried in a conventional device such as a dryer can of a pulp machine or a flash dryer.
摘要翻译：本说明书涉及一种生产包含纤维素长丝（CF）和载体纤维的干混物的方法，以及可再分散纤维素丝和载体纤维的干混物，其允许CF保持其在水中的分散性，因此在造纸配料，复合材料或其他使用CF的材料中具有优异的增强能力。该方法包括将未干燥的CF的水悬浮液与纤维素纤维纸浆载体混合，随后增稠至合适的浓度，使得其可以在常规装置例如纸浆机或闪蒸器的干燥罐中进一步加工和干燥机。

8. 发明申请

WO2017088063A1 STRUCTURALLY ENHANCED AGRICULTURAL MATERIAL SHEETS AND THE METHOD OF PRODUCING THE SAME 审中-公开
标题翻译：结构增强的农用材料片材及其制造方法
公开(公告)号：WO2017088063A1
公开(公告)日：2017-06-01
申请号：PCT/CA2016/051393
申请日：2016-11-25
申请人： FPINNOVATIONS
发明人： BEN, Yuxia , HUA, Xujun , RICARD, Michelle , WANG, Xiaoyu
IPC分类号： A23P30/00 , A24C5/56 , D21H11/12
CPC分类号： A24B15/14 , A23L7/198 , A23L17/60 , A24B13/00 , A24B15/12 , D21H11/12 , D21H17/01
摘要： The present invention relates to a structurally enhanced agricultural product containing cellulose filaments (CF), and a method for producing the structurally enhanced agricultural material into the sheets. Applying CF improves significantly the wet-web strength of the agricultural material sheets. The method comprises preparation of a pulp slurry of agricultural materials followed by mixing with a water suspension of CF or CF-containing cellulose fibers. The pulp blend is then used to produce an agricultural material sheet by papermaking process.
摘要翻译：本发明涉及包含纤维素长丝（CF）的结构增强的农产品，以及用于将结构增强的农业材料制造成薄片的方法。施用CF可以显着改善农用薄片的湿纸幅强度。该方法包括制备农业用材料的纸浆浆料，然后与含有CF或CF的纤维素纤维的水悬浮液混合。纸浆混合物然后用于通过造纸工艺生产农业材料片。

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