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    • 2. 发明申请
    • ENCAPSULATION
    • 包胶
    • WO2017074995A1
    • 2017-05-04
    • PCT/US2016/058771
    • 2016-10-26
    • ENCAPSYS, LLC
    • ZHANG, HanweiSCHWANTES, Todd, ArlinHOBART, Katie, AnnWILLIAMSON, Diane, Jean
    • B01J13/16A61K8/11
    • B01J13/18A01N25/28A61K8/11A61K8/8152A61K8/88A61K9/50A61K9/5026A61K9/5031A61K9/5089A61K2800/412A61Q13/00A61Q15/00A61Q17/04B01J13/14C09B67/0097C10M171/06C10N2220/08C10N2250/16C11D3/505F28D20/023
    • An improved process of making a benefit agent delivery particle and an improved microcapsule made by such process are disclosed. The process comprises the steps of providing a first composition of water phase (1), water phase (2) and water phase (3). Water phase (1) comprises water and an initiator; water phase (2) comprises water, a water-soluble or dispersible amine(meth)acrylate or hydroxyl(meth)acrylate and a multifunctional (meth)acrylate. Water phase (3) comprises water, and carboxyalkyl(meth)acrylate and a base or quarternary ammonium acrylate. The first two water phases are combined to prereact the hydroxy- or amine(meth)acrylate and the multifunctional (meth)acrylate to form a multifunctional hydroxyl- amine(meth)acrylate pre-polymer. The pre-polymer is combined with water phase (3); then an emulsion is formed by emulsifying under high shear agitation a second composition into said first composition; said second composition comprising an oil phase comprising an isocyanate and a benefit agent core material thereby forming a wall surrounding the benefit agent core material.
    • 公开了一种改进的制备有益剂递送颗粒的方法和通过该方法制备的改进的微胶囊。 该方法包括提供水相(1),水相(2)和水相(3)的第一组合物的步骤。 水相(1)包含水和引发剂; 水相(2)包含水,水溶性或分散性胺(甲基)丙烯酸酯或羟基(甲基)丙烯酸酯和多官能(甲基)丙烯酸酯。 水相(3)包含水和(甲基)丙烯酸羧烷基酯以及碱或季铵丙烯酸盐。 将前两个水相合并以预反应羟基 - 或胺(甲基)丙烯酸酯和多官能(甲基)丙烯酸酯以形成多官能羟基 - 胺(甲基)丙烯酸酯预聚物。 预聚物与水相(3)结合; 然后通过在高剪切搅拌下将第二组合物乳化到所述第一组合物中形成乳液; 所述第二组合物包含含有异氰酸酯和有益剂核心物质的油相,由此形成围​​绕有益物质核心物质的壁。