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1. 发明申请

WO2007037892A3 RANDOM COPOLYMERS OF ETHYLENE AND 4-VINYLPHENYL ESTERS AND METHOD FOR PREPARING THE SAME 审中-公开
公开(公告)号：WO2007037892A3
公开(公告)日：2007-04-05
申请号：PCT/US2006/033717
申请日：2006-08-29
申请人： E. I. DU PONT DE NEMOURS AND COMPANY , SHEEHAN, Michael, Thomas , WAGMAN, Mark, E.
发明人： SHEEHAN, Michael, Thomas , WAGMAN, Mark, E.
IPC分类号： C08F18/08 , C08F20/18 , C08F16/18 , C08F20/06 , C08F120/06 , C08F120/14
摘要： The invention discloses a composition consisting essentially of an E/X/M random copolymer wherein X is from 0.1 to 20 mol % of the E/X/M copolymer and is a 4-vinylphenyl ester, preferably 4-acetoxystyrene; M is from 0 to 40 mol % of the E/X/M copolymer and is one or more ethylenically unsaturated monomers; and E is ethylene. The invention further encompasses a high pressure radical polymerization process for providing the novel polymers; and a base catalyzed transesterification process for conversion of the E/X/M copolymer to an E/Y/M copolymer wherein Y is derived from 4-hydroxystyrene. Another embodiment of the invention is a composition consisting essentially of an E/Y/M random copolymer wherein Y is greater than 1.0 to about 20 mol % of the E/Y/M copolymer and is 4-hydroxystyrene; M is from 0 to 40 mol % of the E/Y/M copolymer and is one or more ethylenically unsaturated monomers; and E is ethylene.

2. 发明申请

WO2008085513A1 A METHOD FOR PREPARING GLYCIDYLOXYSTYRENE MONOMERS AND POLYMERS THEREOF 审中-公开
标题翻译：制备甘氨酰基苯乙烯单体及其聚合物的方法
公开(公告)号：WO2008085513A1
公开(公告)日：2008-07-17
申请号：PCT/US2007/026517
申请日：2007-12-28
申请人： E. I. DU PONT DE NEMOURS AND COMPANY , KUNITSKY, Keith , SHAH, Mukesh, C. , SHUEY, Steven, W. , WAGMAN, Mark, E.
发明人： KUNITSKY, Keith , SHAH, Mukesh, C. , SHUEY, Steven, W. , WAGMAN, Mark, E.
IPC分类号： C08F12/22 , C08L25/18 , C07D303/23
CPC分类号： C08F12/22 , C07D303/23
摘要： It was found that glycidyloxystyrenes, including glycidyloxystyrene and substituted glycidyloxystyrene, can be synthesized from hydroxycinnamic acid or substituted hydroxycinnamic acids in a one-pot, two-step process. The substrate can be thermally decarboxylated and then without purification, reacted in the presence of a halomethyl-oxirane and a base. The resulting product can be polymerized or coppolymerized to a fully substituted product.
摘要翻译：发现缩水甘油氧基苯乙烯，包括缩水甘油氧基苯乙烯和取代的缩水甘油氧基苯乙烯，可以一锅二步法从羟基肉桂酸或取代的羟基肉桂酸合成。底物可以热脱羧，然后不经纯化，在卤代甲基 - 环氧乙烷和碱的存在下反应。所得产物可以被聚合或共聚合成完全取代的产物。

3. 发明申请

WO2010118285A1 METHOD OF DISSOLVING AN OXIDIZED POLYSACCHARIDE IN AN AQUEOUS SOLUTION 审中-公开
标题翻译：在水溶液中溶解氧化多糖的方法
公开(公告)号：WO2010118285A1
公开(公告)日：2010-10-14
申请号：PCT/US2010/030476
申请日：2010-04-09
申请人： E. I. du Pont de Nemours and Company , WAGMAN, Mark, E.
发明人： WAGMAN, Mark, E.
IPC分类号： A61K31/765 , A61L24/08 , C08L5/00 , A61L15/58
CPC分类号： A61L24/08 , C08L1/04 , C08L3/10 , C08L5/00 , C08L5/02 , C08L5/08 , C08L71/02 , C08L2666/22 , C08L2666/02
摘要： A method of dissolving an oxidized polysaccharide in an aqueous solution using an oligomer additive is described. The resulting aqueous solution of the oxidized polysaccharide may be used in combination with an aqueous solution comprising an amine-containing component to prepare hydrogel tissue adhesives and sealants for medical and veterinary applications, such as wound closure, supplementing or replacing sutures or staples in internal surgical procedures such as intestinal anastomosis and vascular anastomosis, tissue repair, ophthalmic procedures, drug delivery, and to prevent post-surgical adhesions.
摘要翻译：描述了使用低聚物添加剂将氧化多糖溶解在水溶液中的方法。所得到的氧化多糖水溶液可与包含含胺组分的水溶液组合使用以制备用于医疗和兽医应用的水凝胶组织粘合剂和密封剂，例如伤口闭合，补充或更换内部手术中的缝线或缝钉手术如肠吻合和血管吻合术，组织修复，眼科手术，药物递送，并防止手术后粘连。

4. 发明申请

WO2010118284A1 HYDROGEL TISSUE ADHESIVE HAVING REDUCED DEGRADATION TIME 审中-公开
标题翻译：具有降低降解时间的HYDROGEL TISSUE粘合剂
公开(公告)号：WO2010118284A1
公开(公告)日：2010-10-14
申请号：PCT/US2010/030474
申请日：2010-04-09
申请人： E. I. DU PONT DE NEMOURS AND COMPANY , WAGMAN, Mark, E.
发明人： WAGMAN, Mark, E.
IPC分类号： A61L24/00 , A61L24/04 , C08B37/00 , C08L1/02 , C08L3/10 , C08L5/02 , C08L5/08 , C08L5/12 , C09J101/00 , C09J105/00 , C09J105/02 , C08L3/20
CPC分类号： A61L24/0031 , A61L24/0042 , A61L24/043 , A61L31/041 , A61L31/145 , A61L31/148 , C08L1/04 , C08L3/10 , C08L5/02 , C08L5/08 , C08L5/12 , C08L71/02
摘要： A hydrogel tissue adhesive having decreased degradation time is described. The hydrogel tissue adhesive is formed by reacting an oxidized polysaccharide with a water-dispersible, multi-arm polyether amine in the presence of an oligomer additive, which promotes the degradation of the hydrogel. The hydrogel may be useful as a tissue adhesive or sealant for medical applications, such as a hemostat sealant or to prevent undesired tissue-to-tissue adhesions resulting from trauma or surgery.
摘要翻译：描述了具有降低的降解时间的水凝胶组织粘合剂。水凝胶组织粘合剂通过使氧化多糖与水分散性多臂聚醚胺在低聚物添加剂的存在下反应形成，其促进水凝胶的降解。水凝胶可用作用于医疗应用的组织粘合剂或密封剂，例如止血剂密封剂或用于防止由创伤或手术引起的不希望的组织与组织粘连。

5. 发明申请

WO2014138499A1 A PRINTING FORM AND A PROCESS FOR PREPARING A PRINTING FORM USING TWO-STEP CURE 审中-公开
标题翻译：一种印刷形式和一种使用两步固化印刷印版的方法
公开(公告)号：WO2014138499A1
公开(公告)日：2014-09-12
申请号：PCT/US2014/021442
申请日：2014-03-06
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： LU, Helen, S.M. , WAGMAN, Mark, E.
IPC分类号： B41C1/02 , B41N1/12 , B41N1/22 , B41C1/045 , B41C1/05 , B41C1/18 , B41M1/10
CPC分类号： B41C1/05 , B05D3/0254 , B23K26/40 , B23K2201/35 , B29C59/002 , B41C1/045 , B41C1/18 , B41M1/10 , B41N1/12 , B41N1/22
摘要： The invention pertains to a printing form and a process for preparing the printing form from a curable composition that includes an epoxy resin, less than a stoichiometric amount of at least one amine curing agent, and optionally a catalytic curing agent and/or a latent curing agent. The process includes applying the curable composition to a supporting substrate to form a layer, partially curing the layer at a first temperature, engraving the partially cured layer, and then completing the curing by heating at a second temperature greater than the first temperature. The less than stoichiometric amount of the amine curing agent guarantees that after the first curing step, epoxy functionalities in the curable composition will be available for second curing step. The optional catalytic curing agent or latent curing agent promotes completion of the cure at higher temperature. The process prepares printing forms, particularly gravure printing forms, having a cured resin composition layer that is engravable, resistant to solvent inks and to mechanical wear, and capable of printing gravure-quality images.
摘要翻译：本发明涉及一种由可固化组合物制备印刷形式的印刷形式和方法，所述可固化组合物包括环氧树脂，小于化学计量的至少一种胺固化剂，以及任选的催化固化剂和/或潜在固化剂剂。该方法包括将可固化组合物施加到支撑基底上以形成层，在第一温度下部分固化该层，雕刻部分固化层，然后通过在大于第一温度的第二温度加热来完成固化。胺固化剂的化学计量不足以确保在第一固化步骤之后，可固化组合物中的环氧官能度可用于第二固化步骤。任选的催化固化剂或潜在性固化剂有助于在较高温度下完成固化。该方法制备具有可雕刻，耐溶剂油墨和机械磨损的固化树脂组合物层并且能够印刷凹版印刷图像的印刷形式，特别是凹版印刷形式。

6. 发明申请

WO2014074431A1 A PRINTING FORM AND A PROCESS FOR PREPARING A PRINTING FORM 审中-公开
标题翻译：一种印刷形式和一种制备印刷形式的方法
公开(公告)号：WO2014074431A1
公开(公告)日：2014-05-15
申请号：PCT/US2013/068221
申请日：2013-11-04
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： WAGMAN, Mark, E. , LU, Helen, S., M.
IPC分类号： B41N1/12 , B41N1/22
CPC分类号： B41N1/12 , B41C1/045 , B41C1/05 , B41N1/22
摘要： The invention pertains to a printing form and a process for preparing it from a curable composition that includes an epoxy resin and an amine curing agent selected from primary amines and secondary amines. The process includes applying the curable composition to a supporting substrate to form a layer, curing the layer, and engraving to form at least one cell in the cured layer. Preheating the substrate to a surface temperature greater than 40C and less than about 80C results in improved surface characteristics of the printing for, such as reduction of amine blush, elimination of bubbles, and lessened surface roughness, while not accelerating the curing rate or evaporation of volatile components to an undesirable degree. The process prepares printing forms, particularly gravure printing forms, having a cured resin composition layer that is engravable, resistant to solvent inks and to mechanical wear, and capable of printing gravure-quality images.
摘要翻译：本发明涉及一种印刷形式及其制备方法，该可固化组合物包括环氧树脂和选自伯胺和仲胺的胺固化剂。该方法包括将可固化组合物施加到支撑基底上以形成层，固化层和雕刻以在固化层中形成至少一个电池。将基材预热至大于40℃且小于约80℃的表面温度导致改善的印刷表面特性，例如减少胺腮红，消除气泡和减少表面粗糙度，同时不加速固化速率或蒸发挥发性组分到不期望的程度。该方法制备具有可雕刻，耐溶剂油墨和机械磨损的固化树脂组合物层并且能够印刷凹版印刷图像的印刷形式，特别是凹版印刷形式。

7. 发明申请

WO2005118717A2 A METHOD FOR MAKING POLYOLEFIN GRAFT POLYMERS HAVING IMPROVED ADHESION PROPERTIES 审中-公开
标题翻译：制备具有改进粘合性能的聚烯烃聚合物的方法
公开(公告)号：WO2005118717A2
公开(公告)日：2005-12-15
申请号：PCT/US2005/018888
申请日：2005-05-25
申请人： E.I. DUPONT DE NEMOURS AND COMPANY , WAGMAN, Mark, E. , MORRIS, Barry, Alan
发明人： WAGMAN, Mark, E. , MORRIS, Barry, Alan
IPC分类号： C08L51/00
CPC分类号： C08F255/00 , C08F255/02 , C08F212/14 , C08F220/40
摘要： A solution grafting method for making polyolefin graft polymers by grafting a phenolic ester monomeric compound on olefinic polymers in the presence of a radical initiator in an organic solvent is described. The grafted polymers provide improved adhesion properties, particularly to metal and polyester substrates.
摘要翻译：描述了通过在自由基引发剂存在下在有机溶剂中将酚酯单体化合物接枝到烯烃聚合物上来制备聚烯烃接枝聚合物的溶液接枝方法。接枝聚合物提供改善的粘合性能，特别是金属和聚酯基材。

8. 发明申请

WO2005079537A2 A METHOD FOR PREPARING PARA-(2-HYDROXYALKYLOXY) STYRENE MONOMERS AND OLIGOMERS 审中-公开
标题翻译：制备PARA-（2-羟基喹啉）苯乙烯单体和低聚物的方法
公开(公告)号：WO2005079537A2
公开(公告)日：2005-09-01
申请号：PCT/US2005/005548
申请日：2005-02-17
申请人： E.I. DUPONT DE NEMOURS AND COMPANY , ARTHUR, Samuel, David , KUNITSKY, Keith , TROST, Barry, M. , WAGMAN, Mark, E.
发明人： ARTHUR, Samuel, David , KUNITSKY, Keith , TROST, Barry, M. , WAGMAN, Mark, E.
IPC分类号： C07C41/00 , C07C41/03 , C07C43/23
CPC分类号： C07C41/03 , C08F12/22 , C07C43/23
摘要： A method for preparing p-(2-hydroxyalkyloxy)styrene monomers and oligomers is described. The method comprises a base-catalyzed reaction of a styrene ester, a suitable alcohol and an alkylene oxide in a single vessel reaction. In this method, the reactive p-hydroxystyrene is generated in situ via the base-catalyzed transesterification reaction between the styrene ester and the alcohol in the presence of the base catalyst. The p-hydroxystyrene formed reacts with the alkylene oxide to form the p-(2-hydroxyalkyloxy)styrene monomer or oligomer.
摘要翻译：描述了制备对 - （2-羟基烷氧基）苯乙烯单体和低聚物的方法。该方法包括在单容器反应中苯乙烯酯，合适的醇和烯化氧的碱催化反应。在该方法中，在碱催化剂存在下，通过苯乙烯酯与醇之间的碱催化酯交换反应原位生成反应性对羟基苯乙烯。所形成的对羟基苯乙烯与烯化氧反应形成对 - （2-羟基烷氧基）苯乙烯单体或低聚物。

9. 发明申请

WO2008016496A2 METHODS FOR PREPARING POLYMERS FROM PHENOLIC MATERIALS AND COMPOSITIONS RELATING THERETO 审中-公开
标题翻译：从苯酚材料和组合物制备聚合物的方法
公开(公告)号：WO2008016496A2
公开(公告)日：2008-02-07
申请号：PCT/US2007/016505
申请日：2007-07-21
申请人： DUPONT ELECTRONIC POLYMERS L.P. , KUNITSKY, Keith, J. , SHEEHAN, Michael, T. , SOUNIK, James, R. , WAGMAN, Mark, E.
发明人： KUNITSKY, Keith, J. , SHEEHAN, Michael, T. , SOUNIK, James, R. , WAGMAN, Mark, E.
CPC分类号： C07C37/74 , C07C37/50 , C07C41/18 , C08F112/14 , C08F212/08 , C08F212/14 , C07C39/20 , C07C43/23
摘要： A process for producing a stable polymer such as poly(hydroxystyrene) which comprises the decarboxylation of a corresponding phenolic in the presence of a non-amine basic catalyst and a polar organic solvent, followed by the polymerization thereof.
摘要翻译：一种稳定的聚合物如聚（羟基苯乙烯）的制备方法，其包括在非胺碱性催化剂和极性有机溶剂的存在下相应的酚的脱羧，然后进行聚合。

10. 发明申请

WO2005097719A1 A METHOD FOR PREPARING HYDROXYSTYRENES AND ACETYLATED DERIVATIVES THEREOF 审中-公开
标题翻译：制备羟基苯乙烯和乙酰化衍生物的方法
公开(公告)号：WO2005097719A1
公开(公告)日：2005-10-20
申请号：PCT/US2005/009290
申请日：2005-03-21
申请人： E.I. DUPONT DE NEMOURS AND COMPANY , KUNITSKY, Keith , SHAH, Mukesh, C. , SHUEY, Steven, W. , TROST, Barry, M. , WAGMAN, Mark, E.
发明人： KUNITSKY, Keith , SHAH, Mukesh, C. , SHUEY, Steven, W. , TROST, Barry, M. , WAGMAN, Mark, E.
IPC分类号： C07C37/00
CPC分类号： C07C67/08 , C07C37/50 , C07C41/18 , C07C69/017 , C07C69/157 , C07C69/16 , C07C39/20 , C07C43/23
摘要： A method is provided for the thermal decarboxylation of a phenolic substrate in the presence of a non-amine basic catalyst to produce a vinyl monomer. The product of the decarboxylation reaction may additionally be acetylated in the presence of an acetylating agent in the same reaction vessel.
摘要翻译：在非胺碱性催化剂的存在下，提供酚底物的热脱羧以产生乙烯基单体的方法。在同一反应容器中，乙酰化剂的存在下，脱羧反应的产物可另外进行乙酰化。

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