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1. 发明申请

WO2005021605A1 PROCESS FOR THE PREPARATION OF A FUNCTIONALIZED POLYMER, INTERMEDIATE PRODUCTS, PROCESSES FOR THE PREPARATION THEREOF, A FUNCTIONALIZED POLYMER AND POLYMER COMPOSITION CONTAINING A FUNCTIONALIZED POLYMER AND SHAPED PARTS 审中-公开
标题翻译：功能性聚合物的制备方法，中间产品，其制备方法，功能性聚合物和含有官能化聚合物和成型部件的聚合物组合物
公开(公告)号：WO2005021605A1
公开(公告)日：2005-03-10
申请号：PCT/NL2004/000536
申请日：2004-07-26
申请人： DSM IP ASSETS B.V. , LOONTJENS, Jacobus, Antonius , SCHOLTENS, Boudewijn, Jan, Robert
发明人： LOONTJENS, Jacobus, Antonius , SCHOLTENS, Boudewijn, Jan, Robert
IPC分类号： C08F8/30
CPC分类号： C08G69/48 , C07D265/08 , C08F8/30 , C08G63/91
摘要： Process for the preparation of a functionalized polymer containing an additive, in which process there is first formed a compound that contains, besides at least one oxazine ring, a free amino or hydroxy group; this compound is linked to an additive via the free amino or hydroxy group in the additive; this additive linked to the compound mentioned is contacted with a polymer that contains at least one free carboxylic group, at a temperature above the polymer's melting point and at least above 150 °C, such that the oxazine ring reacts with the free carboxylic group of the polymer to form the functionalized polymer. The invention also relates to the intermediate products formed in the process and in the preparation thereof. Lastly, the invention relates to functionalized polymers and polymer compositions containing the functionalized polymer.
摘要翻译：制备含有添加剂的官能化聚合物的方法，其中首先形成除了至少一个恶嗪环以外含有游离氨基或羟基的化合物; 该化合物通过添加剂中的游离氨基或羟基与添加剂连接; 与所述化合物连接的该添加剂在高于聚合物熔点和至少高于150℃的温度下与含有至少一个游离羧基的聚合物接触，使得恶嗪环与游离羧基的游离羧基反应聚合物形成官能化聚合物。本发明还涉及在该方法和其制备过程中形成的中间产物。最后，本发明涉及含官能化聚合物的官能化聚合物和聚合物组合物。

2. 发明申请

WO2005068532A1 PROCESS FOR PREPARING A HIGH MOLECULAR POLYCONDENSATE 审中-公开
标题翻译：制备高分子量聚碳酸酯的方法
公开(公告)号：WO2005068532A1
公开(公告)日：2005-07-28
申请号：PCT/EP2004/014886
申请日：2004-12-29
申请人： DSM IP ASSETS B.V. , LOONTJENS, Jacobus, Antonius , SCHOLTENS, Boudewijn, Jan, Robert
发明人： LOONTJENS, Jacobus, Antonius , SCHOLTENS, Boudewijn, Jan, Robert
IPC分类号： C08G63/91
CPC分类号： C08G69/04 , C08G63/91 , C08G64/42 , C08G69/28 , C08G69/44 , C08G69/48
摘要： The invention relates to a process for preparing a high-molecular polycondensate, i.e. a polyester, a polyamide, a polyester-amide, a polycarbonate, a polyether or a block copolymer by melt-mixing a polyester, a polyamide, a polycarbonate, a polyether or a mixture of at least two of these said polycondensates with a carbonyl bislactam according to formula (I) in which formula n is an integer of between 3 and 15, and a diepoxide. Preferably said diepoxide is a compound containing epoxy radicals of formula (II), which radicals are linked direct to carbon, oxygen, nitrogen or sulfur atoms, wherein R 1 and R 3 are both hydrogen, R 2 is hydrogen or methyl, and m=0, or wherein R 1 and R 3 , taken together, are - CH 2 -CH 2 - or -CH 2 -CH 2 -CH 2 -, in which case R 2 is hydrogen and m=0 or 1. The present invention results in a more stable process for the production of a polycondensate with a high molecular mass. Furthermore the polycondensate obtained with the process according to the invention has, even under extreme process conditions such as high temperature, less discoloration. With the process according to the invention a permanent increase in the molecular weight of a polycondensate is obtained in an even faster way than with processes according to the state of the art.
摘要翻译：本发明涉及通过熔融混合聚酯，聚酰胺，聚碳酸酯，聚醚等制备高分子缩聚物，即聚酯，聚酰胺，聚酯 - 酰胺，聚碳酸酯，聚醚或嵌段共聚物的方法或这些所述缩聚物中的至少两种与根据式（I）的羰基双内酰胺的混合物，其中式n为3至15的整数，和二环氧化物。优选地，所述二环氧化物是含有式（II）的环氧基的化合物，其基团直接连接到碳，氧，氮或硫原子上，其中R 1和R 3都是氢，R 2是氢或甲基，m = 0，或其中R 1和R 3一起是-CH 2 -CH 2 - 或-CH 2 -CH 2 -CH 2 - ，在这种情况下，R 2是氢并且m = 0或1.本发明导致更稳定的具有高分子量的缩聚物。此外，通过本发明的方法获得的缩聚物即使在极端的工艺条件下，例如高温，较少变色。通过根据本发明的方法，以比根据现有技术的方法更快的方式获得缩聚物的分子量的永久增加。

3. 发明申请

WO2003035767A1 NEW POLYMER COMPOSITIONS, THE PREPARATION AND USE THEREOF AS WELL AS SHAPED PARTS AND THE PREPARATION THEREOF 审中-公开
标题翻译：新型聚合物组合物，其制备和使用以及形成的部件及其制备方法
公开(公告)号：WO2003035767A1
公开(公告)日：2003-05-01
申请号：PCT/NL2002/000681
申请日：2002-10-25
申请人： DSM N.V. , LOONTJENS, Jacobus, Antonius , SCHOLTENS, Boudewijn, Jan, Robert
发明人： LOONTJENS, Jacobus, Antonius , SCHOLTENS, Boudewijn, Jan, Robert
IPC分类号： C08L101/02
CPC分类号： C08G81/00 , C08L101/02
摘要： The invention relates to a polymer composition as well as to a process for the preparation of such a composition wherein two or more essentially incompatible polymers, each containing functional hydroxy groups and/or functional amino groups, are in contact with each other in the presence of at least one compatibilizer, the compatibilizer being a carbonyl bislactam (CBL) having the structure according to formula (I), where n is an integer from 3 to 15 and preferably 5. Preferably, the compatibilizer is carbonyl biscaprolactam. Depending on the ratio of the number of functional -OH or -NH 2 groups to the CBL, the composition can be used as a polymer dispersion, for instance for improvement of the impact resistance or of the VICAT, or as a copolymer. The invention also relates to shaped parts containing at least two parts that are in contact with each other via a boundary face, each of these parts comprising a different polymer, which polymers are essentially incompatible polymers and contain functional hydroxy groups and/or functional amino groups and with at least one of said polymers having reacted with carbonyl bislactam or containing carbonyl bislactam. The invention also relates to a process for the preparation of said shaped part. The shaped part can be prepared by means of coextrusion, insert moulding or overmoulding.
摘要翻译：本发明涉及一种聚合物组合物以及制备这种组合物的方法，其中两种或多种基本上不相容的聚合物（各自含有官能羟基和/或官能氨基）在存在下彼此接触至少一种增容剂，相容剂是具有式（I）结构的羰基双内酰胺（CBL），其中n为3至15的整数，优选为5。优选地，增容剂为羰基双己内酰胺。根据功能性-OH或-NH> 2 <基团与CBL的数目的比例，该组合物可用作聚合物分散体，例如用于改善耐冲击性或VICAT，或作为共聚物。本发明还涉及通过边界面彼此接触的至少两个部分的成形部件，这些部件中的每一个都包含不同的聚合物，该聚合物基本上是不相容的聚合物并且含有官能羟基和/或官能氨基并且所述聚合物中的至少一种与羰基双内酰胺或含有羰基双内酰胺反应。本发明还涉及一种用于制备所述成形部件的方法。成形部件可以通过共挤出，嵌入成型或包覆成型制备。

4. 发明申请

WO2005028541A2 PROCESS FOR THE PREPARATION OF A POLYMER COMPOSITION 审中-公开
标题翻译：制备聚合物组合物的方法
公开(公告)号：WO2005028541A2
公开(公告)日：2005-03-31
申请号：PCT/NL2004/000645
申请日：2004-09-17
申请人： DSM IP ASSETS B.V. , LOONTJENS, Jacobus, Antonius
发明人： LOONTJENS, Jacobus, Antonius
IPC分类号： C08G69/00
CPC分类号： C08G63/91
摘要： The invention relates to a process for the preparation of a polymer composition, the process comprising a step of contacting a polymer that comprises carboxyl groups with a cyclic imino ether compound characterized in that the cyclic imino ether compound is a phenylene oxazine according to formula (I), in which formula R = an oxazine group according to formula (II) n = 0, 1, 2, 3, 4 or 5 and that the polymer is contacted with said oxazine in an extruder at a temperature above 100 °C
摘要翻译：本发明涉及一种制备聚合物组合物的方法，该方法包括使包含羧基的聚合物与环状亚氨基醚化合物接触的步骤，其特征在于环状亚氨基醚化合物是式（I ），式中R =根据式（II）的恶嗪基n = 0,1,2,3,4或5，并且聚合物在挤出机中在高于100℃的温度下与所述恶嗪接触

5. 发明申请

WO2007068460A1 BIOCIDAL COATINGS 审中-公开
标题翻译：生物涂料
公开(公告)号：WO2007068460A1
公开(公告)日：2007-06-21
申请号：PCT/EP2006/011982
申请日：2006-12-13
申请人： DSM IP ASSETS B.V. , LOONTJENS, Jacobus, Antonius , URMANOVA, Antonia , DIJCK, VAN, Michael, Alphonsus, Cornelis, Johannes
发明人： LOONTJENS, Jacobus, Antonius , URMANOVA, Antonia , DIJCK, VAN, Michael, Alphonsus, Cornelis, Johannes
IPC分类号： C08G63/685 , C08G63/692 , C09D167/02 , C09D177/12
CPC分类号： C09D5/14 , C09D167/00 , C08L2666/28
摘要： The invention relates to a polymer with an incorporated biocidal component. The invention also relates to a crosslinker with an incorporated biocidal component, the invention further relates to a composition comprising either the biocidal polymer or crosslinker or both, to a substrate fully or partially coated with a biocidal composition and its use in coatings.
摘要翻译：本发明涉及具有结合的杀生物成分的聚合物。本发明还涉及具有结合的杀生物成分的交联剂，本发明还涉及包含杀生物聚合物或交联剂或两者的组合物与完全或部分涂覆有杀生物剂组合物的底物及其在涂料中的用途。

6. 发明申请

WO2007009540A1 POLYCONDENSATE FIBERS 审中-公开
标题翻译：聚碳酸酯纤维
公开(公告)号：WO2007009540A1
公开(公告)日：2007-01-25
申请号：PCT/EP2006/005762
申请日：2006-06-13
申请人： DSM IP ASSETS B.V. , LOONTJENS, Jacobus, Antonius , VAN DER WERFF, Harm , DORSCHU, Marko , CUYPERS, Theo, Joseph
发明人： LOONTJENS, Jacobus, Antonius , VAN DER WERFF, Harm , DORSCHU, Marko , CUYPERS, Theo, Joseph
IPC分类号： C08G63/91 , C08G77/445 , D01F6/92
CPC分类号： D01F6/92 , C08G63/916 , C08G77/445
摘要： The invention relates to a method of increasing the molecular mass of a polycondensate in solution, wherein polycondensate is reacted with at least one chain extender out of the group consisting of bislactams, cyclic amino ethers, siloxanes and thiols. The invention further relates to a high molecular mass polycondensate in solution, wherein the polycondensate has an intrinsic viscosity as measured in hexafluoroisopropanol of at least 0.9 dl/g and a molecular mass distribution (Mw/Mn) of less than (2). The invention further relates to a process for producing a filament or film of a polycondensate comprising forming a solution of polycondensate by the method according to the invention, extruding the solution through a spinneret or a slot die, through air and into a cooling bath to form a gel filament or film, optionally removing residual solvent from the filament or film and drawing the filament or film at least (15), preferably at least (25) times. The invention further relates to shaped articles obtainable by the process thereof.
摘要翻译：本发明涉及增加溶液中缩聚物分子量的方法，其中缩聚物与至少一种由双内酰胺，环氨基醚，硅氧烷和硫醇组成的组中的扩链剂反应。本发明还涉及溶液中的高分子质量缩聚物，其中缩聚物具有至少0.9dl / g的六氟异丙醇测得的特性粘度和小于（2）的分子量分布（Mw / Mn）。本发明还涉及一种生产缩聚物的长丝或薄膜的方法，包括通过本发明的方法形成缩聚物溶液，通过喷丝头或狭槽模头将溶液通过空气挤出并进入冷却浴中形成凝胶丝或薄膜，任选地从丝或薄膜中除去残留的溶剂，并将丝或薄膜拉伸至少（15），优选至少（25）次。本发明还涉及通过其方法可获得的成型制品。

7. 发明申请

WO2006025738A1 POLYESTER PREPARED FROM PHOSPHORIC ACID OR ITS OLIGOMERS 审中-公开
标题翻译：由磷酸酯或其低聚物制备的聚酯
公开(公告)号：WO2006025738A1
公开(公告)日：2006-03-09
申请号：PCT/NL2005/000632
申请日：2005-09-01
申请人： DSM IP ASSETS B.V. , PENCZEK, Stanislaw , LOONTJENS, Jacobus, Antonius , KALUZYNSKI, Krzysztof , PRETULA, Julia
发明人： PENCZEK, Stanislaw , LOONTJENS, Jacobus, Antonius , KALUZYNSKI, Krzysztof , PRETULA, Julia
IPC分类号： C08G79/04
CPC分类号： C08G79/04
摘要： The invention relates to new, substantially linear polyesters directly prepared from phosphoric acid and/or its oligomers and at least one polyol. The new polyesters can generally be represented by Formula (1). Also a method for the preparation of these new, substantially linear polyesters is developed. The new, substantially linear polyesters can be used in the binder of a coating compostion; they can also be used in other compositions as a flame-retardant or as a primer or adhesion improver.
摘要翻译：本发明涉及由磷酸和/或其低聚物和至少一种多元醇直接制备的新的基本上线性的聚酯。新的聚酯通常可以由式（1）表示。还开发了制备这些新的基本上线性的聚酯的方法。新的基本上线性的聚酯可以用于涂料组合物的粘合剂中; 它们也可以用作其它组合物作为阻燃剂或底漆或粘合改进剂。

8. 发明申请

WO2004020501A1 PROCESS FOR PREPARING BIOCOMPATIBLE POLYUREA 审中-公开
标题翻译：制备生物降解聚氨酯的方法
公开(公告)号：WO2004020501A1
公开(公告)日：2004-03-11
申请号：PCT/NL2003/000567
申请日：2003-08-07
申请人： DSM IP ASSETS B.V. , MÜLHAUPT, Rolf , LOONTJENS, Jacobus, Antonius , MAIER, Steffen , ZIMMERMANN, Jörg
发明人： MÜLHAUPT, Rolf , LOONTJENS, Jacobus, Antonius , MAIER, Steffen , ZIMMERMANN, Jörg
IPC分类号： C08G71/02
CPC分类号： C08G71/02
摘要： A process is provided for preparing urea-containing polymers by contacting a hydroxy-functional organic compound having a functionality of two or more, with a coupling agent in the presence of a strong base, wherein the coupling agent is a carbonylbislactam compound having the general formula (I): wherein n is an integer from 3 to 15, and that the contacting is conducted at a temperature between 0°C and 80°C. The polymers thus obtained are believed to be new and are useful e.g. in tissue engineering and coatings applications.
摘要翻译：提供了一种制备含尿素聚合物的方法，其通过使具有两个或多个官能度的羟基官能的有机化合物与强碱的存在下与偶联剂接触，其中偶联剂是具有通式的羰基双内酰胺化合物（I）：其中n为3至15的整数，并且接触在0℃和80℃之间的温度下进行。由此获得的聚合物被认为是新的并且可用于例如在组织工程和涂料应用中。

9. 发明申请

WO2004046156A1 SILANE COUPLING AGENT, PROCESS FOR THE PREPARATION OF A SILANE COUPLING AGENT, USE OF SAID SILANE COUPLING AGENT IN A COMPOSITE OR ON A SUBSTRATE, NANOPARTICLES AND USE THEREOF IN A COATING. 审中-公开
标题翻译：硅烷偶联剂，制备硅烷偶联剂的方法，在复合材料中或在基材上使用表面的硅烷偶联剂，纳米材料及其在涂料中的用途。
公开(公告)号：WO2004046156A1
公开(公告)日：2004-06-03
申请号：PCT/NL2003/000787
申请日：2003-11-10
申请人： DSM IP ASSESTS B.V. , LOONTJENS, Jacobus, Antonius , PLUM, Bartholomeus, Johannes, Margretha , MULHAUPT, Rolf , MAIER, Steffen
发明人： LOONTJENS, Jacobus, Antonius , PLUM, Bartholomeus, Johannes, Margretha , MULHAUPT, Rolf , MAIER, Steffen
IPC分类号： C07F7/18
CPC分类号： C07F7/1836
摘要： The invention relates to a novel silane coupling agent according to Formula (1) below, wherein Y = a chain composed of aliphatic, cyclic or aromatic groups, furthermore comprising an additional reactive group chosen from the series of a secondary amine, a amine linked to a secondary or tertiary carbon atom or a hydroxyl group linked to a primary, secondary or tertiary carbon atom. R, R'= CH 3 or C 2 H 5 , n = 3-15, q = 1, 2 or 3 and p = 3-q. The invention also relates to the use of the coupling agent according to the invention in a composite, for example in a dental application. The invention further relates to a process for the preparation of a silane coupling agent by reacting, at a temperature lower than 150° C, a carbonyl bislactamate with a silane compound containing at least one amino group. The invention moreover relates to nano particles, in particular nano silicate particles, obtained by hydrolysis of the coupling agent according to the above formula in the presence or absence of tetraethoxysilane and to the use of such particles in a coating.
摘要翻译：本发明涉及根据下式（1）的新型硅烷偶联剂，其中Y =由脂族，环状或芳族基团组成的链，此外还包含另外的反应性基团，其选自一系列仲胺，连接到仲或叔碳原子或与伯，仲或叔碳原子连接的羟基。 R，R'= CH 3或C 2 H 5，n = 3-15，q = 1,2或3，p = 3-q。本发明还涉及根据本发明的偶联剂在复合材料中的用途，例如在牙科应用中。本发明还涉及一种通过在低于150℃的温度下使双氨基甲酸羰基酯与含有至少一个氨基的硅烷化合物反应来制备硅烷偶联剂的方法。此外，本发明涉及通过在存在或不存在四乙氧基硅烷的情况下水解根据上式的偶联剂获得的纳米颗粒，特别是纳米硅酸盐颗粒，以及在涂层中使用这种颗粒。

10. 发明申请

WO2003070704A1 METHOD FOR THE PREPARATION OF ETHYLENICALLY UNSATURATED COMPOUNDS WITH LACTAM-BLOCKED ISOCYANATE GROUPS 审中-公开
标题翻译：用LACTAM阻断的异氰酸酯基团制备乙烯不饱和化合物的方法
公开(公告)号：WO2003070704A1
公开(公告)日：2003-08-28
申请号：PCT/NL2003/000134
申请日：2003-02-20
申请人： DSM N.V. , LOONTJENS, Jacobus, Antonius
发明人： LOONTJENS, Jacobus, Antonius
IPC分类号： C07D223/10
CPC分类号： C08G18/672 , C07D223/10 , C08G18/8074 , C08G18/8116
摘要： The invention relates to a method for the preparation of ethylenically unsaturated lactam-blocked isocyanate compounds, by reacting an unsaturated amine-functional or hydroxy-functional compound with carbonylbislactam. These compounds can be polymerised and are subsequently cured by the built-in crosslinker to form thermosetting polymers which can be applied for instance in powder coatings.
摘要翻译：本发明涉及通过使不饱和胺官能化或羟基官能化合物与羰基双内酰胺反应来制备烯键式不饱和内酰胺封端异氰酸酯化合物的方法。这些化合物可以被聚合并随后通过内置的交联剂固化以形成可用于例如粉末涂料中的热固性聚合物。

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