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1. 发明申请

WO2016099829A1 PROCESS FOR PRODUCING A COMPOSITE ARTICLE 审中-公开
标题翻译：生产复合材料的方法
公开(公告)号：WO2016099829A1
公开(公告)日：2016-06-23
申请号：PCT/US2015/062438
申请日：2015-11-24
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： SHAFI, Asjad , KARUNAKARAN, Krishnan , VYAKARANAM, Kamesh R.
IPC分类号： B29C70/32 , C08J5/24 , B29C53/56
CPC分类号： C08J5/04 , B29C53/58 , B29C2035/0827 , B29D23/001 , C08J3/243 , C08J2363/10
摘要： A multistage filament winding process for manufacturing a composite article using a dual chemistry formulation including the steps of (a) providing a dual chemistry formulation containing components to effectuate dual cure of the formulation; (b) winding fibers on a liner or on a mandrel; (c) impregnating the wound fibers of step (b) with the dual chemistry formulation; (d) activating a first reaction (A) by UV or thermal-free radical initiation sufficient to form first macroscopic gels and to allow the first macroscopic gels to phase separate from the remaining substantially unreacted components in the formulation; (e) optionally, activating a second reaction by heating through IR lamps or other heating apparatus and controlling the second reaction sufficient to form second macroscopic gels subsequent to the formation of the first macroscopic gels which have gelled and phase separated in the formulation; (f) repeating steps (a)-(d) until a composite article having a predetermined thickness is formed; and (g) heating the formed composite article of step (f) sufficient to form a final composite article product having a predetermined glass transition temperature; a cured thermoset article prepared by the above process; and a process for manufacturing spoolable pipe.
摘要翻译：一种用于使用双重化学制剂制造复合制品的多级丝缠绕方法，包括以下步骤：（a）提供含有组分以实现制剂双重固化的双重化学配方; （b）将纤维缠绕在衬里或心轴上; （c）用双重化学制剂浸渍步骤（b）的缠绕纤维; （d）通过紫外线或热自由基引发活化第一反应（A），足以形成第一宏观凝胶并允许第一宏观凝胶与制剂中剩余的基本上未反应的组分相分离; （e）任选地，通过加热IR灯或其它加热装置来激活第二反应，并且控制第二反应足以形成第二宏观凝胶，所述第一宏观凝胶在制剂中胶凝和相分离; （f）重复步骤（a） - （d），直到形成具有预定厚度的复合制品; 和（g）加热步骤（f）的形成的复合制品足以形成具有预定玻璃化转变温度的最终复合制品产品; 通过上述方法制备的固化的热固性物品; 以及制造可缠绕管的工艺。

2. 发明申请

WO2014186031A1 AMINIC HARDENERS WITH IMPROVED CHEMICAL RESISTANCE 审中-公开
标题翻译：具有改善化学电阻的氨基硬化剂
公开(公告)号：WO2014186031A1
公开(公告)日：2014-11-20
申请号：PCT/US2014/022600
申请日：2014-03-10
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： KARUNAKARAN, Krishnan , TURAKHIA, Rajesh H. , RIPPLINGER, Eric B.
IPC分类号： C08G59/18 , C08G59/50
CPC分类号： C08L63/04 , C08G59/184 , C08G59/5006 , C08G59/5026 , C08L2205/24
摘要： A hardener composition comprising: a) an epoxy-amine adduct of i) a novolac epoxy resin; and ii) a first amine and b) a modifier wherein the hardener has a viscosity in the range of from 50 to 20,000 mPa.s and wherein a cured epoxy thermoset comprising the hardener exhibits no more than 1 % weight loss or gain after immersion in concentrated mineral acid for 7 days at a temperature in the range of from 25ºC to 130ºC, is disclosed. The hardener composition can be used with an epoxy resin to form a curable composition.
摘要翻译： 1.一种固化剂组合物，其包含：a）i）酚醛清漆环氧树脂的环氧 - 胺加合物; 和ii）第一胺和b）改性剂，其中所述固化剂具有在50至20,000mPa.s范围内的粘度，并且其中包含所述固化剂的固化的环氧热固性材料在浸渍之后不超过1重量％的重量损失或增益公开了在25℃至130℃的温度范围内的浓缩无机酸7天。固化剂组合物可与环氧树脂一起使用以形成可固化组合物。

3. 发明申请

WO2015094629A1 CURABLE COMPOSITIONS 审中-公开
标题翻译：可固化组合物
公开(公告)号：WO2015094629A1
公开(公告)日：2015-06-25
申请号：PCT/US2014/067995
申请日：2014-12-02
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： KARUNAKARAN, Krishnan , DETTLOFF, Marvin L. , VERGHESE, Nikhil K. E. , PHAM, Ha Q.
IPC分类号： C08J3/24 , C08L83/00
CPC分类号： C08G59/50 , C08F283/065 , C08G59/245 , C08G59/4215 , C08J3/243 , C08J3/246 , C08J2363/02 , C08K5/14 , C08L51/08 , C08L63/00 , C08L83/00 , C08L51/00 , C08L71/00
摘要： A dual cure system including at least two different and separate types of chemical reactions occurring as the process of the present invention proceeds including, for example, the following two reactions: (1) free radical polymerization of methacrylated or acrylated polyol; and (2) an epoxy - curing agent reaction. The dual cure system of the present invention advantageously provides a first cure reaction of methacrylated or acrylated polyol followed by a second epoxy-curing agent thermoset reaction to form a cured thermoset exhibiting an elongation property of greater than about 5 %.
摘要翻译：包括如本发明的方法发生的至少两种不同和分开的化学反应类型的双重固化体系包括例如以下两个反应：（1）甲基丙烯酸酯化或丙烯酸酯化的多元醇的自由基聚合; 和（2）环氧固化剂反应。本发明的双重固化体系有利地提供了甲基丙烯酸酯化或丙烯酸酯化的多元醇的第一固化反应，然后进行第二次环氧固化剂热固化反应以形成展现出大于约5％的伸长率的固化的热固性材料。

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